#------------------------------------------------------------------------------ #$Date: 2023-01-04 15:33:41 +0200 (Wed, 04 Jan 2023) $ #$Revision: 280097 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519441 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.8867 _cell_length_b 18.8866 _cell_length_c 5.8042 _exptl_crystal_F_000 370.88 _reflns_d_resolution_high 0.8211 _cod_data_source_file 05-59DBT_41DBF.fcf _cod_data_source_block jw22472 _shelx_title ' jw22472_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 100.75 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10150.65 10474.35 332.09 o 4 0 0 24.68 25.71 2.68 o 6 0 0 275.92 262.00 11.13 o 8 0 0 10.66 11.82 1.26 o 2 1 0 7034.58 7206.67 186.63 o 4 1 0 284.83 303.45 10.59 o 6 1 0 145.60 144.58 5.75 o 8 1 0 0.20 -0.34 0.34 o 0 2 0 5862.59 5742.22 257.51 o 2 2 0 1480.84 1611.25 38.75 o 4 2 0 150.96 152.17 5.84 o 6 2 0 9.66 9.86 0.72 o 8 2 0 0.34 0.76 0.43 o 2 3 0 2772.80 2871.66 74.62 o 4 3 0 211.19 213.88 6.22 o 6 3 0 392.82 345.01 10.16 o 8 3 0 216.08 207.51 6.27 o 0 4 0 611.93 509.55 23.17 o 2 4 0 477.46 497.98 12.24 o 4 4 0 1.72 2.54 0.58 o 6 4 0 548.66 504.28 14.68 o 8 4 0 21.16 22.29 1.13 o 2 5 0 20.47 22.18 0.98 o 4 5 0 1.60 3.60 0.65 o 6 5 0 479.14 421.89 12.35 o 8 5 0 317.06 302.40 8.87 o 0 6 0 2977.19 3220.43 144.82 o 2 6 0 1604.40 1608.53 41.98 o 4 6 0 3.92 5.07 0.78 o 6 6 0 83.92 74.02 2.51 o 8 6 0 7.51 7.11 0.63 o 2 7 0 826.65 879.51 23.18 o 4 7 0 582.41 506.96 23.67 o 6 7 0 479.67 425.40 13.93 o 8 7 0 61.63 61.71 2.38 o 0 8 0 343.28 364.44 17.06 o 2 8 0 343.84 365.84 9.19 o 4 8 0 398.45 350.53 9.94 o 6 8 0 48.33 44.07 1.98 o 8 8 0 0.53 1.08 0.61 o 2 9 0 2177.16 2320.35 56.03 o 4 9 0 727.19 670.22 18.10 o 6 9 0 189.69 173.25 10.29 o 8 9 0 105.39 111.44 3.90 o 0 10 0 43.08 67.52 4.04 o 2 10 0 1.66 4.58 0.83 o 4 10 0 28.66 29.05 1.65 o 6 10 0 35.06 35.35 2.26 o 8 10 0 151.34 161.92 5.47 o 2 11 0 14.12 16.98 2.68 o 4 11 0 506.05 434.93 9.77 o 6 11 0 60.33 58.03 3.77 o 8 11 0 20.51 19.65 0.99 o 0 12 0 944.08 1020.85 46.82 o 2 12 0 1.26 4.62 1.34 o 4 12 0 1.66 1.73 0.48 o 6 12 0 67.24 70.07 2.41 o 8 12 0 148.11 148.21 4.93 o 2 13 0 85.66 75.66 8.90 o 4 13 0 787.67 678.29 21.91 o 6 13 0 12.11 11.29 0.82 o 0 14 0 304.38 317.55 21.63 o 2 14 0 319.93 273.75 9.13 o 4 14 0 593.69 550.02 17.85 o 6 14 0 229.08 231.17 8.90 o 2 15 0 414.96 382.36 12.50 o 4 15 0 20.05 18.18 1.27 o 6 15 0 4.66 5.33 0.75 o 0 16 0 194.09 179.83 8.81 o 2 16 0 866.63 765.34 24.74 o 4 16 0 454.44 431.45 14.20 o 6 16 0 20.21 21.68 1.11 o 2 17 0 134.94 118.49 4.29 o 4 17 0 5.12 6.20 0.75 o 6 17 0 7.26 6.60 0.57 o 0 18 0 23.99 33.19 2.52 o 2 18 0 82.22 79.38 3.03 o 4 18 0 21.55 17.93 1.47 o 2 19 0 73.94 73.17 3.81 o 4 19 0 181.10 189.69 6.47 o 0 20 0 65.95 72.78 