#------------------------------------------------------------------------------ #$Date: 2023-01-04 15:33:13 +0200 (Wed, 04 Jan 2023) $ #$Revision: 280095 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519439.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519439 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.0978 _cell_length_b 18.8577 _cell_length_c 5.7063 _exptl_crystal_F_000 350.23 _reflns_d_resolution_high 0.8103 _cod_data_source_file 03-31DBF_69FLU.fcf _cod_data_source_block dbflu _shelx_title ' jw23062_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 91.29 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6271.35 5955.05 145.91 o 4 0 0 32.64 34.91 1.10 o 6 0 0 532.81 538.06 10.94 o 8 0 0 1.82 1.61 0.29 o 2 1 0 8333.68 7619.54 186.53 o 4 1 0 59.55 65.91 1.26 o 6 1 0 0.81 0.82 0.44 o 8 1 0 17.33 11.50 0.70 o 0 2 0 3328.46 2904.42 71.24 o 2 2 0 385.78 369.22 3.45 o 4 2 0 55.65 49.09 0.97 o 6 2 0 51.70 48.73 1.49 o 8 2 0 36.80 35.98 0.65 o 2 3 0 1493.51 1353.14 11.96 o 4 3 0 2.36 2.19 0.23 o 6 3 0 109.69 101.75 1.60 o 8 3 0 77.12 71.55 1.07 o 0 4 0 1863.53 1755.60 19.39 o 2 4 0 30.91 25.39 0.47 o 4 4 0 92.37 99.10 1.30 o 6 4 0 461.56 416.85 5.28 o 8 4 0 0.26 0.73 0.24 o 2 5 0 89.44 80.92 1.53 o 4 5 0 283.75 279.78 2.93 o 6 5 0 126.15 124.31 2.47 o 8 5 0 119.59 99.89 2.07 o 0 6 0 1268.48 1288.32 14.43 o 2 6 0 537.20 552.67 5.58 o 4 6 0 89.41 97.59 1.33 o 6 6 0 45.61 40.77 0.87 o 8 6 0 0.17 0.60 0.25 o 2 7 0 362.88 375.33 4.33 o 4 7 0 167.93 180.17 2.26 o 6 7 0 170.40 181.03 2.50 o 8 7 0 12.70 15.57 0.72 o 0 8 0 997.72 1035.95 11.82 o 2 8 0 19.52 19.04 0.87 o 4 8 0 263.36 243.57 3.19 o 6 8 0 92.19 90.21 1.24 o 8 8 0 21.45 22.98 0.61 o 2 9 0 1472.43 1595.92 14.36 o 4 9 0 284.94 302.22 3.79 o 6 9 0 13.21 15.51 0.45 o 8 9 0 65.31 76.96 1.22 o 0 10 0 313.68 434.57 5.52 o 2 10 0 195.49 214.07 2.66 o 4 10 0 12.66 17.98 1.26 o 6 10 0 22.88 25.90 0.54 o 8 10 0 124.89 135.63 3.63 o 2 11 0 8.82 4.71 0.38 o 4 11 0 175.02 144.56 2.93 o 6 11 0 8.23 16.20 0.49 o 8 11 0 10.30 6.71 0.39 o 0 12 0 163.07 223.51 4.29 o 2 12 0 206.39 164.42 2.65 o 4 12 0 8.22 4.91 0.28 o 6 12 0 54.55 56.55 1.10 o 8 12 0 143.36 158.59 3.41 o 2 13 0 57.22 34.31 1.14 o 4 13 0 438.79 421.55 4.10 o 6 13 0 6.19 12.26 0.52 o 8 13 0 61.59 63.22 2.53 o 0 14 0 0.49 4.52 0.65 o 2 14 0 42.03 40.68 0.84 o 4 14 0 453.33 464.85 4.59 o 6 14 0 206.21 237.86 4.25 o 2 15 0 326.65 284.02 3.27 o 4 15 0 14.02 7.96 0.41 o 6 15 0 43.08 43.10 0.85 o 0 16 0 46.98 56.08 1.16 o 2 16 0 615.34 560.68 5.63 o 4 16 0 381.66 361.74 3.79 o 6 16 0 7.61 8.50 0.34 o 2 17 0 10.96 7.87 0.39 o 4 17 0 119.67 128.72 1.67 o 6 17 0 10.58 8.27 0.41 o 0 18 0 1.49 2.53 0.35 o 2 18 0 15.76 21.57 0.55 o 4 18 0 2.89 