#------------------------------------------------------------------------------ #$Date: 2023-01-04 15:34:25 +0200 (Wed, 04 Jan 2023) $ #$Revision: 280099 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519443.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519443 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.9686 _cell_length_b 18.8543 _cell_length_c 5.8060 _exptl_crystal_F_000 375.28 _reflns_d_resolution_high 0.8201 _cod_data_source_file 07-73DBT_27DBF.fcf _cod_data_source_block jw2251 _shelx_title ' jw2251_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.31 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11301.71 10659.12 383.56 o 4 0 0 5.69 7.14 0.59 o 6 0 0 166.45 172.20 5.96 o 8 0 0 42.50 42.60 1.14 o 2 1 0 5978.21 4756.86 241.35 o 4 1 0 492.23 493.70 6.86 o 6 1 0 233.08 237.94 5.14 o 8 1 0 0.29 0.28 0.08 o 0 2 0 6355.48 5783.55 207.87 o 2 2 0 1661.48 1709.45 23.22 o 4 2 0 92.89 97.41 1.50 o 6 2 0 3.69 3.26 0.22 o 8 2 0 19.85 21.49 0.47 o 2 3 0 3395.47 3273.22 50.05 o 4 3 0 335.11 340.90 4.81 o 6 3 0 443.38 423.80 6.36 o 8 3 0 230.10 232.71 4.31 o 0 4 0 417.44 329.09 7.54 o 2 4 0 511.70 514.26 7.06 o 4 4 0 17.10 18.35 0.46 o 6 4 0 987.85 924.14 14.93 o 8 4 0 117.31 120.17 2.28 o 2 5 0 84.54 92.11 1.27 o 4 5 0 7.56 6.48 0.29 o 6 5 0 514.76 480.10 7.47 o 8 5 0 364.27 370.79 6.78 o 0 6 0 3427.54 3954.29 81.87 o 2 6 0 1659.69 1703.58 22.37 o 4 6 0 17.90 20.76 0.52 o 6 6 0 234.58 228.34 4.01 o 8 6 0 64.12 66.25 1.25 o 2 7 0 1160.76 1250.76 17.07 o 4 7 0 864.77 894.83 17.79 o 6 7 0 596.53 566.56 9.19 o 8 7 0 61.00 59.90 1.36 o 0 8 0 322.57 356.19 7.55 o 2 8 0 333.56 351.48 5.30 o 4 8 0 288.37 293.38 5.59 o 6 8 0 5.08 5.17 0.29 o 8 8 0 10.84 10.92 0.32 o 2 9 0 2565.64 2722.30 50.90 o 4 9 0 922.26 955.01 22.23 o 6 9 0 248.07 229.87 3.83 o 8 9 0 89.56 89.96 1.71 o 0 10 0 30.83 50.72 1.39 o 2 10 0 1.63 5.37 0.38 o 4 10 0 2.42 2.78 0.31 o 6 10 0 123.96 115.67 2.00 o 8 10 0 293.56 298.25 6.66 o 2 11 0 39.47 44.27 0.89 o 4 11 0 712.05 690.61 9.79 o 6 11 0 100.17 95.14 1.77 o 8 11 0 5.10 4.70 0.20 o 0 12 0 1275.53 1374.83 35.14 o 2 12 0 7.50 8.37 0.37 o 4 12 0 0.56 1.08 0.13 o 6 12 0 64.45 68.07 1.55 o 8 12 0 204.53 206.74 4.55 o 2 13 0 141.95 139.58 3.27 o 4 13 0 1198.63 1184.09 18.17 o 6 13 0 40.22 38.49 0.85 o 8 13 0 137.14 135.88 3.53 o 0 14 0 541.68 531.31 13.84 o 2 14 0 443.26 428.41 7.37 o 4 14 0 662.62 651.38 10.57 o 6 14 0 290.87 294.98 5.10 o 2 15 0 555.46 541.19 8.39 o 4 15 0 73.12 69.46 1.25 o 6 15 0 1.55 2.72 0.16 o 0 16 0 264.85 267.93 8.03 o 2 16 0 975.24 912.47 14.05 o 4 16 0 483.88 485.64 7.53 o 6 16 0 48.74 54.18 1.07 o 2 17 0 233.93 210.56 3.70 o 4 17 0 1.29 1.39 0.13 o 6 17 0 15.43 13.76 0.33 o 0 18 0 21.56 27.83 0.80 