5.75 o 2 20 0 15.47 22.76 1.27 o 4 20 0 1.15 1.55 0.40 o 2 21 0 0.92 -0.02 0.47 o 0 22 0 220.18 293.25 19.29 o 2 22 0 98.08 114.26 4.49 o 1 0 1 3617.02 3338.94 94.81 o 2 0 1 6343.30 6174.51 175.18 o 3 0 1 4848.71 5039.58 130.94 o 4 0 1 328.75 349.14 9.71 o 5 0 1 281.67 260.49 11.47 o 6 0 1 0.55 0.28 0.39 o 7 0 1 19.08 15.16 0.82 o 8 0 1 47.24 51.79 1.74 o 9 0 1 9.09 7.99 0.71 o 0 1 1 335.29 447.39 14.49 o 1 1 1 4746.00 4408.97 93.31 o 2 1 1 8624.15 8671.03 173.95 o 3 1 1 3.79 4.31 0.34 o 4 1 1 2469.47 2571.28 47.53 o 5 1 1 55.23 55.14 1.94 o 6 1 1 1.98 1.52 0.30 o 7 1 1 11.93 11.70 0.55 o 8 1 1 0.13 -0.25 0.29 o 9 1 1 28.98 31.85 1.02 o 1 2 1 31.56 36.09 1.24 o 2 2 1 659.59 720.55 12.86 o 3 2 1 103.31 117.66 2.39 o 4 2 1 293.77 286.48 6.27 o 5 2 1 8.08 7.24 0.74 o 6 2 1 95.22 87.84 2.06 o 7 2 1 1.60 1.25 0.30 o 8 2 1 5.46 6.60 0.42 o 9 2 1 16.39 19.11 0.73 o 0 3 1 1849.81 1909.41 60.87 o 1 3 1 1198.26 1228.89 26.18 o 2 3 1 26.47 20.72 0.72 o 3 3 1 121.51 131.18 3.23 o 4 3 1 16.00 16.86 0.90 o 5 3 1 21.65 25.78 1.34 o 6 3 1 38.96 37.13 1.25 o 7 3 1 5.78 7.04 0.46 o 8 3 1 68.71 71.88 1.73 o 9 3 1 37.31 38.96 1.22 o 1 4 1 16.28 15.87 0.66 o 2 4 1 20.59 17.74 0.69 o 3 4 1 124.85 141.86 3.70 o 4 4 1 1459.05 1438.11 31.05 o 5 4 1 25.07 23.37 1.47 o 6 4 1 241.17 229.26 5.15 o 7 4 1 12.63 12.24 0.61 o 8 4 1 2.89 2.66 0.41 o 9 4 1 0.77 0.40 0.30 o 0 5 1 969.90 994.17 32.04 o 1 5 1 64.00 55.59 1.68 o 2 5 1 3.99 3.98 0.37 o 3 5 1 209.93 228.53 5.69 o 4 5 1 1.50 1.52 0.50 o 5 5 1 302.35 301.75 8.58 o 6 5 1 4.39 4.16 0.51 o 7 5 1 35.55 34.80 1.16 o 8 5 1 124.80 124.14 3.07 o 9 5 1 2.25 1.86 0.32 o 1 6 1 340.28 340.25 8.06 o 2 6 1 363.63 388.66 8.26 o 3 6 1 309.00 327.60 7.92 o 4 6 1 660.72 612.86 16.64 o 5 6 1 21.12 18.34 1.31 o 6 6 1 113.04 105.64 2.70 o 7 6 1 0.65 0.89 0.33 o 8 6 1 63.40 62.85 1.72 o 9 6 1 2.44 2.84 0.33 o 0 7 1 1917.37 2060.35 66.05 o 1 7 1 351.37 396.60 9.98 o 2 7 1 498.87 506.82 10.56 o 3 7 1 135.56 146.71 4.24 o 4 7 1 245.71 225.84 5.21 o 5 7 1 2.20 1.90 0.84 o 6 7 1 9.84 9.97 0.60 o 7 7 1 14.43 14.99 1.01 o 8 7 1 17.55 18.37 0.77 o 9 7 1 3.57 3.94 0.38 o 1 8 1 132.53 130.95 3.50 o 2 8 1 20.22 23.78 1.10 o 3 8 1 364.28 375.52 9.83 o 4 8 1 637.38 583.10 16.12 o 5 8 1 11.69 10.71 0.53 o 6 8 1 279.45 255.77 6.04 o 7 8 1 7.63 6.77 0.51 o 8 8 1 65.48 64.83 1.73 o 0 9 1 1073.16 1163.53 37.77 o 1 9 1 1326.45 1430.34 34.84 o 2 9 1 63.82 71.22 2.76 o 3 9 1 33.40 30.28 1.27 o 4 9 1 16.40 14.34 1.15 o 5 9 1 15.34 14.96 0.65 o 6 9 1 0.14 0.32 0.29 o 7 9 1 0.90 1.34 0.35 o 8 9 1 2.68 3.77 0.42 o 1 10 1 43.40 56.86 2.00 o 2 10 1 46.37 45.35 1.98 o 3 10 1 15.17 20.55 1.19 o 4 10 1 226.48 181.23 5.66 o 5 10 1 24.01 21.57 0.92 o 6 10 1 390.49 374.97 8.21 o 7 10 1 4.80 4.41 0.47 o 8 10 1 93.75 98.67 