1.38 0.19 o 6 18 0 3.71 1.62 0.15 o 2 19 0 10.30 9.31 0.38 o 4 19 0 64.63 60.22 1.46 o 0 20 0 0.61 0.49 0.19 o 2 20 0 4.79 4.61 0.27 o 4 20 0 0.79 1.63 0.20 o 2 21 0 6.50 6.72 0.36 o 4 21 0 0.02 -0.08 0.16 o 0 22 0 194.56 189.71 8.99 o 2 22 0 48.87 46.81 0.84 o 1 0 1 3986.57 3728.15 45.83 o 2 0 1 4646.14 4671.88 51.40 o 3 0 1 3831.75 3846.48 30.09 o 4 0 1 1192.35 1182.10 9.65 o 5 0 1 58.21 56.90 1.07 o 6 0 1 24.10 22.28 1.16 o 7 0 1 7.02 4.46 0.29 o 8 0 1 12.93 11.28 0.41 o 9 0 1 3.78 4.28 0.37 o 0 1 1 12.53 14.65 0.22 o 1 1 1 6360.29 5886.18 58.93 o 2 1 1 7106.13 7189.29 58.78 o 3 1 1 7.42 8.13 0.42 o 4 1 1 1846.78 1946.74 11.29 o 5 1 1 16.50 15.49 0.41 o 6 1 1 1.77 1.84 0.19 o 7 1 1 20.65 19.52 0.37 o 8 1 1 41.57 43.03 0.53 o 9 1 1 13.84 16.72 0.36 o 1 2 1 19.62 19.14 0.35 o 2 2 1 261.38 290.56 1.89 o 3 2 1 20.17 26.61 0.35 o 4 2 1 7.74 7.71 0.32 o 5 2 1 19.35 18.30 0.46 o 6 2 1 0.93 0.79 0.17 o 7 2 1 5.51 5.99 0.24 o 8 2 1 4.40 5.44 0.24 o 9 2 1 16.67 17.82 0.35 o 0 3 1 512.16 433.92 3.97 o 1 3 1 679.62 648.88 3.94 o 2 3 1 407.59 396.49 2.60 o 3 3 1 31.85 35.59 0.41 o 4 3 1 68.16 63.02 0.67 o 5 3 1 24.10 24.06 0.53 o 6 3 1 68.97 63.71 0.79 o 7 3 1 5.45 5.90 0.26 o 8 3 1 37.17 35.54 0.53 o 9 3 1 29.49 32.53 0.63 o 1 4 1 0.01 0.26 0.15 o 2 4 1 190.26 188.77 1.34 o 3 4 1 51.06 54.07 0.61 o 4 4 1 512.12 508.93 3.63 o 5 4 1 2.37 1.75 0.20 o 6 4 1 9.90 6.14 0.28 o 7 4 1 42.53 39.14 0.60 o 8 4 1 5.59 5.51 0.27 o 9 4 1 0.15 0.27 0.14 o 0 5 1 151.10 141.97 1.43 o 1 5 1 280.60 256.44 1.84 o 2 5 1 178.79 186.71 1.42 o 3 5 1 68.92 70.72 0.74 o 4 5 1 15.18 13.90 0.34 o 5 5 1 300.02 281.49 2.66 o 6 5 1 1.93 1.49 0.17 o 7 5 1 57.34 52.04 0.80 o 8 5 1 93.66 94.56 1.27 o 9 5 1 1.41 1.65 0.16 o 1 6 1 251.09 262.99 1.91 o 2 6 1 109.67 129.63 1.10 o 3 6 1 185.34 187.78 1.54 o 4 6 1 141.47 149.24 1.42 o 5 6 1 0.49 0.31 0.20 o 6 6 1 1.92 1.25 0.16 o 7 6 1 10.64 8.82 0.30 o 8 6 1 33.06 40.29 0.62 o 9 6 1 6.88 6.31 0.24 o 0 7 1 668.28 692.28 6.41 o 1 7 1 152.63 169.06 1.40 o 2 7 1 78.03 81.67 0.95 o 3 7 1 43.30 51.58 0.73 o 4 7 1 118.14 124.03 1.23 o 5 7 1 3.91 3.38 0.31 o 6 7 1 17.94 17.49 0.39 o 7 7 1 7.85 6.87 0.27 o 8 7 1 0.03 0.14 0.13 o 9 7 1 0.13 0.10 0.13 o 1 8 1 254.40 255.32 1.99 o 2 8 1 0.29 0.23 0.12 o 3 8 1 574.93 609.84 4.65 o 4 8 1 210.52 217.50 2.10 o 5 8 1 55.04 61.12 0.64 o 6 8 1 101.09 110.72 1.02 o 7 8 1 0.89 2.36 0.18 o 8 8 1 20.99 25.61 0.41 o 9 8 1 0.01 0.03 0.12 o 0 9 1 288.51 296.94 3.30 o 1 9 1 1009.14 1140.41 7.65 o 2 9 1 0.08 0.60 0.14 o 3 9 1 0.03 0.16 0.15 o 4 9 1 60.69 64.60 1.08 o 5 9 1 21.76 24.06 0.39 o 6 9 1 10.00 9.84 0.50 o 7 9 1 0.65 0.88 0.13 o 8 9 1 10.27 9.74 0.32 o 9 9 1 0.00 0.01 0.14 o 1 10 1 91.05 117.14 1.15 o 2 10 1 1.51 0.16 0.13 