#------------------------------------------------------------------------------ #$Date: 2022-12-24 22:12:14 +0200 (Sat, 24 Dec 2022) $ #$Revision: 280037 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519436.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519436 _cell_angle_alpha 90.000 _cell_angle_beta 98.829 _cell_angle_gamma 90.000 _cell_length_a 18.6780 _cell_length_b 10.7344 _cell_length_c 16.0745 _exptl_crystal_F_000 1736.00 _reflns_d_resolution_high 0.7693 _cod_data_source_file 3-ada138.fcf _cod_data_source_block ada138 _shelx_title ' ada138_a.res in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 392.95 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3094.42 4377.49 122.52 o 4 0 0 14643.25 20012.05 818.40 o 6 0 0 174.80 180.73 6.28 o 8 0 0 59873.84 80780.80 3804.93 o 10 0 0 2544.96 2263.08 57.25 o 12 0 0 1524.08 1699.60 75.89 o 14 0 0 7574.80 7443.12 172.17 o 16 0 0 1351.42 1024.08 35.53 o 18 0 0 6173.04 5190.61 169.81 o 20 0 0 2253.22 2084.42 56.27 o 22 0 0 585.83 563.15 29.66 o 1 1 0 15963.54 10161.74 330.62 o 3 1 0 15303.60 13325.60 371.05 o 5 1 0 30782.23 25663.45 636.88 o 7 1 0 1513.42 951.15 31.86 o 9 1 0 1267.50 1023.36 17.83 o 11 1 0 2957.10 3456.28 75.92 o 13 1 0 737.90 607.12 12.44 o 15 1 0 1186.30 1175.31 33.19 o 17 1 0 28.07 23.15 2.67 o 19 1 0 3691.15 3128.00 64.70 o 21 1 0 85.45 89.14 3.57 o 23 1 0 448.48 474.32 13.61 o 0 2 0 25754.80 24289.21 992.52 o 2 2 0 104.48 133.12 3.84 o 4 2 0 13342.20 13290.81 378.27 o 6 2 0 1401.74 1689.96 34.18 o 8 2 0 6163.72 6548.56 132.05 o 10 2 0 8.51 7.42 1.36 o 12 2 0 3501.39 3463.70 79.11 o 14 2 0 3.82 2.27 1.90 o 16 2 0 786.61 693.81 14.90 o 18 2 0 1160.70 1001.85 52.56 o 20 2 0 44.48 48.17 3.29 o 22 2 0 8.01 11.94 4.83 o 1 3 0 215.32 195.40 5.37 o 3 3 0 3105.34 2776.48 60.73 o 5 3 0 5465.63 5871.20 117.53 o 7 3 0 14052.82 15740.65 280.83 o 9 3 0 2823.10 2963.69 40.53 o 11 3 0 252.29 230.62 5.15 o 13 3 0 2211.58 2241.65 37.03 o 15 3 0 1104.38 1009.66 29.07 o 17 3 0 1552.55 1514.62 30.62 o 19 3 0 982.53 807.39 16.64 o 21 3 0 243.30 231.54 6.25 o 23 3 0 87.35 94.38 3.63 o 0 4 0 28218.51 33904.58 2778.65 o 2 4 0 197.49 229.24 5.76 o 4 4 0 815.73 1118.73 29.76 o 6 4 0 116.64 238.93 4.27 o 8 4 0 10988.20 11592.87 192.61 o 10 4 0 1289.57 1324.18 19.11 o 12 4 0 7253.84 7957.65 210.91 o 14 4 0 588.48 597.82 11.12 o 16 4 0 1983.02 1695.87 74.36 o 18 4 0 471.12 475.31 14.99 o 20 4 0 448.22 442.01 8.55 