o 2 18 0 75.01 78.16 1.39 o 4 18 0 11.03 9.32 0.28 o 6 18 0 14.04 12.67 0.41 o 2 19 0 130.58 131.26 2.21 o 4 19 0 282.96 281.43 5.15 o 0 20 0 111.06 116.19 2.79 o 2 20 0 30.00 38.14 0.76 o 4 20 0 0.16 0.33 0.09 o 2 21 0 5.33 5.13 0.20 o 0 22 0 296.31 326.26 8.92 o 2 22 0 136.59 139.31 2.94 o 1 0 1 3358.57 3044.86 62.98 o 2 0 1 8143.79 8073.02 213.30 o 3 0 1 5226.07 5304.20 89.67 o 4 0 1 104.54 113.25 1.72 o 5 0 1 400.65 398.97 6.75 o 6 0 1 6.19 5.55 0.23 o 7 0 1 15.68 13.24 0.39 o 8 0 1 54.27 58.32 1.18 o 9 0 1 1.20 0.57 0.09 o 0 1 1 361.25 417.98 5.02 o 1 1 1 4791.83 4292.36 88.80 o 2 1 1 8466.06 8435.51 129.47 o 3 1 1 41.88 40.94 0.52 o 4 1 1 2437.01 2576.43 24.80 o 5 1 1 31.03 32.18 0.53 o 6 1 1 24.30 21.13 0.37 o 7 1 1 23.87 24.04 0.40 o 8 1 1 6.70 6.98 0.18 o 9 1 1 58.70 65.96 0.93 o 1 2 1 28.88 31.38 0.35 o 2 2 1 988.17 1031.99 11.24 o 3 2 1 134.18 146.75 1.61 o 4 2 1 528.79 541.02 5.33 o 5 2 1 22.02 21.31 0.41 o 6 2 1 143.19 133.64 1.82 o 7 2 1 1.49 1.26 0.09 o 8 2 1 1.87 1.92 0.11 o 9 2 1 9.20 10.73 0.20 o 0 3 1 2220.16 2208.74 31.07 o 1 3 1 1344.37 1297.71 12.03 o 2 3 1 22.19 16.54 0.23 o 3 3 1 129.35 137.23 1.48 o 4 3 1 64.76 64.54 0.75 o 5 3 1 15.99 19.80 0.44 o 6 3 1 4.90 5.37 0.14 o 7 3 1 9.32 9.71 0.20 o 8 3 1 152.27 159.90 1.94 o 9 3 1 53.66 56.06 1.03 o 1 4 1 32.90 32.71 0.38 o 2 4 1 1.85 1.68 0.08 o 3 4 1 202.13 223.42 2.21 o 4 4 1 1860.94 1907.61 19.47 o 5 4 1 53.39 52.75 0.87 o 6 4 1 337.36 318.77 3.52 o 7 4 1 11.67 11.26 0.21 o 8 4 1 0.32 0.43 0.07 o 9 4 1 5.32 4.66 0.15 o 0 5 1 1166.22 1196.77 16.89 o 1 5 1 42.93 35.14 0.43 o 2 5 1 11.10 10.19 0.22 o 3 5 1 226.96 241.63 2.39 o 4 5 1 8.06 11.11 0.26 o 5 5 1 318.36 347.28 4.57 o 6 5 1 3.57 3.27 0.12 o 7 5 1 44.74 44.15 0.57 o 8 5 1 230.43 230.95 2.78 o 9 5 1 2.63 2.61 0.10 o 1 6 1 362.99 377.40 3.76 o 2 6 1 551.14 599.43 6.18 o 3 6 1 372.97 401.00 4.04 o 4 6 1 932.83 982.74 11.66 o 5 6 1 37.32 35.88 0.70 o 6 6 1 184.08 178.62 2.13 o 7 6 1 0.58 1.03 0.11 o 8 6 1 51.10 52.63 0.68 o 9 6 1 8.72 9.31 0.19 o 0 7 1 2270.79 2358.95 33.20 o 1 7 1 416.60 468.13 4.56 o 2 7 1 580.56 602.23 6.10 o 3 7 1 150.48 168.65 1.90 o 4 7 1 163.20 165.97 2.15 o 5 7 1 7.81 8.28 0.34 o 6 7 1 1.54 1.33 0.09 o 7 7 1 26.58 27.32 0.40 o 8 7 1 68.22 69.20 0.93 o 9 7 1 6.88 6.53 0.18 o 1 8 1 107.63 108.18 1.21 o 2 8 1 40.01 50.58 0.65 o 3 8 1 342.98 367.14 3.95 o 4 8 1 836.07 849.48 10.38 o 5 8 1 11.05 12.12 0.25 o 6 8 1 346.20 332.87 4.08 o 7 8 1 9.43 8.46 0.21 o 8 8 1 59.66 55.41 0.76 o 9 8 1 3.47 3.51 0.15 o 0 9 1 1349.83 1475.03 21.70 o 1 9 1 1444.82 1624.55 17.26 o 2 9 1 62.65 73.60 0.94 o 3 9 1 54.43 56.68 0.77 o 4 9 1 61.06 59.62 1.14 o 5 9 1 18.70 18.39 0.31 o 6 9 1 21.14 20.02 0.34 o 7 9 1 4.15 3.53 0.14 o 8 