3.00 o 0 11 1 5.55 5.50 0.96 o 1 11 1 151.32 173.75 4.87 o 2 11 1 143.82 146.60 5.27 o 3 11 1 49.20 43.36 1.88 o 4 11 1 4.13 4.31 0.40 o 5 11 1 16.86 15.34 0.72 o 6 11 1 198.06 188.67 4.56 o 7 11 1 31.74 30.20 1.31 o 8 11 1 13.65 14.22 0.76 o 1 12 1 0.45 0.33 0.62 o 2 12 1 425.59 403.35 13.92 o 3 12 1 0.18 0.59 0.53 o 4 12 1 2.29 3.23 0.38 o 5 12 1 18.99 14.18 0.69 o 6 12 1 115.76 109.07 2.95 o 7 12 1 72.95 71.95 2.17 o 8 12 1 148.07 162.23 5.39 o 0 13 1 141.60 151.97 6.74 o 1 13 1 179.55 169.24 5.83 o 2 13 1 694.30 630.36 21.27 o 3 13 1 0.33 0.70 0.35 o 4 13 1 128.27 122.64 2.75 o 5 13 1 120.63 115.04 2.74 o 6 13 1 87.00 85.94 2.39 o 7 13 1 30.72 32.34 1.16 o 1 14 1 56.32 50.29 1.88 o 2 14 1 16.72 17.90 0.82 o 3 14 1 65.57 58.34 1.84 o 4 14 1 8.83 6.80 0.53 o 5 14 1 15.64 16.63 0.74 o 6 14 1 50.61 47.73 1.59 o 7 14 1 113.22 112.18 3.13 o 0 15 1 1518.88 1317.95 48.87 o 1 15 1 16.07 19.17 0.86 o 2 15 1 455.11 414.85 10.29 o 3 15 1 82.57 76.23 2.15 o 4 15 1 39.09 34.89 1.39 o 5 15 1 69.86 70.74 1.93 o 6 15 1 53.21 52.59 1.56 o 7 15 1 6.23 6.60 0.75 o 1 16 1 1.17 0.07 0.46 o 2 16 1 73.83 57.35 1.73 o 3 16 1 40.54 38.29 1.39 o 4 16 1 151.10 147.36 3.64 o 5 16 1 124.78 129.52 3.44 o 6 16 1 44.72 46.16 1.50 o 0 17 1 675.74 588.29 19.16 o 1 17 1 1.25 1.77 0.49 o 2 17 1 71.58 66.12 1.87 o 3 17 1 8.70 7.17 0.59 o 4 17 1 1.90 1.72 0.37 o 5 17 1 0.01 0.15 0.36 o 6 17 1 18.37 17.82 0.71 o 1 18 1 0.03 0.07 0.46 o 2 18 1 9.33 10.42 0.61 o 3 18 1 0.05 0.22 0.33 o 4 18 1 87.97 93.96 2.56 o 5 18 1 3.72 2.64 0.35 o 0 19 1 29.85 31.96 1.96 o 1 19 1 86.51 80.12 2.49 o 2 19 1 31.15 28.75 1.34 o 3 19 1 26.96 29.08 0.99 o 4 19 1 10.06 11.55 0.59 o 5 19 1 4.92 5.89 0.39 o 1 20 1 0.22 0.62 0.41 o 2 20 1 49.10 48.38 1.74 o 3 20 1 0.21 0.17 0.29 o 4 20 1 29.24 33.88 1.04 o 0 21 1 59.63 78.03 6.45 o 1 21 1 0.06 -0.19 0.31 o 2 21 1 54.09 60.82 2.05 o 3 21 1 3.35 3.51 0.35 o 1 22 1 9.45 9.91 0.66 o 2 22 1 17.92 19.89 0.98 o 0 0 2 2713.76 2925.61 132.34 o 1 0 2 22.61 24.70 1.56 o 2 0 2 13.10 10.29 0.78 o 3 0 2 1827.80 1903.81 54.90 o 4 0 2 250.69 255.44 8.47 o 5 0 2 513.65 518.95 14.61 o 6 0 2 852.76 826.23 30.68 o 7 0 2 12.98 17.99 1.27 o 8 0 2 16.01 20.10 1.25 o 9 0 2 9.69 13.73 0.98 o 1 1 2 99.05 110.26 2.83 o 2 1 2 57.61 61.44 1.82 o 3 1 2 22.41 23.61 1.26 o 4 1 2 1582.40 1563.95 30.41 o 5 1 2 843.35 810.38 24.83 o 6 1 2 53.36 55.62 1.78 o 7 1 2 361.43 367.09 9.23 o 8 1 2 21.01 20.13 0.92 o 9 1 2 77.32 81.20 2.36 o 0 2 2 1199.63 1251.69 36.10 o 1 2 2 302.75 341.13 7.27 o 2 2 2 591.85 601.17 12.51 o 3 2 2 0.35 0.53 0.26 o 4 2 2 111.33 124.76 3.63 o 5 2 2 94.93 95.48 4.01 o 6 2 2 1.49 2.50 0.42 o 7 2 2 30.05 30.22 1.16 o 8 2 2 90.56 104.18 2.67 o 9 2 2 0.25 0.90 0.34 o 1 3 2 43.83 49.11 1.51 o 2 3 2 427.47 472.06 10.50 o 3 3 2 