o 22 4 0 25.71 30.93 2.50 o 1 5 0 1756.94 1735.74 31.84 o 3 5 0 74.13 139.38 3.29 o 5 5 0 14106.68 15847.97 242.91 o 7 5 0 3380.54 3940.88 76.10 o 9 5 0 982.75 989.40 15.59 o 11 5 0 8596.67 8623.30 136.93 o 13 5 0 7447.58 7525.91 125.65 o 15 5 0 1248.11 1079.54 19.88 o 17 5 0 185.34 187.68 5.64 o 19 5 0 666.29 686.41 19.44 o 21 5 0 39.18 41.35 3.60 o 0 6 0 1226.36 1553.14 33.81 o 2 6 0 14382.10 15220.48 230.02 o 4 6 0 70.60 91.19 2.41 o 6 6 0 70.53 57.35 2.14 o 8 6 0 560.17 591.03 10.63 o 10 6 0 1678.21 1652.41 23.78 o 12 6 0 3590.38 3748.92 88.93 o 14 6 0 1851.35 1804.93 33.42 o 16 6 0 2188.60 1981.58 99.46 o 18 6 0 114.51 122.87 11.35 o 20 6 0 714.07 750.07 17.78 o 1 7 0 375.58 330.85 5.71 o 3 7 0 1711.24 1680.68 25.92 o 5 7 0 43.15 49.62 1.80 o 7 7 0 10297.88 11185.17 250.40 o 9 7 0 38.54 45.16 2.16 o 11 7 0 3255.10 3502.30 62.20 o 13 7 0 1181.84 1129.27 23.35 o 15 7 0 101.66 88.79 3.30 o 17 7 0 741.15 733.80 19.33 o 19 7 0 222.17 228.49 8.61 o 0 8 0 31.47 36.73 2.76 o 2 8 0 6424.86 6002.37 91.10 o 4 8 0 1154.37 1092.44 20.83 o 6 8 0 1457.83 1364.73 25.72 o 8 8 0 977.34 995.77 19.09 o 10 8 0 89.22 82.37 3.08 o 12 8 0 1843.47 1951.18 53.47 o 14 8 0 188.00 192.93 5.75 o 16 8 0 703.85 730.04 22.18 o 18 8 0 121.15 109.17 4.47 o 1 9 0 1092.41 1063.34 19.65 o 3 9 0 2966.17 2767.66 105.81 o 5 9 0 1654.18 1562.37 28.47 o 7 9 0 466.74 454.68 15.92 o 9 9 0 0.63 4.17 1.83 o 11 9 0 1290.49 1176.03 35.66 o 13 9 0 35.81 30.68 2.79 o 15 9 0 42.42 34.99 2.50 o 17 9 0 32.83 42.15 3.77 o 0 10 0 1907.29 1707.15 47.80 o 2 10 0 1668.49 1608.99 29.29 o 4 10 0 217.73 211.76 5.75 o 6 10 0 50.74 49.74 2.51 o 8 10 0 748.41 738.81 22.63 o 10 10 0 381.44 416.82 9.22 o 12 10 0 255.09 278.00 16.02 o 14 10 0 127.22 151.28 5.67 o 16 10 0 53.04 57.79 4.17 o 1 11 0 1882.41 1888.89 34.19 o 3 11 0 358.45 351.18 8.11 o 5 11 0 87.62 103.03 3.21 o 7 11 0 1490.97 1759.73 47.66 o 9 11 0 305.80 269.91 5.79 o 11 11 0 404.92 441.54 14.32 o 13 11 0 601.21 632.29 19.48 o 0 12 0 362.20 335.28 10.62 o 2 12 0 128.72 139.37 4.38 o 4 12 0 944.80 753.25 20.09 o 6 12 0 432.46 417.69 9.83 o 8 12 0 307.52 328.24 11.12 o 10 12 0 9.74 13.85 2.46 o 12 12 0 395.72 427.65 22.45 o 1 13 0 106.97 118.85 4.47 o 3 13 0 10.12 13.02 3.42 o 5 13 0 629.19 706.02 16.82 o 7 13 0 90.25 108.66 5.15 o -18 0 4 113.29 98.17 6.32 o -12 0 2 6355.03 5642.71 183.31 o 4 0 0 4759.28 5064.90 293.04 o -4 0 2 523.42 597.40 30.55 o -18 0 6 426.62 326.00 