o 3 10 1 69.99 88.15 1.18 o 4 10 1 12.02 12.20 0.51 o 5 10 1 5.29 6.49 0.24 o 6 10 1 218.55 221.97 1.74 o 7 10 1 0.09 0.02 0.11 o 8 10 1 29.93 28.59 0.43 o 0 11 1 299.11 262.72 3.17 o 1 11 1 63.70 63.98 0.82 o 2 11 1 5.17 5.65 0.31 o 3 11 1 19.78 11.89 0.45 o 4 11 1 74.02 82.87 0.86 o 5 11 1 12.51 10.51 0.28 o 6 11 1 170.70 172.09 1.70 o 7 11 1 72.72 75.21 0.91 o 8 11 1 0.75 0.77 0.15 o 1 12 1 0.24 0.17 0.16 o 2 12 1 209.16 184.37 1.90 o 3 12 1 18.31 11.01 0.31 o 4 12 1 82.43 95.17 1.04 o 5 12 1 0.01 0.72 0.14 o 6 12 1 59.35 58.80 0.70 o 7 12 1 38.52 45.62 0.56 o 8 12 1 82.20 70.23 2.48 o 0 13 1 2.68 1.65 0.32 o 1 13 1 151.75 109.05 1.40 o 2 13 1 185.68 210.80 2.04 o 3 13 1 0.02 0.32 0.10 o 4 13 1 17.36 22.99 0.42 o 5 13 1 124.98 132.52 1.29 o 6 13 1 48.75 52.69 0.68 o 7 13 1 16.94 16.58 0.52 o 8 13 1 10.41 14.20 0.49 o 1 14 1 112.03 96.41 0.85 o 2 14 1 1.34 0.12 0.10 o 3 14 1 175.86 165.35 1.44 o 4 14 1 0.04 1.31 0.15 o 5 14 1 0.25 0.35 0.14 o 6 14 1 13.79 15.22 0.36 o 7 14 1 53.59 55.91 1.35 o 0 15 1 922.70 800.37 7.88 o 1 15 1 4.15 5.87 0.28 o 2 15 1 160.84 179.27 1.43 o 3 15 1 161.50 137.95 1.21 o 4 15 1 13.64 18.82 0.37 o 5 15 1 80.55 85.24 0.92 o 6 15 1 121.54 120.13 1.99 o 7 15 1 2.94 3.05 0.16 o 1 16 1 8.85 6.31 0.23 o 2 16 1 161.96 145.18 1.18 o 3 16 1 18.54 20.98 0.33 o 4 16 1 36.14 39.97 0.50 o 5 16 1 96.59 97.98 1.01 o 6 16 1 0.00 0.13 0.12 o 7 16 1 15.13 15.85 0.47 o 0 17 1 341.93 329.38 3.78 o 1 17 1 56.79 62.53 0.64 o 2 17 1 18.24 14.22 0.32 o 3 17 1 50.66 45.27 0.51 o 4 17 1 5.84 5.06 0.21 o 5 17 1 1.29 0.65 0.11 o 6 17 1 31.91 30.65 0.56 o 1 18 1 0.12 0.87 0.12 o 2 18 1 0.03 0.05 0.10 o 3 18 1 0.67 0.06 0.10 o 4 18 1 2.81 4.89 0.18 o 5 18 1 0.02 0.20 0.09 o 6 18 1 2.72 2.91 0.16 o 0 19 1 6.17 5.33 0.31 o 1 19 1 31.07 28.86 0.41 o 2 19 1 0.17 0.06 0.11 o 3 19 1 11.81 13.35 0.30 o 4 19 1 2.98 3.00 0.16 o 5 19 1 10.10 8.87 0.21 o 1 20 1 0.11 0.12 0.10 o 2 20 1 13.61 14.65 0.29 o 3 20 1 5.62 5.83 0.22 o 4 20 1 0.48 0.52 0.10 o 0 21 1 7.06 6.34 0.28 o 1 21 1 9.92 9.65 0.30 o 2 21 1 15.10 14.24 0.28 o 3 21 1 0.04 -0.06 0.10 o 1 22 1 10.25 10.97 0.29 o 2 22 1 4.95 4.93 0.22 o 0 0 2 1505.78 1588.20 19.70 o 1 0 2 442.78 435.25 4.43 o 2 0 2 210.01 205.86 2.46 o 3 0 2 3790.98 3979.07 31.30 o 4 0 2 353.81 369.13 4.05 o 5 0 2 464.71 483.17 4.96 o 6 0 2 1020.23 1026.16 8.87 o 7 0 2 0.02 0.76 0.22 o 8 0 2 1.91 3.94 0.30 o 9 0 2 10.42 4.98 0.67 o 1 1 2 351.65 346.70 2.55 o 2 1 2 32.00 36.26 0.48 o 3 1 2 6.06 7.81 0.53 o 4 1 2 1041.72 1078.23 6.38 o 5 1 2 563.51 553.00 3.66 o 6 1 2 2.33 3.38 0.20 o 7 1 2 105.62 119.74 1.27 o 8 1 2 25.31 17.65 0.40 o 9 1 2 25.15 25.10 0.47 o 0 2 2 473.17 488.79 4.28 o 1 2 2 4.07 7.98 0.23 o 2 2 2 173.69 181.79 1.41 o 3 2 2 