9 1 41.68 45.45 0.65 o 1 10 1 28.82 39.32 0.55 o 2 10 1 76.68 82.41 1.47 o 3 10 1 4.53 8.27 0.27 o 4 10 1 333.61 301.98 4.28 o 5 10 1 35.09 33.41 0.57 o 6 10 1 440.78 425.32 5.05 o 7 10 1 7.71 6.94 0.18 o 8 10 1 92.08 92.96 1.25 o 0 11 1 1.93 3.29 0.46 o 1 11 1 194.12 227.26 2.60 o 2 11 1 177.11 180.82 2.37 o 3 11 1 62.56 60.79 1.15 o 4 11 1 10.97 11.45 0.24 o 5 11 1 14.26 14.58 0.26 o 6 11 1 366.99 362.06 4.32 o 7 11 1 21.11 21.78 0.36 o 8 11 1 61.53 63.12 0.88 o 1 12 1 0.95 1.82 0.17 o 2 12 1 619.23 624.65 7.66 o 3 12 1 0.62 1.28 0.14 o 4 12 1 1.50 1.34 0.09 o 5 12 1 20.34 18.38 0.31 o 6 12 1 129.80 127.33 1.58 o 7 12 1 90.56 90.61 1.26 o 8 12 1 181.61 176.09 2.52 o 0 13 1 258.12 270.73 4.85 o 1 13 1 192.00 191.68 2.65 o 2 13 1 952.82 946.42 12.62 o 3 13 1 0.15 0.15 0.07 o 4 13 1 170.99 168.40 2.06 o 5 13 1 201.71 202.64 2.34 o 6 13 1 168.83 171.94 2.03 o 7 13 1 88.83 93.76 1.22 o 1 14 1 54.06 51.41 0.65 o 2 14 1 52.08 52.89 0.68 o 3 14 1 68.65 66.04 0.83 o 4 14 1 24.30 22.43 0.36 o 5 14 1 14.61 15.66 0.28 o 6 14 1 72.44 68.00 0.85 o 7 14 1 141.79 142.81 1.93 o 0 15 1 1875.55 1770.21 25.97 o 1 15 1 9.74 13.23 0.23 o 2 15 1 598.35 574.94 6.30 o 3 15 1 111.33 108.90 1.27 o 4 15 1 35.35 32.12 0.47 o 5 15 1 121.31 120.18 1.57 o 6 15 1 33.51 33.49 0.49 o 7 15 1 27.46 24.63 0.44 o 1 16 1 0.35 0.23 0.07 o 2 16 1 50.34 40.98 0.55 o 3 16 1 54.45 58.96 0.73 o 4 16 1 246.88 247.36 3.05 o 5 16 1 144.96 151.91 1.89 o 6 16 1 84.68 83.17 1.12 o 0 17 1 795.45 740.50 11.44 o 1 17 1 0.12 0.28 0.07 o 2 17 1 75.92 71.64 0.84 o 3 17 1 6.14 5.21 0.15 o 4 17 1 1.19 1.60 0.09 o 5 17 1 0.51 0.76 0.07 o 6 17 1 5.81 5.36 0.15 o 1 18 1 0.04 0.35 0.07 o 2 18 1 22.97 24.33 0.36 o 3 18 1 0.05 0.04 0.06 o 4 18 1 153.04 154.86 1.92 o 5 18 1 3.17 2.50 0.09 o 0 19 1 55.43 60.03 1.08 o 1 19 1 124.97 119.94 1.52 o 2 19 1 42.02 39.71 0.53 o 3 19 1 37.27 38.59 0.56 o 4 19 1 4.46 4.77 0.12 o 5 19 1 7.49 7.33 0.16 o 1 20 1 0.66 0.83 0.08 o 2 20 1 78.02 74.57 0.99 o 3 20 1 0.15 0.24 0.06 o 4 20 1 60.43 64.81 0.90 o 0 21 1 105.17 124.78 2.33 o 1 21 1 0.23 0.85 0.07 o 2 21 1 75.72 77.64 1.05 o 3 21 1 2.87 2.31 0.09 o 1 22 1 12.72 13.08 0.23 o 2 22 1 35.46 35.49 0.60 o 0 0 2 2877.28 2761.61 53.00 o 1 0 2 7.28 6.74 0.22 o 2 0 2 38.26 33.55 0.65 o 3 0 2 1823.39 1999.63 27.28 o 4 0 2 99.78 101.49 1.86 o 5 0 2 877.66 896.13 15.56 o 6 0 2 803.62 764.06 11.28 o 7 0 2 110.21 118.05 1.85 o 8 0 2 32.26 38.59 0.70 o 9 0 2 54.93 63.68 1.84 o 1 1 2 67.47 70.60 0.78 o 2 1 2 101.93 108.38 1.27 o 3 1 2 19.58 18.04 0.32 o 4 1 2 2149.09 2217.82 23.64 o 5 1 2 824.04 829.23 9.42 o 6 1 2 133.34 128.31 1.48 o 7 1 2 402.11 382.42 4.22 o 8 1 2 45.99 44.68 0.59 o 9 1 2 91.19 96.28 1.75 o 0 2 2 1411.73 1391.11 16.71 o 1 2 2 