16.13 o -23 1 1 113.63 112.87 4.39 o -21 1 1 31.47 32.37 2.48 o -19 1 1 2015.08 1914.08 40.00 o -17 1 1 338.36 292.61 7.10 o -15 1 1 2919.37 2200.30 42.86 o -13 1 1 31.47 38.26 2.40 o -11 1 1 3455.73 3665.50 88.82 o -9 1 1 6149.62 6896.57 123.04 o -7 1 1 2248.11 2002.00 99.99 o -5 1 1 13119.25 14229.99 299.61 o -3 1 1 3016.19 3918.33 73.89 o -1 1 1 33818.83 48600.38 1986.05 o 1 1 1 15705.13 10433.64 339.09 o 3 1 1 18861.30 15615.57 383.01 o 5 1 1 2111.58 2154.27 43.43 o 7 1 1 9819.02 11429.87 408.84 o 9 1 1 15437.57 17747.47 310.12 o 11 1 1 10374.37 11181.20 237.22 o 13 1 1 943.81 945.75 20.04 o 15 1 1 536.21 526.08 10.75 o 17 1 1 1205.51 1112.76 24.10 o 19 1 1 171.01 140.22 4.09 o 21 1 1 586.53 576.99 11.83 o 23 1 1 524.01 570.27 29.67 o -22 2 1 75.80 97.01 7.05 o -20 2 1 1742.84 1809.48 38.14 o -18 2 1 317.82 266.56 8.81 o -16 2 1 2894.52 2992.41 55.74 o -14 2 1 4714.19 4696.51 76.75 o -12 2 1 736.25 770.35 27.52 o -10 2 1 2918.29 2357.74 41.10 o -8 2 1 694.39 854.39 14.98 o -6 2 1 4922.27 4312.70 81.12 o -4 2 1 7373.70 7458.79 154.88 o -2 2 1 2025.57 1824.46 41.77 o 0 2 1 138.99 225.04 9.06 o 2 2 1 746.65 646.19 16.41 o 4 2 1 34601.75 44721.70 1336.17 o 6 2 1 2163.97 2477.93 46.95 o 8 2 1 8774.65 8765.44 169.01 o 10 2 1 430.40 449.18 8.06 o 12 2 1 13960.23 14377.39 334.42 o 14 2 1 465.46 442.60 8.80 o 16 2 1 1295.65 1354.27 25.31 o 18 2 1 917.39 970.71 31.85 o 20 2 1 51.79 49.05 3.16 o 22 2 1 628.13 626.63 23.34 o -23 3 1 136.84 153.50 4.46 o -21 3 1 24.11 35.76 2.79 o -19 3 1 1530.20 1469.76 33.60 o -17 3 1 693.91 688.59 13.99 o -15 3 1 1198.44 899.82 19.59 o -13 3 1 5287.18 5185.45 84.60 o -11 3 1 2681.63 2698.58 50.78 o -9 3 1 1144.59 1443.92 21.52 o -7 3 1 2662.15 3004.67 65.94 o -5 3 1 4544.02 4713.04 110.68 o -3 3 1 1033.99 928.05 20.90 o -1 3 1 35693.44 47018.59 1924.38 o 1 3 1 30002.34 34995.43 1168.07 o 3 3 1 2519.71 1988.39 172.13 o 5 3 1 11769.83 13561.37 278.75 o 7 3 1 1606.77 1534.37 26.88 o 9 3 1 168.56 155.82 2.72 o 11 3 1 1489.20 1555.30 28.79 o 13 3 1 3814.05 3802.77 62.21 o 15 3 1 8944.66 8188.99 146.58 o 17 3 1 3638.94 3283.94 59.55 o 19 3 1 314.82 350.12 9.95 o 21 3 1 766.57 832.60 18.05 o 23 3 1 297.42 349.04 8.65 o -22 4 1 206.96 147.68 11.85 o -20 4 1 76.37 109.77 3.66 o -18 4 1 2986.40 2721.69 89.53 o -16 4 1 1820.61 1773.04 35.62 o -14 4 1 868.06 813.01 15.71 o -12 4 1 846.97 757.50 14.02 o -10 4 1 2.82 8.70 1.30 o -8 4 1 6464.06 7487.93 