108.23 125.77 1.11 o 4 2 2 94.08 104.39 0.96 o 5 2 2 138.93 151.41 1.50 o 6 2 2 0.21 0.57 0.15 o 7 2 2 8.12 8.34 0.30 o 8 2 2 56.17 63.81 0.79 o 9 2 2 10.53 13.42 0.35 o 1 3 2 35.64 31.14 0.41 o 2 3 2 173.66 187.85 1.50 o 3 3 2 79.41 88.93 0.90 o 4 3 2 157.06 154.37 1.34 o 5 3 2 48.72 45.69 0.70 o 6 3 2 4.54 6.10 0.25 o 7 3 2 71.19 82.82 0.99 o 8 3 2 52.59 49.33 0.77 o 9 3 2 8.38 9.97 0.27 o 0 4 2 1159.95 1206.70 12.53 o 1 4 2 285.53 300.10 2.12 o 2 4 2 12.92 11.18 0.30 o 3 4 2 480.75 491.88 3.28 o 4 4 2 33.60 32.87 0.58 o 5 4 2 3.24 2.75 0.27 o 6 4 2 108.34 108.74 0.98 o 7 4 2 15.76 14.70 0.42 o 8 4 2 5.00 5.34 0.24 o 9 4 2 66.92 59.04 1.35 o 1 5 2 2.52 2.36 0.15 o 2 5 2 1023.65 1068.94 6.99 o 3 5 2 15.05 15.86 0.47 o 4 5 2 79.52 76.28 0.99 o 5 5 2 0.31 1.03 0.15 o 6 5 2 58.38 62.02 0.62 o 7 5 2 6.79 5.40 0.23 o 8 5 2 4.43 3.84 0.18 o 9 5 2 11.67 9.66 0.44 o 0 6 2 52.26 51.09 0.81 o 1 6 2 214.16 251.52 1.83 o 2 6 2 44.75 47.32 0.66 o 3 6 2 0.26 0.40 0.14 o 4 6 2 53.15 48.49 0.78 o 5 6 2 3.44 3.76 0.18 o 6 6 2 21.61 22.31 0.57 o 7 6 2 30.99 35.25 0.51 o 8 6 2 32.65 40.28 0.50 o 9 6 2 0.04 0.15 0.11 o 1 7 2 42.77 54.15 0.67 o 2 7 2 6.33 7.32 0.29 o 3 7 2 7.57 8.66 0.35 o 4 7 2 3.04 1.92 0.25 o 5 7 2 4.79 7.11 0.22 o 6 7 2 38.50 41.14 0.74 o 7 7 2 17.48 24.87 0.46 o 8 7 2 6.22 6.50 0.25 o 9 7 2 12.03 14.01 1.04 o 0 8 2 1037.57 1128.83 12.05 o 1 8 2 12.07 18.64 0.43 o 2 8 2 677.25 699.56 4.98 o 3 8 2 102.97 106.76 1.16 o 4 8 2 18.77 20.15 0.63 o 5 8 2 8.29 9.72 0.27 o 6 8 2 19.77 15.23 0.35 o 7 8 2 18.03 17.87 0.46 o 8 8 2 0.03 0.10 0.11 o 1 9 2 85.45 82.68 0.95 o 2 9 2 25.64 33.79 0.65 o 3 9 2 0.77 1.33 0.20 o 4 9 2 13.42 15.52 0.31 o 5 9 2 222.05 249.69 1.85 o 6 9 2 4.56 3.79 0.19 o 7 9 2 45.92 51.65 0.61 o 8 9 2 44.28 43.75 0.59 o 0 10 2 119.62 133.06 2.34 o 1 10 2 34.72 27.77 0.60 o 2 10 2 8.31 7.58 0.34 o 3 10 2 427.46 424.23 3.72 o 4 10 2 0.08 0.37 0.11 o 5 10 2 179.83 182.87 1.49 o 6 10 2 3.20 1.92 0.17 o 7 10 2 1.37 1.23 0.15 o 8 10 2 1.20 1.07 0.13 o 1 11 2 3.76 8.01 0.39 o 2 11 2 13.71 11.45 0.49 o 3 11 2 19.00 22.16 0.33 o 4 11 2 306.91 294.05 2.00 o 5 11 2 7.10 5.88 0.24 o 6 11 2 35.86 36.64 0.51 o 7 11 2 75.11 65.78 0.94 o 8 11 2 0.73 1.22 0.12 o 0 12 2 378.70 333.01 4.49 o 1 12 2 51.76 34.93 0.79 o 2 12 2 59.77 64.64 0.61 o 3 12 2 5.74 3.91 0.18 o 4 12 2 84.71 84.28 0.77 o 5 12 2 165.40 160.22 1.43 o 6 12 2 22.95 23.50 0.40 o 7 12 2 30.64 28.55 0.40 o 8 12 2 5.73 6.56 0.49 o 1 13 2 0.18 0.18 0.09 o 2 13 2 268.60 265.03 1.87 o 3 13 2 29.20 34.12 0.43 o 4 13 2 8.14 13.22 0.29 o 5 13 2 15.25 20.75 0.38 o 6 13 2 19.79 16.45 0.31 o 7 13 2 26.48 21.99 0.41 o 0 14 2 652.38 713.22 5.89 o 1 14 2 132.96 128.44 1.11 o 2 14 2 159.05 153.83 1.17 o 3 14 2 5.66 