380.45 396.23 3.69 o 2 2 2 605.94 631.15 6.40 o 3 2 2 0.27 0.86 0.09 o 4 2 2 48.62 53.18 0.70 o 5 2 2 176.56 185.90 2.28 o 6 2 2 24.19 24.46 0.37 o 7 2 2 95.44 94.73 1.11 o 8 2 2 164.23 176.62 2.19 o 9 2 2 3.25 3.41 0.10 o 1 3 2 64.08 61.49 0.68 o 2 3 2 589.15 656.63 6.53 o 3 3 2 10.51 6.75 0.19 o 4 3 2 0.86 1.21 0.11 o 5 3 2 11.53 11.05 0.31 o 6 3 2 35.34 33.70 0.43 o 7 3 2 156.00 163.25 1.85 o 8 3 2 91.89 100.76 1.29 o 9 3 2 31.52 31.83 0.53 o 0 4 2 397.80 428.32 5.93 o 1 4 2 1612.26 1710.49 16.77 o 2 4 2 306.42 312.94 3.12 o 3 4 2 868.36 916.47 9.26 o 4 4 2 139.06 157.43 1.74 o 5 4 2 10.32 9.82 0.32 o 6 4 2 227.54 212.07 2.28 o 7 4 2 6.31 5.70 0.16 o 8 4 2 68.78 74.74 0.97 o 9 4 2 6.05 5.25 0.17 o 1 5 2 0.28 0.21 0.07 o 2 5 2 1897.91 2047.53 19.73 o 3 5 2 12.76 8.75 0.22 o 4 5 2 472.55 473.20 4.98 o 5 5 2 73.12 64.85 0.84 o 6 5 2 177.81 167.33 1.75 o 7 5 2 47.51 44.75 0.64 o 8 5 2 19.83 19.96 0.33 o 9 5 2 0.35 0.57 0.07 o 0 6 2 155.23 148.41 2.25 o 1 6 2 1082.25 1205.06 12.59 o 2 6 2 403.25 417.58 4.47 o 3 6 2 41.34 49.65 0.67 o 4 6 2 139.12 142.03 1.79 o 5 6 2 1.30 1.22 0.08 o 6 6 2 0.09 0.16 0.06 o 7 6 2 0.30 0.28 0.07 o 8 6 2 0.26 0.46 0.06 o 1 7 2 14.61 16.92 0.30 o 2 7 2 108.76 112.25 1.32 o 3 7 2 80.79 83.44 1.19 o 4 7 2 75.02 73.06 1.16 o 5 7 2 83.92 79.26 0.96 o 6 7 2 154.81 149.15 1.70 o 7 7 2 1.57 1.55 0.09 o 8 7 2 25.17 25.81 0.40 o 0 8 2 1702.52 1843.65 27.15 o 1 8 2 243.99 256.93 2.94 o 2 8 2 1331.00 1375.79 14.69 o 3 8 2 202.02 198.47 2.47 o 4 8 2 42.02 39.72 0.74 o 5 8 2 36.96 33.04 0.41 o 6 8 2 128.03 128.05 1.45 o 7 8 2 26.26 24.94 0.47 o 8 8 2 37.28 39.13 0.57 o 1 9 2 142.10 146.37 1.79 o 2 9 2 52.98 41.15 0.61 o 3 9 2 174.70 187.25 2.35 o 4 9 2 15.45 15.49 0.32 o 5 9 2 4.67 4.97 0.14 o 6 9 2 74.07 72.16 1.14 o 7 9 2 6.01 4.89 0.14 o 8 9 2 75.52 75.80 1.14 o 0 10 2 244.35 285.95 4.75 o 1 10 2 353.75 349.25 3.97 o 2 10 2 61.44 62.74 0.95 o 3 10 2 722.87 727.85 9.19 o 4 10 2 1.87 2.18 0.10 o 5 10 2 213.09 202.23 2.34 o 6 10 2 17.24 15.75 0.27 o 7 10 2 0.36 0.56 0.08 o 8 10 2 36.90 35.41 0.52 o 1 11 2 50.83 51.02 1.12 o 2 11 2 18.87 15.38 0.43 o 3 11 2 182.73 161.95 1.88 o 4 11 2 646.15 612.79 6.56 o 5 11 2 53.95 50.91 0.68 o 6 11 2 178.02 175.75 1.99 o 7 11 2 5.07 4.66 0.14 o 8 11 2 0.82 0.78 0.07 o 0 12 2 1162.10 1107.55 21.42 o 1 12 2 138.35 147.10 1.99 o 2 12 2 6.17 5.24 0.15 o 3 12 2 36.36 34.37 0.44 o 4 12 2 91.11 88.69 1.19 o 5 12 2 101.85 94.31 1.17 o 6 12 2 6.08 5.06 0.15 o 7 12 2 9.06 9.51 0.20 o 1 13 2 25.47 24.82 0.33 o 2 13 2 183.67 178.42 1.87 o 3 13 2 298.67 290.58 3.04 o 4 13 2 157.34 149.11 1.55 o 5 13 2 237.72 250.41 2.80 o 6 13 2 120.69 119.61 1.56 o 7 13 2 2.63 3.48 0.11 o 0 14 2 1324.56 1295.96 17.65 o 1 14 2 111.75 