141.96 o -6 4 1 4.64 9.32 2.05 o -4 4 1 2165.83 2340.91 78.83 o -2 4 1 119.48 199.51 6.12 o 0 4 1 288.01 379.52 14.47 o 2 4 1 2929.21 3308.07 69.82 o 4 4 1 1895.70 2087.57 58.41 o 6 4 1 716.82 657.38 11.33 o 8 4 1 47.35 22.43 2.35 o 10 4 1 2363.88 2280.14 31.98 o 12 4 1 694.61 637.42 14.18 o 14 4 1 1664.63 1555.73 28.70 o 16 4 1 39.26 41.70 3.05 o 18 4 1 944.12 812.67 28.06 o 20 4 1 1328.63 1306.27 25.58 o 22 4 1 496.74 559.21 15.47 o -21 5 1 300.01 265.87 7.23 o -19 5 1 918.47 835.76 21.70 o -17 5 1 3897.97 3933.13 85.17 o -15 5 1 351.28 303.65 8.38 o -13 5 1 1846.51 1789.01 33.14 o -11 5 1 6191.87 6936.39 112.80 o -9 5 1 1681.61 1670.64 23.29 o -7 5 1 527.64 511.18 11.86 o -5 5 1 4362.83 5184.13 84.76 o -3 5 1 25649.94 29860.32 485.80 o -1 5 1 4346.56 4714.18 82.57 o 1 5 1 5191.72 4593.64 76.51 o 3 5 1 5496.28 6541.79 114.38 o 5 5 1 1561.03 1450.16 22.66 o 7 5 1 3476.92 3800.07 62.88 o 9 5 1 2476.35 2605.27 39.93 o 11 5 1 3694.90 3792.10 60.88 o 13 5 1 3926.26 3761.92 67.23 o 15 5 1 1608.85 1226.21 23.42 o 17 5 1 101.15 105.28 3.78 o 19 5 1 1784.46 1669.81 38.21 o 21 5 1 61.11 75.90 3.40 o -20 6 1 158.82 146.06 4.77 o -18 6 1 1545.22 1536.25 77.64 o -16 6 1 1005.18 1014.55 52.88 o -14 6 1 407.53 378.79 8.15 o -12 6 1 2918.63 2962.65 70.58 o -10 6 1 5840.80 5903.56 83.20 o -8 6 1 2551.84 2638.03 45.90 o -6 6 1 59.76 58.27 2.07 o -4 6 1 181.88 189.36 4.45 o -2 6 1 9921.83 10497.23 158.79 o 0 6 1 4182.83 4030.08 68.31 o 2 6 1 12626.90 14573.44 208.97 o 4 6 1 8880.73 9921.14 160.89 o 6 6 1 70.13 89.70 2.22 o 8 6 1 3287.63 3625.61 58.75 o 10 6 1 3196.27 3183.11 45.15 o 12 6 1 2091.67 1971.54 41.44 o 14 6 1 247.71 234.59 5.73 o 16 6 1 3168.59 3311.26 60.38 o 18 6 1 410.01 367.27 21.96 o 20 6 1 198.60 193.10 5.64 o -19 7 1 60.78 52.05 3.13 o -17 7 1 228.63 246.54 7.80 o -15 7 1 21.14 21.49 2.54 o -13 7 1 1114.83 1134.46 20.83 o -11 7 1 309.75 321.08 8.34 o -9 7 1 7.83 12.15 1.63 o -7 7 1 368.49 365.88 8.59 o -5 7 1 123.32 128.00 2.92 o -3 7 1 1662.19 1802.45 27.81 o -1 7 1 3171.35 3465.85 52.83 o 1 7 1 64.38 70.60 2.22 o 3 7 1 1958.52 2007.10 109.22 o 5 7 1 7.47 3.72 1.16 o 7 7 1 169.76 162.85 5.50 o 9 7 1 457.71 482.39 8.53 o 11 7 1 1794.78 1733.07 33.91 o 13 7 1 953.02 965.10 20.13 o 15 7 1 8.15 4.66 2.20 o 17 7 1 164.85 166.53 5.93 o 19 7 1 765.44 743.57 28.59 o -18 8 1 844.24 883.98 51.11 o -16 8 1 173.74 173.33 6.97 o -14 8 1 191.89 176.54 6.22 o -12 8 1 620.79 597.62 22.01 