11.96 0.28 o 4 14 2 2.45 2.40 0.15 o 5 14 2 0.69 1.30 0.14 o 6 14 2 14.97 9.53 0.28 o 7 14 2 21.66 23.86 0.58 o 1 15 2 128.51 110.01 0.97 o 2 15 2 2.60 1.38 0.13 o 3 15 2 57.46 59.16 0.59 o 4 15 2 22.52 17.01 0.31 o 5 15 2 1.64 0.91 0.13 o 6 15 2 12.76 14.26 0.32 o 7 15 2 8.29 7.57 0.24 o 0 16 2 23.30 22.72 0.56 o 1 16 2 336.76 293.64 2.12 o 2 16 2 57.38 59.85 0.59 o 3 16 2 1.11 1.17 0.13 o 4 16 2 41.68 43.63 0.46 o 5 16 2 21.17 18.69 0.38 o 6 16 2 0.91 0.63 0.13 o 1 17 2 25.74 24.94 0.38 o 2 17 2 74.32 90.92 0.78 o 3 17 2 29.14 31.39 0.39 o 4 17 2 0.20 0.52 0.11 o 5 17 2 9.52 12.11 0.28 o 6 17 2 33.77 42.44 0.58 o 0 18 2 1.93 -0.03 0.13 o 1 18 2 0.21 -0.09 0.09 o 2 18 2 8.71 8.69 0.24 o 3 18 2 7.97 6.25 0.19 o 4 18 2 6.44 7.47 0.29 o 5 18 2 0.23 0.80 0.13 o 1 19 2 10.35 11.32 0.28 o 2 19 2 22.49 20.22 0.30 o 3 19 2 0.22 0.17 0.08 o 4 19 2 5.71 6.69 0.21 o 0 20 2 35.99 36.98 0.64 o 1 20 2 12.04 14.42 0.30 o 2 20 2 3.57 4.67 0.18 o 3 20 2 0.09 0.10 0.10 o 4 20 2 0.51 0.65 0.16 o 1 21 2 0.19 0.33 0.10 o 2 21 2 13.24 15.24 0.40 o 3 21 2 0.00 0.08 0.12 o 0 22 2 0.12 1.21 0.19 o 1 22 2 1.35 0.29 0.11 o 1 0 3 175.13 176.05 2.07 o 2 0 3 164.32 160.62 2.29 o 3 0 3 16.15 13.63 0.76 o 4 0 3 0.46 0.54 0.25 o 5 0 3 121.04 113.28 1.13 o 6 0 3 516.36 585.95 4.75 o 7 0 3 247.38 212.58 2.16 o 8 0 3 174.30 182.57 2.37 o 9 0 3 73.23 46.93 1.45 o 0 1 3 0.45 0.13 0.20 o 1 1 3 424.09 439.65 3.38 o 2 1 3 66.74 70.71 0.92 o 3 1 3 18.42 20.03 0.51 o 4 1 3 82.90 88.24 1.02 o 5 1 3 348.60 344.70 2.07 o 6 1 3 105.05 108.93 0.87 o 7 1 3 141.62 117.69 1.02 o 8 1 3 69.57 78.91 1.00 o 9 1 3 0.14 0.16 0.18 o 1 2 3 2.04 2.68 0.19 o 2 2 3 35.38 36.96 0.55 o 3 2 3 62.90 60.87 0.82 o 4 2 3 2.16 2.46 0.25 o 5 2 3 87.37 90.80 0.71 o 6 2 3 169.93 196.08 1.33 o 7 2 3 19.09 18.05 0.36 o 8 2 3 78.47 82.78 0.79 o 9 2 3 0.03 -0.12 0.25 o 0 3 3 668.51 667.41 5.92 o 1 3 3 62.64 56.69 0.74 o 2 3 3 10.78 12.05 0.36 o 3 3 3 56.25 54.09 0.76 o 4 3 3 79.97 76.65 1.07 o 5 3 3 145.68 139.85 1.02 o 6 3 3 9.71 12.10 0.27 o 7 3 3 172.26 172.53 1.38 o 8 3 3 0.76 0.59 0.12 o 1 4 3 203.25 198.48 1.68 o 2 4 3 128.60 135.39 1.26 o 3 4 3 8.35 8.98 0.35 o 4 4 3 80.04 73.54 0.92 o 5 4 3 41.71 42.06 0.45 o 6 4 3 42.07 40.41 0.47 o 7 4 3 20.63 15.33 0.37 o 8 4 3 4.07 5.09 0.16 o 0 5 3 386.47 378.99 4.20 o 1 5 3 685.46 681.72 4.73 o 2 5 3 0.03 0.40 0.15 o 3 5 3 70.97 74.28 0.96 o 4 5 3 11.39 13.00 0.28 o 5 5 3 24.66 25.61 0.36 o 6 5 3 44.02 46.16 0.53 o 7 5 3 1.50 1.56 0.15 o 8 5 3 1.23 1.51 0.13 o 1 6 3 0.00 0.28 0.13 o 2 6 3 12.14 13.59 0.49 o 3 6 3 41.81 40.47 0.75 o 4 6 3 89.70 96.18 0.77 o 5 6 3 78.40 89.58 0.79 o 6 6 3 2.78 2.20 0.17 o 7 6 3 0.22 0.61 0.13 o 8 6 3 0.70 0.69 0.12 o 0 7 3 484.48 513.48 7.66 o 1 7 3 