98.80 1.15 o 2 14 2 344.16 332.69 3.47 o 3 14 2 15.24 12.81 0.23 o 4 14 2 2.08 2.78 0.11 o 5 14 2 4.25 4.54 0.14 o 6 14 2 33.62 35.76 0.49 o 7 14 2 46.81 44.49 0.77 o 1 15 2 173.77 170.32 1.78 o 2 15 2 77.23 66.67 0.76 o 3 15 2 284.36 291.63 2.88 o 4 15 2 17.31 18.05 0.28 o 5 15 2 71.46 73.72 0.91 o 6 15 2 50.92 51.09 0.69 o 0 16 2 2.68 3.67 0.18 o 1 16 2 73.92 65.18 0.74 o 2 16 2 142.95 132.48 1.44 o 3 16 2 10.57 10.84 0.20 o 4 16 2 78.30 76.18 0.89 o 5 16 2 7.02 6.37 0.15 o 6 16 2 35.14 35.83 0.51 o 1 17 2 49.31 46.44 0.56 o 2 17 2 263.93 269.51 2.88 o 3 17 2 106.12 105.67 1.18 o 4 17 2 38.30 36.53 0.48 o 5 17 2 44.91 48.46 0.62 o 0 18 2 64.90 57.08 0.92 o 1 18 2 84.22 89.89 1.01 o 2 18 2 80.63 79.06 0.91 o 3 18 2 23.68 20.39 0.30 o 4 18 2 0.89 1.76 0.08 o 5 18 2 9.68 10.15 0.18 o 1 19 2 0.18 0.63 0.07 o 2 19 2 0.59 0.38 0.06 o 3 19 2 22.30 20.80 0.31 o 4 19 2 8.24 6.63 0.16 o 0 20 2 166.13 158.38 2.62 o 1 20 2 81.46 81.60 1.17 o 2 20 2 51.62 56.84 0.76 o 3 20 2 11.87 11.11 0.21 o 1 21 2 2.63 2.67 0.10 o 2 21 2 55.54 64.27 0.84 o 0 22 2 9.48 8.73 0.28 o 1 0 3 170.05 182.99 2.58 o 2 0 3 419.83 412.72 7.65 o 3 0 3 135.79 146.63 3.39 o 4 0 3 2.86 2.31 0.21 o 5 0 3 26.07 22.82 0.42 o 6 0 3 407.27 382.42 5.29 o 7 0 3 384.21 392.03 5.84 o 8 0 3 435.29 448.21 8.12 o 0 1 3 6.16 8.01 0.22 o 1 1 3 2.75 1.67 0.10 o 2 1 3 177.27 166.18 1.89 o 3 1 3 12.51 13.29 0.32 o 4 1 3 55.44 55.44 0.84 o 5 1 3 204.36 194.80 1.82 o 6 1 3 531.70 512.13 4.90 o 7 1 3 296.96 278.88 2.90 o 8 1 3 1.30 3.42 0.11 o 1 2 3 87.20 86.06 0.96 o 2 2 3 0.32 0.80 0.10 o 3 2 3 558.47 559.65 6.13 o 4 2 3 23.39 25.34 0.49 o 5 2 3 502.35 462.60 4.28 o 6 2 3 217.42 216.56 2.11 o 7 2 3 99.85 95.53 1.00 o 8 2 3 124.42 132.33 1.69 o 0 3 3 1421.35 1490.55 20.36 o 1 3 3 592.31 595.52 5.94 o 2 3 3 73.75 85.13 1.12 o 3 3 3 40.55 37.05 0.58 o 4 3 3 82.91 81.13 1.16 o 5 3 3 127.92 126.02 1.19 o 6 3 3 32.17 29.09 0.35 o 7 3 3 58.92 56.67 0.66 o 8 3 3 23.36 23.62 0.33 o 1 4 3 21.43 30.42 0.45 o 2 4 3 140.63 153.52 1.84 o 3 4 3 86.58 76.46 1.02 o 4 4 3 204.08 190.87 2.40 o 5 4 3 286.00 272.13 2.52 o 6 4 3 95.69 102.05 1.02 o 7 4 3 12.60 12.63 0.20 o 8 4 3 0.22 0.48 0.06 o 0 5 3 1374.49 1473.01 22.73 o 1 5 3 1792.63 1857.14 19.32 o 2 5 3 134.38 144.27 1.79 o 3 5 3 379.71 367.59 4.18 o 4 5 3 8.42 8.74 0.18 o 5 5 3 3.35 3.83 0.12 o 6 5 3 5.84 5.65 0.14 o 7 5 3 50.94 53.55 0.64 o 8 5 3 23.84 25.39 0.59 o 1 6 3 60.74 58.01 0.78 o 2 6 3 0.61 1.48 0.14 o 3 6 3 47.20 45.92 0.79 o 4 6 3 151.05 137.85 1.34 o 5 6 3 10.85 10.47 0.21 o 6 6 3 23.47 24.66 0.32 o 7 6 3 53.33 54.82 0.69 o 8 6 3 2.04 1.71 0.09 o 0 7 3 781.26 767.29 13.38 o 1 7 3 55.58 56.63 0.86 o 2 7 3 288.08 283.35 3.44 o 3 7 3 134.54 125.82 1.72 o 4 7 3 67.19 