0.27 1.51 0.39 o 4 3 2 8.19 9.04 0.83 o 5 3 2 1.86 1.11 0.71 o 6 3 2 22.27 21.70 0.95 o 7 3 2 128.36 146.05 3.93 o 8 3 2 91.05 108.42 2.78 o 9 3 2 28.68 27.54 0.91 o 0 4 2 511.74 564.87 18.68 o 1 4 2 1232.75 1367.17 29.42 o 2 4 2 258.11 250.75 5.87 o 3 4 2 773.62 788.88 18.47 o 4 4 2 147.42 156.71 7.06 o 5 4 2 15.85 16.56 1.45 o 6 4 2 129.89 126.60 3.23 o 7 4 2 0.15 -0.21 0.36 o 8 4 2 27.62 30.53 1.09 o 9 4 2 9.58 9.26 0.71 o 1 5 2 1.85 1.13 0.61 o 2 5 2 1529.42 1632.77 35.15 o 3 5 2 2.46 1.40 0.61 o 4 5 2 286.18 276.98 10.44 o 5 5 2 48.69 43.36 1.57 o 6 5 2 140.05 142.70 3.60 o 7 5 2 42.56 45.76 1.59 o 8 5 2 22.94 24.67 0.93 o 0 6 2 59.04 59.14 2.73 o 1 6 2 899.97 1044.21 24.08 o 2 6 2 341.90 341.67 7.88 o 3 6 2 36.43 43.47 1.91 o 4 6 2 155.23 143.59 5.37 o 5 6 2 6.02 6.51 0.56 o 6 6 2 7.21 7.85 0.58 o 7 6 2 3.63 5.11 0.53 o 8 6 2 4.74 3.94 0.42 o 1 7 2 25.53 27.04 1.42 o 2 7 2 60.39 61.34 2.10 o 3 7 2 30.87 29.17 2.52 o 4 7 2 32.33 26.25 1.43 o 5 7 2 46.27 43.96 1.30 o 6 7 2 124.88 115.79 3.21 o 7 7 2 1.75 1.56 0.41 o 8 7 2 24.47 26.53 0.99 o 0 8 2 1507.98 1849.50 59.79 o 1 8 2 228.10 261.49 6.63 o 2 8 2 1183.73 1199.96 29.75 o 3 8 2 215.21 205.27 6.52 o 4 8 2 54.91 47.34 2.15 o 5 8 2 38.41 32.98 1.23 o 6 8 2 45.67 43.80 1.67 o 7 8 2 18.55 18.09 1.02 o 8 8 2 6.85 7.62 0.55 o 1 9 2 106.60 119.79 3.73 o 2 9 2 11.99 7.73 0.86 o 3 9 2 81.68 85.49 5.83 o 4 9 2 5.15 4.96 0.48 o 5 9 2 26.87 23.38 0.97 o 6 9 2 60.18 55.06 1.74 o 7 9 2 7.61 6.73 0.61 o 8 9 2 66.06 70.19 2.09 o 0 10 2 212.81 299.90 10.85 o 1 10 2 263.50 283.56 7.29 o 2 10 2 38.76 38.88 2.27 o 3 10 2 642.56 614.03 21.08 o 4 10 2 5.13 5.71 0.45 o 5 10 2 199.49 185.12 4.49 o 6 10 2 0.64 0.89 0.34 o 7 10 2 0.14 -0.38 0.38 o 8 10 2 11.05 10.37 0.57 o 1 11 2 31.92 34.37 1.85 o 2 11 2 4.18 3.61 1.08 o 3 11 2 112.85 96.63 2.52 o 4 11 2 496.71 471.09 11.62 o 5 11 2 22.53 19.68 1.11 o 6 11 2 131.15 131.02 3.50 o 7 11 2 7.04 7.19 0.61 o 0 12 2 823.96 900.47 31.99 o 1 12 2 128.90 138.58 4.42 o 2 12 2 0.31 0.82 0.39 o 3 12 2 43.24 40.71 1.21 o 4 12 2 58.80 57.63 1.53 o 5 12 2 127.74 120.45 2.88 o 6 12 2 17.15 15.32 0.75 o 7 12 2 16.40 17.26 0.87 o 1 13 2 14.13 14.17 0.71 o 2 13 2 188.49 194.74 4.74 o 3 13 2 196.02 190.52 4.15 o 4 13 2 95.41 89.54 2.15 o 5 13 2 153.51 157.61 3.47 o 6 13 2 82.39 85.76 2.36 o 7 13 2 1.63 1.73 0.42 o 0 14 2 1048.55 1051.25 33.84 o 1 14 2 62.97 62.21 1.84 o 2 14 2 280.38 277.46 7.03 o 3 14 2 0.96 2.06 0.46 o 4 14 2 0.07 0.17 0.33 o 5 14 2 0.36 0.57 0.33 o 6 14 2 11.28 11.68 0.66 o 7 14 2 18.13 17.81 1.57 o 1 15 2 145.86 143.59 3.58 o 2 15 2 34.79 27.81 1.15 o 3 15 2 206.00 217.42 4.97 o 4 15 2 2.37 2.63 0.44 o 5 15 2 41.78 42.26 1.22 o 6 15 2 33.94 34.26 1.11 o 0 16 2 1.39 2.10 0.82 o 1 16 2 82.87 76.86 2.50 o 2 16 2 132.70 