31.48 29.24 0.83 o 2 7 3 133.20 144.06 1.53 o 3 7 3 3.44 4.86 0.34 o 4 7 3 71.12 80.85 0.67 o 5 7 3 0.23 0.25 0.11 o 6 7 3 37.70 47.12 0.56 o 7 7 3 14.86 15.98 0.33 o 8 7 3 7.13 5.12 0.22 o 1 8 3 6.59 9.16 0.41 o 2 8 3 2.80 3.03 0.27 o 3 8 3 40.32 32.34 0.37 o 4 8 3 0.25 1.66 0.13 o 5 8 3 22.86 18.35 0.33 o 6 8 3 24.93 30.80 0.42 o 7 8 3 15.89 19.66 0.51 o 8 8 3 4.92 5.79 0.23 o 0 9 3 65.50 56.47 1.64 o 1 9 3 14.22 13.19 0.52 o 2 9 3 245.77 242.35 2.33 o 3 9 3 13.53 15.60 0.26 o 4 9 3 183.02 191.23 1.40 o 5 9 3 37.84 35.57 0.44 o 6 9 3 15.56 16.38 0.33 o 7 9 3 47.18 46.66 0.81 o 8 9 3 3.28 2.71 0.14 o 1 10 3 37.59 39.63 0.50 o 2 10 3 181.59 171.33 1.31 o 3 10 3 47.56 42.21 0.46 o 4 10 3 3.53 3.23 0.17 o 5 10 3 4.30 2.02 0.15 o 6 10 3 4.09 4.35 0.20 o 7 10 3 17.43 17.67 0.40 o 0 11 3 138.02 154.54 1.78 o 1 11 3 272.72 265.58 1.70 o 2 11 3 76.81 59.51 0.58 o 3 11 3 260.61 230.94 1.68 o 4 11 3 135.56 114.81 0.95 o 5 11 3 11.02 13.34 0.28 o 6 11 3 0.78 0.25 0.12 o 7 11 3 0.81 1.97 0.15 o 1 12 3 77.82 68.04 0.63 o 2 12 3 288.90 288.58 1.94 o 3 12 3 0.04 0.27 0.10 o 4 12 3 0.12 -0.01 0.10 o 5 12 3 73.64 59.31 0.61 o 6 12 3 0.10 0.06 0.10 o 7 12 3 5.15 6.86 0.25 o 0 13 3 80.74 100.73 1.26 o 1 13 3 100.10 110.99 0.90 o 2 13 3 20.14 18.93 0.35 o 3 13 3 58.88 53.97 0.61 o 4 13 3 74.03 68.57 0.66 o 5 13 3 5.85 3.79 0.16 o 6 13 3 2.81 5.52 0.17 o 7 13 3 0.07 -0.03 0.11 o 1 14 3 22.54 30.92 0.39 o 2 14 3 82.63 95.11 0.90 o 3 14 3 110.54 118.57 1.06 o 4 14 3 9.70 8.00 0.30 o 5 14 3 37.00 39.01 0.44 o 6 14 3 2.53 1.58 0.12 o 0 15 3 2.00 2.03 0.20 o 1 15 3 63.32 72.33 0.69 o 2 15 3 2.37 1.53 0.14 o 3 15 3 211.33 201.15 1.57 o 4 15 3 16.05 19.71 0.32 o 5 15 3 7.47 10.60 0.23 o 6 15 3 12.09 13.00 0.23 o 1 16 3 60.25 55.24 0.57 o 2 16 3 15.69 16.92 0.31 o 3 16 3 1.09 1.26 0.13 o 4 16 3 125.12 148.45 1.44 o 5 16 3 24.71 22.57 0.37 o 0 17 3 0.07 0.05 0.13 o 1 17 3 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0.09 0.24 0.11 o 8 2 4 3.16 5.57 0.26 o 1 3 4 263.20 236.46 2.57 o 2 3 4 107.37 99.08 0.95 o 3 3 4 101.99 105.78 0.82 o 4 3 4 126.66 126.19 0.94 o 5 3 4 40.92 38.08 0.42 o 6 3 4 34.34 33.74 0.40 o 7 3 4 0.12 -0.10 0.10 o 8 3 4 0.22 0.50 0.11 o 0 4 4 21.47 16.78 1.69 o 1 4 4 2.00 2.12 0.35 o 2 4 4 91.49 80.91 0.67 o 3 4 4 508.95 488.44 2.93 o 4 4 4 49.50 43.44 0.46 o 5 4 4 58.02 63.91 0.58 o 6 4 4 0.71 0.29 0.11 o 7 4 4 5.37 6.58 0.20 o 8 4 4 4.85 2.97 0.38 o 1 5 4 30.30 24.97 0.48 o 2 5 4 11.20 13.55 0.25 o 3 5 4 5.23 5.39 0.19 o 4 5 4 81.65 83.65 0.69 o 5 5 4 22.63 22.17 0.32 o 6 5 4 0.02 0.26 0.10 o 7 5 4 0.09 0.06 0.09 o 0 6 4 75.27 70.73 1.24 o 1 6 4 16.79 18.70 0.30 o 2 6 4 270.03 275.36 1.87 o 3 6 4 0.00 0.27 0.09 o 4 6 4 58.80 66.60 0.62 o 5 6 4 5.04 5.47 0.18 