60.35 0.64 o 5 7 3 2.48 2.08 0.09 o 6 7 3 13.64 12.42 0.24 o 7 7 3 76.18 74.62 0.92 o 8 7 3 28.52 26.39 0.40 o 1 8 3 98.30 106.56 1.62 o 2 8 3 38.13 38.14 0.67 o 3 8 3 333.44 318.29 3.13 o 4 8 3 99.50 90.09 0.92 o 5 8 3 253.56 263.91 2.67 o 6 8 3 0.26 0.28 0.06 o 7 8 3 13.17 11.94 0.20 o 8 8 3 23.25 19.57 0.35 o 0 9 3 271.68 239.57 5.46 o 1 9 3 411.95 392.42 4.69 o 2 9 3 228.15 228.20 3.08 o 3 9 3 39.83 32.00 0.39 o 4 9 3 131.18 124.73 1.33 o 5 9 3 31.90 28.50 0.37 o 6 9 3 24.75 22.77 0.34 o 7 9 3 6.49 5.37 0.17 o 1 10 3 9.74 9.56 0.33 o 2 10 3 199.96 186.89 1.79 o 3 10 3 10.68 11.03 0.25 o 4 10 3 57.49 49.99 0.58 o 5 10 3 81.89 82.25 0.91 o 6 10 3 1.13 1.69 0.08 o 7 10 3 7.24 7.02 0.15 o 0 11 3 20.77 19.41 0.43 o 1 11 3 990.20 878.86 8.50 o 2 11 3 129.77 121.01 1.26 o 3 11 3 414.66 376.97 3.70 o 4 11 3 145.52 132.87 1.44 o 5 11 3 9.46 10.76 0.22 o 6 11 3 3.54 4.13 0.12 o 7 11 3 16.51 15.59 0.25 o 1 12 3 116.02 104.82 1.37 o 2 12 3 617.08 546.78 6.91 o 3 12 3 109.33 104.31 1.41 o 4 12 3 31.30 29.00 0.40 o 5 12 3 12.54 14.13 0.23 o 6 12 3 4.14 5.72 0.13 o 7 12 3 61.26 59.07 0.82 o 0 13 3 175.66 173.64 2.70 o 1 13 3 2.83 3.24 0.13 o 2 13 3 24.58 21.39 0.32 o 3 13 3 91.33 91.13 1.03 o 4 13 3 96.31 88.74 1.00 o 5 13 3 0.00 0.36 0.06 o 6 13 3 29.05 32.61 0.44 o 1 14 3 81.34 83.76 0.96 o 2 14 3 295.65 298.58 3.07 o 3 14 3 343.07 356.00 3.86 o 4 14 3 113.33 117.83 1.31 o 5 14 3 234.56 244.46 2.71 o 6 14 3 12.38 13.43 0.20 o 0 15 3 0.25 0.50 0.10 o 1 15 3 7.70 9.30 0.21 o 2 15 3 5.91 7.18 0.17 o 3 15 3 67.34 65.95 0.79 o 4 15 3 0.38 0.48 0.07 o 5 15 3 33.03 35.58 0.45 o 6 15 3 1.75 2.41 0.09 o 1 16 3 21.21 21.13 0.31 o 2 16 3 17.12 17.78 0.27 o 3 16 3 13.05 13.09 0.22 o 4 16 3 263.69 281.08 3.03 o 5 16 3 128.28 124.69 1.46 o 0 17 3 56.28 55.67 0.93 o 1 17 3 207.61 212.65 2.29 o 2 17 3 6.46 9.24 0.18 o 3 17 3 12.27 15.49 0.23 o 4 17 3 2.70 3.55 0.10 o 5 17 3 0.54 0.19 0.05 o 1 18 3 31.49 36.47 0.47 o 2 18 3 10.19 9.85 0.18 o 3 18 3 85.00 91.04 1.09 o 4 18 3 99.64 107.31 1.33 o 0 19 3 29.84 33.49 0.61 o 1 19 3 22.63 21.82 0.30 o 2 19 3 12.56 11.21 0.18 o 3 19 3 105.77 112.66 1.32 o 1 20 3 24.28 22.73 0.31 o 2 20 3 12.82 10.36 0.20 o 0 0 4 42.61 38.41 1.52 o 1 0 4 146.06 151.29 2.91 o 2 0 4 195.86 200.85 3.57 o 3 0 4 8.27 10.37 0.34 o 4 0 4 271.12 258.14 3.49 o 5 0 4 23.71 24.49 0.44 o 6 0 4 23.70 21.42 0.38 o 7 0 4 13.81 15.47 0.29 o 8 0 4 161.01 162.64 3.76 o 1 1 4 33.12 32.28 0.58 o 2 1 4 0.21 0.52 0.12 o 3 1 4 491.80 450.47 4.56 o 4 1 4 287.61 271.91 2.64 o 5 1 4 341.96 332.71 3.11 o 6 1 4 39.62 42.69 0.47 o 7 1 4 0.52 0.46 0.05 o 8 1 4 0.46 0.28 0.06 o 0 2 4 88.90 96.81 2.29 o 1 2 4 98.29 90.99 1.32 o 2 2 4 78.06 71.87 1.10 o 3 2 4 235.36 214.57 2.13 o 4 2 4 3.08 