126.51 3.46 o 3 16 2 13.07 12.46 0.71 o 4 16 2 78.76 78.31 2.07 o 5 16 2 1.38 1.13 0.30 o 6 16 2 8.74 10.03 0.48 o 1 17 2 41.20 36.39 2.24 o 2 17 2 174.15 181.71 4.75 o 3 17 2 79.28 80.43 2.18 o 4 17 2 19.07 19.29 0.78 o 5 17 2 32.16 34.33 1.05 o 0 18 2 36.97 32.12 2.26 o 1 18 2 45.31 49.67 2.47 o 2 18 2 56.37 56.68 2.00 o 3 18 2 13.65 11.90 0.66 o 4 18 2 0.08 0.38 0.28 o 5 18 2 8.11 8.84 0.49 o 1 19 2 0.93 1.39 0.53 o 2 19 2 2.82 2.93 0.39 o 3 19 2 9.84 9.20 0.54 o 4 19 2 2.64 2.37 0.30 o 0 20 2 112.30 110.18 7.78 o 1 20 2 62.33 61.14 2.27 o 2 20 2 31.82 34.55 1.46 o 3 20 2 9.58 9.66 0.50 o 1 21 2 1.28 1.63 0.52 o 2 21 2 27.04 32.90 1.30 o 0 22 2 3.85 3.09 0.75 o 1 0 3 171.72 187.24 8.64 o 2 0 3 296.11 277.41 11.99 o 3 0 3 94.83 102.81 10.97 o 4 0 3 0.61 -1.81 3.84 o 5 0 3 21.56 24.85 2.07 o 6 0 3 431.20 431.28 16.42 o 7 0 3 387.09 424.79 16.16 o 8 0 3 297.55 342.82 13.02 o 0 1 3 8.52 11.97 1.21 o 1 1 3 5.11 9.41 0.75 o 2 1 3 168.36 154.60 4.35 o 3 1 3 14.47 17.22 1.54 o 4 1 3 32.83 24.50 4.88 o 5 1 3 128.50 128.18 4.67 o 6 1 3 251.40 260.22 7.20 o 7 1 3 137.93 137.17 3.97 o 8 1 3 12.55 11.56 0.87 o 1 2 3 50.35 50.53 1.82 o 2 2 3 8.06 9.31 0.73 o 3 2 3 365.99 338.85 19.51 o 4 2 3 8.19 9.40 1.19 o 5 2 3 375.61 382.70 12.62 o 6 2 3 184.74 207.52 5.85 o 7 2 3 94.77 98.57 3.00 o 8 2 3 95.13 110.87 3.17 o 0 3 3 1177.04 1292.94 42.09 o 1 3 3 471.44 494.69 11.21 o 2 3 3 55.46 55.60 1.85 o 3 3 3 25.44 23.97 1.59 o 4 3 3 56.90 53.39 7.89 o 5 3 3 146.95 151.30 4.89 o 6 3 3 14.22 12.05 0.71 o 7 3 3 84.80 92.75 2.57 o 8 3 3 8.85 8.49 0.54 o 1 4 3 48.77 63.37 2.60 o 2 4 3 153.77 155.69 4.08 o 3 4 3 30.91 23.40 1.75 o 4 4 3 141.68 110.92 13.01 o 5 4 3 194.32 195.09 5.58 o 6 4 3 64.98 73.82 2.50 o 7 4 3 7.42 8.15 0.55 o 8 4 3 1.47 2.32 0.35 o 0 5 3 963.04 1002.40 33.03 o 1 5 3 1499.19 1592.62 36.59 o 2 5 3 56.90 58.76 2.30 o 3 5 3 322.62 285.48 10.10 o 4 5 3 6.93 7.17 0.91 o 5 5 3 17.71 18.42 1.05 o 6 5 3 15.17 15.74 0.99 o 7 5 3 15.37 17.98 0.86 o 8 5 3 9.66 9.95 0.52 o 1 6 3 32.43 31.70 1.40 o 2 6 3 6.80 10.01 0.90 o 3 6 3 13.64 11.29 1.17 o 4 6 3 115.91 96.54 2.71 o 5 6 3 1.57 2.53 0.46 o 6 6 3 15.44 17.10 1.23 o 7 6 3 37.86 39.72 1.43 o 8 6 3 0.41 0.84 0.35 o 0 7 3 691.27 734.86 24.68 o 1 7 3 45.93 52.42 1.97 o 2 7 3 241.43 236.79 6.72 o 3 7 3 136.90 123.27 5.09 o 4 7 3 75.00 65.77 2.02 o 5 7 3 0.90 1.31 0.37 o 6 7 3 22.39 19.81 1.07 o 7 7 3 36.18 34.31 1.52 o 8 7 3 15.13 13.13 0.72 o 1 8 3 60.66 70.35 2.46 o 2 8 3 13.34 12.16 1.06 o 3 8 3 199.96 195.73 4.08 o 4 8 3 33.93 28.64 1.31 o 5 8 3 148.56 145.79 3.65 o 6 8 3 4.65 3.17 0.47 o 7 8 3 7.60 6.87 0.59 o 8 8 3 9.91 9.07 0.71 o 0 9 3 201.07 194.84 7.65 o 1 9 3 306.64 312.64 8.09 o 2 9 3 226.02 236.26 6.90 o 3 9 3 35.77 27.75 1.20 o 4 9 3 149.06 143.19 3.40 