o 6 6 4 44.34 38.41 0.54 o 7 6 4 0.66 0.52 0.10 o 1 7 4 2.00 3.40 0.16 o 2 7 4 33.85 31.43 0.38 o 3 7 4 0.21 0.14 0.08 o 4 7 4 11.37 14.03 0.28 o 5 7 4 24.48 20.94 0.32 o 6 7 4 0.22 0.12 0.11 o 7 7 4 6.74 3.47 0.16 o 0 8 4 51.60 64.44 0.83 o 1 8 4 62.05 67.06 0.62 o 2 8 4 45.13 51.76 0.51 o 3 8 4 37.71 48.91 0.50 o 4 8 4 48.88 54.46 0.53 o 5 8 4 36.97 40.04 0.46 o 6 8 4 35.08 38.70 0.45 o 7 8 4 1.92 2.49 0.23 o 1 9 4 4.82 4.92 0.18 o 2 9 4 10.08 13.88 0.27 o 3 9 4 0.17 0.17 0.09 o 4 9 4 24.07 22.38 0.30 o 5 9 4 0.21 0.39 0.11 o 6 9 4 0.02 -0.07 0.10 o 7 9 4 26.03 25.19 0.41 o 0 10 4 706.96 658.26 5.45 o 1 10 4 58.62 58.11 0.58 o 2 10 4 99.94 81.50 0.70 o 3 10 4 8.57 13.66 0.25 o 4 10 4 17.37 13.53 0.25 o 5 10 4 1.83 1.65 0.13 o 6 10 4 35.00 32.95 0.42 o 7 10 4 0.08 0.27 0.17 o 1 11 4 88.90 75.44 0.67 o 2 11 4 102.25 100.18 0.82 o 3 11 4 56.33 54.99 0.58 o 4 11 4 0.01 0.50 0.10 o 5 11 4 2.92 2.22 0.14 o 6 11 4 3.62 2.21 0.15 o 0 12 4 183.70 172.71 1.69 o 1 12 4 302.45 321.11 2.13 o 2 12 4 23.12 12.39 0.27 o 3 12 4 29.64 20.91 0.34 o 4 12 4 4.04 1.48 0.12 o 5 12 4 3.29 4.64 0.22 o 6 12 4 5.37 4.45 0.16 o 1 13 4 88.67 90.38 0.77 o 2 13 4 8.21 7.99 0.23 o 3 13 4 11.73 10.25 0.26 o 4 13 4 58.66 76.76 0.97 o 5 13 4 74.68 80.39 0.91 o 6 13 4 14.74 17.09 0.67 o 0 14 4 22.30 21.44 0.46 o 1 14 4 0.05 0.14 0.09 o 2 14 4 24.51 31.03 0.40 o 3 14 4 41.20 53.51 0.68 o 4 14 4 6.23 8.53 0.30 o 5 14 4 34.34 35.81 0.59 o 1 15 4 8.11 5.41 0.19 o 2 15 4 5.80 6.88 0.22 o 3 15 4 7.09 7.58 0.25 o 4 15 4 17.11 18.90 0.40 o 5 15 4 0.12 0.27 0.14 o 0 16 4 1.41 1.27 0.17 o 1 16 4 3.64 1.88 0.13 o 2 16 4 0.22 1.51 0.13 o 3 16 4 6.19 6.20 0.20 o 4 16 4 19.65 16.98 0.27 o 1 17 4 0.61 0.52 0.11 o 2 17 4 10.61 13.49 0.30 o 3 17 4 17.93 22.05 0.33 o 0 18 4 39.78 41.21 0.82 o 1 18 4 28.83 39.15 0.47 o 2 18 4 0.69 2.53 0.14 o 1 0 5 76.69 59.00 0.86 o 2 0 5 49.32 58.25 0.80 o 3 0 5 2.71 7.62 0.44 o 4 0 5 9.05 5.13 0.25 o 5 0 5 21.87 16.87 0.45 o 6 0 5 14.67 18.90 0.49 o 7 0 5 41.49 33.09 1.33 o 0 1 5 133.38 128.42 1.62 o 1 1 5 1.56 2.72 0.17 o 2 1 5 13.72 7.21 0.29 o 3 1 5 40.83 30.29 0.38 o 4 1 5 0.51 0.18 0.09 o 5 1 5 34.78 40.65 0.45 o 6 1 5 17.57 22.06 0.29 o 7 1 5 0.28 0.11 0.15 o 1 2 5 21.94 25.36 0.44 o 2 2 5 208.60 211.99 1.64 o 3 2 5 80.08 85.95 0.74 o 4 2 5 33.30 29.66 0.36 o 5 2 5 3.44 1.85 0.12 o 6 2 5 5.90 9.15 0.21 o 0 3 5 26.39 35.21 0.79 o 1 3 5 355.79 357.09 5.11 o 2 3 5 22.45 17.42 0.31 o 3 3 5 0.14 0.05 0.09 o 4 3 5 121.74 109.66 0.85 o 5 3 5 2.17 2.52 0.13 o 6 3 5 14.54 10.88 0.21 o 1 4 5 95.36 87.10 0.95 o 2 4 5 27.23 25.27 0.38 o 3 4 5 5.09 6.01 0.20 o 4 4 5 14.14 17.53 0.28 o 5 4 5 25.08 23.94 0.31 o 6 4 5 3.10 2.71 0.12 o 0 5 5 293.69 299.64 4.13 o 1 5 5 9.81 10.90 0.30 