2.10 0.09 o 5 2 4 69.87 65.12 0.68 o 6 2 4 11.21 11.05 0.18 o 7 2 4 20.89 22.58 0.28 o 1 3 4 337.79 342.54 4.32 o 2 3 4 278.61 275.81 3.77 o 3 3 4 495.32 451.11 4.48 o 4 3 4 117.37 109.45 1.16 o 5 3 4 41.14 39.40 0.46 o 6 3 4 10.40 10.57 0.17 o 7 3 4 28.83 30.80 0.36 o 0 4 4 4.05 5.22 0.49 o 1 4 4 278.39 261.54 4.19 o 2 4 4 168.36 165.36 1.80 o 3 4 4 675.75 642.31 6.23 o 4 4 4 95.91 97.00 1.02 o 5 4 4 62.19 58.34 0.63 o 6 4 4 4.04 4.31 0.11 o 7 4 4 15.76 16.04 0.25 o 1 5 4 92.59 95.42 1.76 o 2 5 4 24.57 23.36 0.33 o 3 5 4 218.60 211.27 2.19 o 4 5 4 83.57 76.29 0.79 o 5 5 4 134.15 131.98 1.32 o 6 5 4 4.57 3.67 0.10 o 7 5 4 32.74 34.50 0.44 o 0 6 4 100.09 94.06 1.74 o 1 6 4 274.10 254.40 3.19 o 2 6 4 247.20 229.83 2.42 o 3 6 4 11.50 14.22 0.23 o 4 6 4 38.03 40.38 0.46 o 5 6 4 3.39 2.52 0.09 o 6 6 4 72.05 67.24 0.74 o 7 6 4 16.43 18.43 0.25 o 1 7 4 2.51 2.80 0.11 o 2 7 4 55.35 55.97 0.64 o 3 7 4 153.10 157.25 1.60 o 4 7 4 1.19 0.44 0.06 o 5 7 4 309.31 309.73 2.99 o 6 7 4 0.10 0.17 0.05 o 7 7 4 81.65 71.09 1.08 o 0 8 4 11.63 9.12 0.27 o 1 8 4 102.73 87.01 0.98 o 2 8 4 40.45 32.21 0.40 o 3 8 4 3.33 3.31 0.11 o 4 8 4 36.59 37.05 0.45 o 5 8 4 55.26 53.02 0.58 o 6 8 4 3.06 3.82 0.10 o 7 8 4 75.53 76.80 0.94 o 1 9 4 48.11 45.65 0.56 o 2 9 4 1.12 0.72 0.07 o 3 9 4 85.86 91.04 0.99 o 4 9 4 5.83 6.78 0.15 o 5 9 4 66.06 67.26 0.74 o 6 9 4 0.01 0.14 0.05 o 7 9 4 121.17 117.10 1.63 o 0 10 4 586.82 535.11 7.38 o 1 10 4 403.09 364.11 3.65 o 2 10 4 152.18 136.68 1.45 o 3 10 4 173.55 172.05 1.71 o 4 10 4 5.56 4.76 0.13 o 5 10 4 3.76 3.84 0.12 o 6 10 4 1.42 1.03 0.06 o 1 11 4 2.08 1.45 0.12 o 2 11 4 120.58 111.28 1.17 o 3 11 4 14.56 14.07 0.23 o 4 11 4 0.07 0.28 0.07 o 5 11 4 108.60 106.92 1.26 o 6 11 4 0.01 0.17 0.05 o 0 12 4 281.56 246.32 3.55 o 1 12 4 766.97 739.24 7.16 o 2 12 4 4.41 2.61 0.11 o 3 12 4 5.55 8.80 0.22 o 4 12 4 19.78 18.71 0.28 o 5 12 4 1.78 1.18 0.08 o 6 12 4 0.91 1.86 0.07 o 1 13 4 36.08 32.91 0.41 o 2 13 4 0.03 0.22 0.08 o 3 13 4 10.34 9.88 0.19 o 4 13 4 134.96 153.40 1.70 o 5 13 4 225.49 231.23 2.55 o 0 14 4 28.68 32.81 0.63 o 1 14 4 179.09 189.23 1.94 o 2 14 4 80.83 85.02 0.97 o 3 14 4 0.21 0.21 0.07 o 4 14 4 66.65 69.76 0.86 o 5 14 4 49.68 53.71 0.64 o 1 15 4 23.36 23.63 0.33 o 2 15 4 10.48 10.32 0.19 o 3 15 4 25.00 23.71 0.33 o 4 15 4 15.28 11.74 0.19 o 0 16 4 1.57 2.35 0.15 o 1 16 4 82.19 91.75 1.05 o 2 16 4 4.69 5.21 0.13 o 3 16 4 88.26 90.61 1.09 o 4 16 4 20.40 22.11 0.30 o 1 17 4 13.21 12.04 0.20 o 2 17 4 14.06 17.54 0.26 o 3 17 4 14.10 12.09 0.19 o 0 18 4 5.68 8.58 0.23 o 1 18 4 222.65 244.07 2.89 o 2 18 4 12.44 13.67 0.25 o 1 0 5 140.56 141.61 2.55 o 2 0 5 157.56 161.81 2.60 o 3 0 5 103.66 99.57 1.59 o 4 0 5 0.03 0.04 0.08 o 5 0 5 22.04 24.74 