o -10 8 1 389.98 395.99 7.71 o -8 8 1 2799.62 2893.17 79.81 o -6 8 1 133.35 108.17 3.26 o -4 8 1 3469.23 3272.96 78.11 o -2 8 1 63.94 62.58 2.20 o 0 8 1 1780.77 1748.87 27.79 o 2 8 1 2475.12 2501.43 38.32 o 4 8 1 2284.91 2135.11 36.55 o 6 8 1 1803.76 1792.11 29.50 o 8 8 1 331.46 340.15 7.42 o 10 8 1 1285.94 1247.67 22.51 o 12 8 1 2069.18 1956.44 66.14 o 14 8 1 18.29 21.20 2.47 o 16 8 1 241.22 245.19 7.42 o 18 8 1 8.56 7.45 3.06 o -17 9 1 318.62 311.53 8.37 o -15 9 1 386.44 329.33 10.97 o -13 9 1 1326.70 1416.12 28.64 o -11 9 1 150.82 86.16 4.91 o -9 9 1 3734.89 3797.55 69.91 o -7 9 1 1247.61 1230.22 38.71 o -5 9 1 1238.96 1229.16 22.58 o -3 9 1 7148.69 7189.66 272.67 o -1 9 1 744.61 792.46 14.87 o 1 9 1 1705.44 1726.66 31.36 o 3 9 1 1382.46 1296.15 50.96 o 5 9 1 1853.90 1817.82 35.89 o 7 9 1 781.31 934.81 26.16 o 9 9 1 269.23 270.17 5.93 o 11 9 1 1367.38 1600.46 34.91 o 13 9 1 570.06 549.56 12.24 o 15 9 1 1005.55 1051.82 31.76 o 17 9 1 20.26 28.74 3.45 o -16 10 1 35.58 42.21 3.43 o -14 10 1 611.64 669.54 16.17 o -12 10 1 316.00 314.86 17.66 o -10 10 1 163.41 148.13 4.36 o -8 10 1 2395.50 1634.82 53.55 o -6 10 1 272.75 247.61 5.62 o -4 10 1 302.88 288.49 7.21 o -2 10 1 507.55 522.95 10.18 o 0 10 1 2081.35 1891.18 34.18 o 2 10 1 2615.07 2660.41 47.88 o 4 10 1 58.35 54.05 2.74 o 6 10 1 116.31 128.24 3.66 o 8 10 1 1047.87 1062.29 26.82 o 10 10 1 1444.28 1467.60 27.28 o 12 10 1 73.51 78.95 7.30 o 14 10 1 303.51 326.17 9.92 o 16 10 1 326.49 342.81 12.10 o -13 11 1 347.53 392.44 11.44 o -11 11 1 173.75 196.55 7.57 o -9 11 1 18.63 18.18 2.09 o -7 11 1 172.54 177.63 9.04 o -5 11 1 468.65 386.30 7.96 o -3 11 1 2066.12 1873.66 102.71 o -1 11 1 1571.68 1616.75 31.15 o 1 11 1 856.23 759.76 43.26 o 3 11 1 45.99 45.51 2.53 o 5 11 1 432.23 449.64 9.12 o 7 11 1 114.61 107.60 6.45 o 9 11 1 2.32 4.16 1.82 o 11 11 1 240.61 230.01 8.55 o 13 11 1 214.34 208.99 6.80 o -12 12 1 73.81 81.93 5.42 o -10 12 1 348.36 408.36 11.97 o -8 12 1 650.63 630.32 24.54 o -6 12 1 928.88 943.42 18.94 o -4 12 1 902.12 622.70 17.53 o -2 12 1 216.65 216.99 5.05 o 0 12 1 2306.50 2241.97 45.59 o 2 12 1 31.78 40.93 2.96 o 4 12 1 74.55 73.82 3.67 o 6 12 1 109.37 114.73 3.47 o 8 12 1 875.91 864.10 29.60 o 10 12 1 18.64 21.22 2.61 o -7 13 1 409.69 458.79 31.37 o -5 13 1 746.98 813.22 30.94 o -3 13 1 280.86 300.74 8.74 o -1 13 1 946.94 977.12 26.19 o 1 13 1 345.21 350.16 10.15 o 3 13 1 152.33 160.67 5.51 o 5 13 1 35.01 