o 2 5 5 60.94 56.56 0.57 o 3 5 5 9.39 7.09 0.22 o 4 5 5 23.65 24.20 0.34 o 5 5 5 43.04 37.46 0.41 o 6 5 5 31.20 33.25 0.36 o 1 6 5 0.84 1.55 0.16 o 2 6 5 58.14 66.63 0.64 o 3 6 5 53.94 48.52 0.53 o 4 6 5 22.61 21.06 0.31 o 5 6 5 19.61 13.96 0.23 o 6 6 5 0.45 3.37 0.13 o 0 7 5 99.64 122.21 1.94 o 1 7 5 44.49 59.29 0.72 o 2 7 5 0.18 1.15 0.12 o 3 7 5 25.95 30.29 0.37 o 4 7 5 2.31 0.79 0.11 o 5 7 5 7.92 14.63 0.28 o 6 7 5 11.40 13.46 0.22 o 1 8 5 0.63 0.22 0.13 o 2 8 5 2.85 2.12 0.13 o 3 8 5 0.58 0.76 0.11 o 4 8 5 6.46 5.35 0.21 o 5 8 5 2.37 2.13 0.12 o 6 8 5 4.71 1.88 0.12 o 0 9 5 8.87 8.55 0.41 o 1 9 5 18.26 19.56 0.34 o 2 9 5 78.96 77.66 0.69 o 3 9 5 25.96 27.09 0.36 o 4 9 5 23.23 24.22 0.31 o 5 9 5 7.06 7.57 0.28 o 1 10 5 14.66 13.74 0.33 o 2 10 5 1.66 2.19 0.14 o 3 10 5 28.99 29.56 0.36 o 4 10 5 47.21 48.12 0.50 o 5 10 5 8.63 10.25 0.24 o 0 11 5 188.71 173.18 2.00 o 1 11 5 38.16 24.46 0.33 o 2 11 5 197.46 199.41 1.53 o 3 11 5 45.10 54.51 0.52 o 4 11 5 12.64 11.45 0.27 o 5 11 5 18.28 26.34 0.50 o 1 12 5 83.11 83.20 0.72 o 2 12 5 17.00 12.92 0.27 o 3 12 5 18.56 19.50 0.29 o 4 12 5 2.92 3.50 0.17 o 0 13 5 29.36 19.40 0.46 o 1 13 5 0.01 0.32 0.09 o 2 13 5 1.54 1.29 0.12 o 3 13 5 82.73 94.76 0.87 o 4 13 5 14.31 18.19 0.44 o 1 14 5 0.73 1.80 0.13 o 2 14 5 0.31 0.61 0.10 o 3 14 5 0.03 0.03 0.09 o 0 15 5 4.01 3.71 0.30 o 1 15 5 0.52 0.15 0.11 o 2 15 5 11.87 12.39 0.39 o 1 16 5 7.87 6.80 0.41 o 0 0 6 3.42 0.03 0.30 o 1 0 6 69.65 53.81 0.89 o 2 0 6 16.32 17.90 0.49 o 3 0 6 16.49 16.15 0.53 o 4 0 6 33.00 34.30 0.58 o 5 0 6 35.84 34.98 0.58 o 1 1 6 47.27 42.49 0.56 o 2 1 6 7.22 14.29 0.40 o 3 1 6 3.27 2.07 0.13 o 4 1 6 5.24 10.87 0.23 o 5 1 6 4.98 2.93 0.13 o 0 2 6 232.56 258.57 4.04 o 1 2 6 109.74 110.98 1.41 o 2 2 6 14.91 13.25 0.29 o 3 2 6 9.28 13.56 0.27 o 4 2 6 20.04 23.69 0.34 o 5 2 6 1.55 4.90 0.17 o 1 3 6 0.01 0.21 0.15 o 2 3 6 91.26 94.29 1.02 o 3 3 6 24.97 21.86 0.32 o 4 3 6 0.12 0.68 0.10 o 5 3 6 13.49 11.79 0.35 o 0 4 6 225.98 212.76 2.97 o 1 4 6 4.37 9.47 0.34 o 2 4 6 85.28 82.78 1.05 o 3 4 6 48.61 52.18 0.67 o 4 4 6 5.38 4.23 0.15 o 1 5 6 38.00 32.64 0.53 o 2 5 6 22.27 24.08 0.44 o 3 5 6 4.79 5.29 0.21 o 4 5 6 0.02 0.57 0.09 o 0 6 6 46.56 51.59 1.05 o 1 6 6 28.31 36.15 0.54 o 2 6 6 11.94 17.26 0.40 o 3 6 6 0.19 1.20 0.13 o 4 6 6 15.40 14.83 0.31 o 1 7 6 6.87 6.44 0.23 o 2 7 6 38.61 38.67 0.61 o 3 7 6 2.23 3.16 0.17 o 4 7 6 1.19 5.40 0.27 o 0 8 6 0.13 -0.15 0.15 o 1 8 6 14.96 22.79 0.39 o 2 8 6 0.06 -0.06 0.12 o 3 8 6 11.14 19.07 0.41 o 1 9 6 0.68 0.80 0.13 o 2 9 6 1.98 2.46 0.17 o 3 9 6 4.90 5.92 0.19 o 0 10 6 33.41 36.74 0.71 o 1 10 6 25.14 19.59 0.34 o 2 10 6 0.58 0.65 0.13 o 1 11 6 0.10 0.11 0.10 o 2 11 6 27.26 24.36 0.53 o 0 12 6 0.12 -0.15 0.30 o