o 5 9 3 43.11 39.35 1.35 o 6 9 3 18.61 18.58 1.24 o 7 9 3 12.80 12.84 0.88 o 1 10 3 14.07 13.02 1.11 o 2 10 3 158.66 153.90 3.62 o 3 10 3 0.42 1.61 0.83 o 4 10 3 17.88 16.24 0.74 o 5 10 3 36.69 35.62 1.32 o 6 10 3 0.12 -0.07 0.32 o 7 10 3 3.65 3.29 0.49 o 0 11 3 49.81 46.43 2.19 o 1 11 3 765.78 718.65 15.50 o 2 11 3 87.87 87.81 2.40 o 3 11 3 384.45 358.64 7.96 o 4 11 3 124.15 115.84 2.83 o 5 11 3 18.02 18.89 0.89 o 6 11 3 0.85 0.50 0.34 o 7 11 3 3.22 3.40 0.50 o 1 12 3 91.90 87.81 2.26 o 2 12 3 439.78 421.17 9.87 o 3 12 3 55.37 61.73 1.77 o 4 12 3 11.84 10.46 0.63 o 5 12 3 1.33 2.08 0.39 o 6 12 3 2.16 2.85 0.39 o 7 12 3 42.72 39.66 3.41 o 0 13 3 131.28 136.78 5.04 o 1 13 3 2.19 4.02 0.49 o 2 13 3 24.17 21.79 1.00 o 3 13 3 114.54 118.79 3.08 o 4 13 3 88.44 81.39 2.22 o 5 13 3 6.43 9.43 0.56 o 6 13 3 10.93 14.07 0.69 o 1 14 3 61.20 61.94 1.84 o 2 14 3 183.57 200.80 4.90 o 3 14 3 250.95 273.37 6.50 o 4 14 3 52.10 57.57 1.68 o 5 14 3 164.26 177.52 4.27 o 6 14 3 2.97 3.75 0.36 o 0 15 3 0.19 0.51 0.76 o 1 15 3 2.19 2.88 0.44 o 2 15 3 1.07 2.38 0.44 o 3 15 3 50.12 53.04 1.60 o 4 15 3 7.37 8.86 0.53 o 5 15 3 8.70 10.22 0.60 o 6 15 3 6.55 7.56 0.54 o 1 16 3 21.83 21.85 1.45 o 2 16 3 13.75 14.54 0.80 o 3 16 3 7.89 8.44 0.54 o 4 16 3 178.48 204.47 4.86 o 5 16 3 97.89 100.30 2.59 o 0 17 3 24.49 27.23 4.16 o 1 17 3 123.81 127.42 4.09 o 2 17 3 8.51 12.20 0.65 o 3 17 3 5.26 7.92 0.49 o 4 17 3 0.11 0.93 0.31 o 5 17 3 0.02 0.32 0.30 o 1 18 3 18.78 22.51 1.66 o 2 18 3 4.95 5.46 0.50 o 3 18 3 48.63 54.22 1.94 o 4 18 3 63.51 74.80 2.32 o 0 19 3 14.89 13.11 1.49 o 1 19 3 11.21 10.22 0.66 o 2 19 3 5.49 4.70 0.40 o 3 19 3 80.60 87.14 2.50 o 1 20 3 16.68 15.99 1.60 o 2 20 3 5.16 4.03 0.49 o 0 0 4 18.78 13.77 2.20 o 1 0 4 80.64 87.54 5.71 o 2 0 4 154.32 160.71 14.34 o 3 0 4 10.74 10.42 1.20 o 4 0 4 138.26 142.69 10.76 o 5 0 4 35.83 44.55 4.90 o 6 0 4 6.46 6.75 1.17 o 7 0 4 9.37 9.79 1.04 o 1 1 4 14.63 15.37 1.73 o 2 1 4 0.72 1.80 0.64 o 3 1 4 323.38 269.03 6.72 o 4 1 4 225.83 215.63 10.81 o 5 1 4 204.30 208.42 8.44 o 6 1 4 27.80 32.26 2.22 o 7 1 4 0.50 1.07 0.52 o 0 2 4 73.49 80.62 5.84 o 1 2 4 30.41 30.50 1.88 o 2 2 4 66.89 71.03 3.16 o 3 2 4 189.17 167.40 4.73 o 4 2 4 1.62 1.54 0.57 o 5 2 4 92.84 95.87 4.28 o 6 2 4 13.60 16.11 1.37 o 7 2 4 5.51 6.31 0.83 o 1 3 4 280.99 294.48 8.81 o 2 3 4 168.24 169.70 6.22 o 3 3 4 342.41 306.75 8.35 o 4 3 4 75.36 64.10 2.05 o 5 3 4 14.59 14.34 1.34 o 6 3 4 8.59 10.72 1.72 o 7 3 4 21.12 29.41 1.71 o 0 4 4 0.33 1.10 0.89 o 1 4 4 192.72 185.62 6.75 o 2 4 4 103.24 95.67 2.66 o 3 4 4 644.94 603.66 14.86 o 4 4 4 52.33 50.77 2.02 o 5 4 4 84.77 81.39 3.26 o 6 4 4 3.00 3.72 0.77 o 7 4 4 1.68 1.04 0.61 o 1 5 4 61.98 65.62 4.02 o 2 5 4 13.79 14.15 0.69 o 3 5 4 92.80 87.71 2.52 o 4 5 4 87.58 76.42 