35.65 2.30 o 7 13 1 370.07 413.51 21.88 o -24 0 2 70.99 107.61 5.38 o -22 0 2 908.66 870.33 45.37 o -20 0 2 1183.91 1094.02 30.41 o -18 0 2 477.29 411.28 17.53 o -16 0 2 2529.60 2548.53 66.39 o -14 0 2 120.77 147.64 5.86 o -12 0 2 19553.00 20437.99 662.62 o -10 0 2 11898.62 15156.85 323.88 o -8 0 2 128674.03 203610.00 11766.65 o -6 0 2 8618.41 8885.77 248.98 o -4 0 2 1610.45 2175.27 99.49 o -2 0 2 32638.88 24792.10 1284.27 o 0 0 2 2006.09 1371.46 58.35 o 2 0 2 16337.83 9741.10 316.48 o 4 0 2 99.06 117.50 4.20 o 6 0 2 23605.84 29776.18 1216.56 o 8 0 2 1895.85 1883.37 53.70 o 10 0 2 134.51 121.27 4.22 o 12 0 2 2031.75 1826.87 81.32 o 14 0 2 1436.07 1320.88 37.27 o 16 0 2 8344.64 7755.63 252.76 o 18 0 2 407.82 352.92 22.05 o 20 0 2 1058.68 1136.68 31.32 o 22 0 2 108.04 126.95 6.21 o -23 1 2 64.65 58.32 2.83 o -21 1 2 1056.54 1016.23 19.97 o -19 1 2 167.85 120.59 5.47 o -17 1 2 925.47 871.94 17.33 o -15 1 2 105.62 90.96 3.30 o -13 1 2 2003.86 1942.01 34.10 o -11 1 2 1294.09 1332.71 27.87 o -9 1 2 4267.84 4926.84 73.97 o -7 1 2 4565.19 4456.72 118.99 o -5 1 2 5962.62 6091.83 107.90 o -3 1 2 48145.07 21846.17 724.71 o -1 1 2 8956.03 8452.32 275.33 o 1 1 2 5175.44 5150.30 99.67 o 3 1 2 5368.88 6524.99 116.13 o 5 1 2 245.98 182.04 4.30 o 7 1 2 13557.73 14881.33 394.07 o 9 1 2 513.38 681.71 13.18 o 11 1 2 4506.98 4303.66 79.21 o 13 1 2 708.53 689.62 12.76 o 15 1 2 105.59 89.69 3.93 o 17 1 2 1711.30 1619.43 34.29 o 19 1 2 922.68 971.18 23.76 o 21 1 2 257.16 281.71 6.46 o 23 1 2 22.44 25.95 2.46 o -22 2 2 28.96 26.47 5.72 o -20 2 2 6.15 4.76 2.38 o -18 2 2 3683.27 2610.09 85.63 o -16 2 2 1237.09 1067.22 34.62 o -14 2 2 7.90 8.51 2.16 o -12 2 2 1878.82 1921.51 64.12 o -10 2 2 1030.35 893.13 14.64 o -8 2 2 4125.94 4472.30 76.22 o -6 2 2 189.64 271.88 5.51 o -4 2 2 22291.05 27983.15 795.00 o -2 2 2 640.62 542.56 11.51 o 0 2 2 16141.11 19739.02 807.70 o 2 2 2 8118.84 7774.02 181.19 o 4 2 2 24363.94 30756.53 784.36 o 6 2 2 31.52 66.64 2.17 o 8 2 2 822.89 884.44 16.52 o 10 2 2 13164.25 14557.69 226.88 o 12 2 2 3140.88 2721.80 61.64 o 14 2 2 7982.20 7868.34 127.86 o 16 2 2 1002.64 903.87 17.31 o 18 2 2 793.96 694.82 25.11 o 20 2 2 99.85 121.93 3.90 o 22 2 2 23.48 26.60 3.92 o -23 3 2 351.46 364.93 12.56 o -21 3 2 252.17 253.06 7.79 o -19 3 2 812.92 626.72 14.43 o -17 3 2 2107.64 1942.06 36.68 o -15 3 2 11249.99 10247.04 199.28 o -13 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