2.26 o 5 5 4 49.12 42.26 1.73 o 6 5 4 3.55 3.74 0.65 o 7 5 4 22.29 25.17 2.24 o 0 6 4 56.07 53.53 2.66 o 1 6 4 226.77 219.75 5.29 o 2 6 4 201.23 191.20 4.63 o 3 6 4 24.30 28.35 1.10 o 4 6 4 35.72 33.98 1.29 o 5 6 4 0.06 0.43 0.37 o 6 6 4 51.91 45.18 2.63 o 7 6 4 2.26 3.87 0.84 o 1 7 4 0.41 0.46 0.31 o 2 7 4 34.17 34.21 1.33 o 3 7 4 78.14 83.51 2.50 o 4 7 4 8.53 6.80 0.72 o 5 7 4 196.82 172.90 4.63 o 6 7 4 1.13 0.39 0.52 o 7 7 4 62.63 55.15 2.58 o 0 8 4 16.29 14.77 0.87 o 1 8 4 48.67 42.87 1.23 o 2 8 4 41.75 34.91 1.28 o 3 8 4 1.93 1.32 0.37 o 4 8 4 34.26 34.21 1.24 o 5 8 4 20.53 17.72 0.85 o 6 8 4 5.23 6.68 0.73 o 7 8 4 20.08 22.62 1.06 o 1 9 4 25.44 27.27 0.98 o 2 9 4 1.13 2.12 0.45 o 3 9 4 44.48 46.39 1.51 o 4 9 4 1.65 2.76 0.43 o 5 9 4 43.94 40.55 1.41 o 6 9 4 0.33 0.69 0.32 o 0 10 4 459.11 458.65 13.47 o 1 10 4 306.66 292.70 6.54 o 2 10 4 95.32 90.07 2.45 o 3 10 4 127.99 126.46 3.27 o 4 10 4 2.48 1.98 0.39 o 5 10 4 0.02 0.05 0.34 o 6 10 4 2.91 3.15 0.39 o 1 11 4 11.57 11.01 0.64 o 2 11 4 105.84 102.10 2.72 o 3 11 4 0.65 0.90 0.39 o 4 11 4 0.60 0.01 0.32 o 5 11 4 58.39 54.98 1.69 o 6 11 4 0.86 0.74 0.29 o 0 12 4 169.58 157.56 4.51 o 1 12 4 612.69 605.39 13.17 o 2 12 4 1.97 0.94 0.39 o 3 12 4 4.29 7.62 0.54 o 4 12 4 7.54 7.66 0.61 o 5 12 4 0.72 1.16 0.33 o 6 12 4 1.38 1.87 0.34 o 1 13 4 39.65 37.36 1.23 o 2 13 4 0.10 0.55 0.36 o 3 13 4 3.54 3.62 0.44 o 4 13 4 80.78 90.31 2.34 o 5 13 4 169.60 161.55 4.48 o 0 14 4 25.30 27.41 1.62 o 1 14 4 96.89 101.84 2.52 o 2 14 4 52.17 55.09 1.64 o 3 14 4 0.68 0.28 0.37 o 4 14 4 29.82 31.16 1.09 o 5 14 4 21.26 22.12 1.52 o 1 15 4 14.71 14.52 0.82 o 2 15 4 6.36 6.22 0.47 o 3 15 4 12.76 11.05 0.60 o 4 15 4 11.88 9.85 0.57 o 0 16 4 2.25 3.16 0.76 o 1 16 4 41.66 45.39 1.68 o 2 16 4 1.80 1.58 0.34 o 3 16 4 56.12 56.07 1.63 o 4 16 4 14.94 15.16 0.80 o 1 17 4 6.47 5.41 0.89 o 2 17 4 7.89 10.99 0.54 o 3 17 4 2.40 1.97 0.29 o 0 18 4 11.78 17.18 2.82 o 1 18 4 138.29 156.82 7.38 o 2 18 4 4.19 5.11 0.54 o 1 0 5 90.39 87.42 3.17 o 2 0 5 106.08 100.43 3.26 o 3 0 5 35.01 31.85 1.59 o 4 0 5 0.03 -1.17 1.17 o 5 0 5 7.06 9.91 2.34 o 6 0 5 1.38 0.85 1.39 o 0 1 5 385.17 379.02 12.39 o 1 1 5 210.90 197.88 4.47 o 2 1 5 53.76 50.92 1.39 o 3 1 5 150.91 137.43 3.40 o 4 1 5 3.07 1.80 0.62 o 5 1 5 10.61 13.49 1.77 o 6 1 5 29.77 37.51 2.67 o 1 2 5 5.69 7.99 0.54 o 2 2 5 96.08 88.38 2.15 o 3 2 5 5.15 5.52 0.57 o 4 2 5 2.86 2.65 0.86 o 5 2 5 33.27 42.21 3.09 o 6 2 5 0.93 0.16 1.01 o 0 3 5 27.43 30.01 1.84 o 1 3 5 753.04 747.47 15.23 o 2 3 5 0.42 0.45 0.30 o 3 3 5 23.31 21.72 1.16 o 4 3 5 24.54 19.82 1.07 o 5 3 5 0.61 0.60 0.71 o 6 3 5 6.82 5.54 0.98 o 1 4 5 19.54 22.19 0.81 o 2 4 5 0.09 0.08 0.32 o 3 4 5 17.70 16.98 0.78 o 4 4 5 2.66 2.92 0.42 o 5 4 5 132.81 138.34 6.80 o 6 4 5 22.43 19.92 1.46 o 0 5 5 96.60 91.63 3.03 o 1 5 5 99.53 100.48 2.33 o 2 5 5 0.60 1.38 0.34 o 3 5 5 13.31 14.62 0.73 o 4 5 5 0.66 0.34 0.30 o 5 5 5 14.58 13.31 1.00 o 6 5 5 26.43 25.96 2.02 o 1 6 5 37.08 38.83 1.07 o 2 6 5 57.80 56.07 1.84 o 3 6 5 182.53 163.51 4.67 o 4 6 5 5.10 3.14 0.42 o 5 6 5 99.59 94.35 4.41 o 6 6 5 7.39 11.18 2.50 o 0 7 5 20.19 19.94 1.02 o 1 7 5 5.02 6.69 0.46 o 2 7 5 14.01 12.26 0.65 o 3 7 5 3.70 3.31 0.40 o 4 7 5 23.04 17.34 0.85 o 5 7 5 7.77 11.40 0.79 o 6 7 5 1.83 2.09 0.51 o 1 8 5 5.49 5.55 0.44 o 2 8 5 6.94 6.32 0.56 o 3 8 5 53.20 44.92 1.40 o 4 8 5 0.19 0.15 0.27 o 5 8 5 71.38 67.08 2.38 o 0 9 5 2.38 1.50 0.55 o 1 9 5 30.76 31.59 1.10 o 2 9 5 9.90 8.81 0.52 o 3 9 5 0.15 0.02 0.30 o 4 9 5 0.94 0.84 0.42 o 5 9 5 1.09 1.40 0.40 o 1 10 5 21.71 21.71 0.78 o 2 10 5 0.75 0.58 0.29 o 3 10 5 128.15 128.81 3.22 o 4 10 5 47.80 44.54 1.30 o 5 10 5 88.13 86.31 2.68 o 0 11 5 26.70 25.43 1.07 o 1 11 5 7.97 8.19 0.50 o 2 11 5 56.54 59.97 1.73 o 3 11 5 89.15 94.79 2.44 o 4 11 5 3.48 4.11 0.34 o 5 11 5 32.82 36.17 1.55 o 1 12 5 97.78 94.16 2.29 o 2 12 5 4.84 3.42 0.38 o 3 12 5 100.46 99.09 2.52 o 4 12 5 25.30 25.61 0.85 o 0 13 5 5.91 5.50 0.63 o 1 13 5 45.36 52.18 1.40 o 2 13 5 3.33 2.14 0.48 o 3 13 5 148.89 160.17 3.83 o 4 13 5 27.21 22.52 1.00 o 1 14 5 12.34 11.56 0.50 o 2 14 5 0.00 0.41 0.30 o 3 14 5 19.82 22.13 0.72 o 0 15 5 20.28 19.55 1.32 o 1 15 5 48.30 44.63 1.43 o 2 15 5 33.38 35.31 1.00 o 1 16 5 0.04 0.80 0.31 o 0 0 6 15.36 15.14 1.36 o 1 0 6 255.69 265.40 8.79 o 2 0 6 92.05 91.15 3.28 o 3 0 6 3.06 2.40 0.53 o 1 1 6 11.04 12.46 0.60 o 2 1 6 57.43 62.37 1.67 o 3 1 6 5.50 6.56 0.49 o 4 1 6 1.51 1.71 1.07 o 0 2 6 56.78 67.38 2.54 o 1 2 6 178.20 182.45 4.35 o 2 2 6 3.27 3.53 0.35 o 3 2 6 48.13 47.89 1.60 o 4 2 6 53.82 55.14 8.12 o 1 3 6 12.56 16.60 0.67 o 2 3 6 112.19 113.50 2.86 o 3 3 6 10.76 11.91 0.77 o 4 3 6 40.02 38.72 2.30 o 0 4 6 10.30 10.08 0.72 o 1 4 6 38.67 41.95 1.15 o 2 4 6 7.46 7.18 0.48 o 3 4 6 58.99 62.25 2.01 o 4 4 6 1.19 0.97 0.65 o 1 5 6 24.84 23.87 0.80 o 2 5 6 6.15 6.07 0.47 o 3 5 6 39.13 39.67 1.47 o 4 5 6 25.60 25.35 1.88 o 0 6 6 188.21 190.68 5.80 o 1 6 6 7.97 9.07 0.47 o 2 6 6 9.89 8.92 0.52 o 3 6 6 0.98 0.22 0.24 o 4 6 6 0.17 -0.26 0.26 o 1 7 6 8.01 7.33 0.46 o 2 7 6 9.68 8.14 0.49 o 3 7 6 39.18 42.55 1.79 o 4 7 6 20.30 23.55 1.83 o 0 8 6 47.03 43.21 1.58 o 1 8 6 1.80 1.87 0.28 o 2 8 6 23.81 23.95 0.81 o 3 8 6 0.14 0.27 0.25 o 1 9 6 14.82 15.84 0.59 o 2 9 6 6.30 5.67 0.37 o 3 9 6 42.62 43.03 1.26 o 0 10 6 3.56 3.52 0.34 o 1 10 6 1.73 1.74 0.25 o 2 10 6 12.04 12.91 0.55 o 1 11 6 1.92 1.68 0.23 o 2 11 6 2.39 2.88 0.29 o 0 12 6 20.26 13.37 1.29 o 1 0 7 29.89 35.26 2.00 o 0 1 7 41.47 46.61 1.74 o 1 1 7 11.03 11.54 0.48 o 1 2 7 20.57 21.03 0.84 o 0 3 7 9.36 10.43 0.91 o