0.45 o 6 0 5 0.45 0.16 0.08 o 0 1 5 475.47 450.03 9.54 o 1 1 5 389.20 371.05 4.82 o 2 1 5 65.85 64.76 0.79 o 3 1 5 232.35 224.58 2.36 o 4 1 5 3.78 2.83 0.10 o 5 1 5 15.25 16.67 0.24 o 6 1 5 47.86 54.70 0.60 o 1 2 5 4.12 5.49 0.19 o 2 2 5 91.00 80.17 0.98 o 3 2 5 0.93 0.77 0.07 o 4 2 5 1.89 2.35 0.09 o 5 2 5 63.80 70.12 0.74 o 6 2 5 1.20 1.17 0.06 o 0 3 5 3.58 3.41 0.24 o 1 3 5 1083.84 1064.54 14.51 o 2 3 5 0.94 0.75 0.07 o 3 3 5 27.02 23.48 0.33 o 4 3 5 26.77 24.70 0.32 o 5 3 5 13.17 12.43 0.19 o 6 3 5 13.64 13.55 0.19 o 1 4 5 11.38 12.39 0.32 o 2 4 5 1.48 1.58 0.09 o 3 4 5 49.18 49.04 0.59 o 4 4 5 7.22 7.74 0.16 o 5 4 5 228.43 235.34 2.36 o 6 4 5 17.55 14.84 0.23 o 0 5 5 116.23 103.68 2.90 o 1 5 5 121.43 116.27 2.23 o 2 5 5 0.42 1.10 0.09 o 3 5 5 13.88 14.87 0.24 o 4 5 5 0.81 0.98 0.07 o 5 5 5 1.93 1.72 0.08 o 6 5 5 49.08 47.24 0.58 o 1 6 5 80.75 77.06 1.14 o 2 6 5 47.67 44.91 0.59 o 3 6 5 320.30 307.93 3.21 o 4 6 5 14.92 13.62 0.22 o 5 6 5 166.28 167.82 1.76 o 6 6 5 4.51 6.53 0.11 o 0 7 5 14.01 13.95 0.54 o 1 7 5 19.64 22.21 0.40 o 2 7 5 22.96 19.26 0.30 o 3 7 5 8.78 9.26 0.19 o 4 7 5 35.60 29.91 0.39 o 5 7 5 27.66 37.75 0.47 o 6 7 5 1.03 0.93 0.05 o 1 8 5 11.07 10.28 0.27 o 2 8 5 10.03 8.66 0.19 o 3 8 5 95.31 87.38 0.97 o 4 8 5 0.20 0.23 0.06 o 5 8 5 120.89 121.91 1.29 o 0 9 5 8.03 6.28 0.24 o 1 9 5 73.80 73.08 0.90 o 2 9 5 13.38 12.32 0.24 o 3 9 5 0.53 0.68 0.07 o 4 9 5 0.54 0.40 0.06 o 5 9 5 7.10 6.72 0.14 o 1 10 5 32.10 31.25 0.45 o 2 10 5 0.21 0.16 0.07 o 3 10 5 239.87 237.71 2.48 o 4 10 5 45.41 42.39 0.59 o 5 10 5 180.95 187.86 2.08 o 0 11 5 26.30 25.14 0.53 o 1 11 5 13.75 16.22 0.27 o 2 11 5 74.89 78.27 0.92 o 3 11 5 93.24 96.17 1.10 o 4 11 5 11.22 12.28 0.19 o 5 11 5 31.81 35.60 0.53 o 1 12 5 148.31 140.40 1.58 o 2 12 5 0.34 0.03 0.06 o 3 12 5 199.66 196.86 2.02 o 4 12 5 30.84 32.62 0.42 o 0 13 5 12.54 12.15 0.28 o 1 13 5 87.23 98.78 1.13 o 2 13 5 1.93 1.38 0.08 o 3 13 5 214.84 226.47 2.63 o 4 13 5 27.82 25.95 0.38 o 1 14 5 22.42 21.73 0.31 o 2 14 5 0.02 -0.05 0.05 o 3 14 5 43.70 49.57 0.61 o 0 15 5 20.30 18.79 0.37 o 1 15 5 104.23 101.37 1.28 o 2 15 5 39.41 45.60 0.63 o 1 16 5 1.18 1.60 0.08 o 0 0 6 12.50 11.10 0.76 o 1 0 6 489.51 536.83 13.81 o 2 0 6 114.10 120.56 2.45 o 3 0 6 17.60 17.26 0.38 o 4 0 6 92.48 107.28 1.80 o 5 0 6 15.62 20.02 0.44 o 1 1 6 5.05 5.79 0.23 o 2 1 6 94.80 103.23 1.45 o 3 1 6 24.90 28.79 0.41 o 4 1 6 5.15 4.19 0.14 o 5 1 6 61.96 71.49 0.95 o 0 2 6 95.96 104.23 5.32 o 1 2 6 252.16 269.68 5.01 o 2 2 6 0.63 0.75 0.14 o 3 2 6 82.12 91.47 1.11 o 4 2 6 56.18 61.17 0.74 o 5 2 6 1.72 2.12 0.07 o 1 3 6 38.90 45.84 1.58 o 2 3 6 151.04 159.40 2.34 o 3 3 6 54.72 58.20 0.77 o 4 3 6 76.47 80.29 0.95 o 5 3 6 11.20 13.25 0.61 o 0 4 6 8.73 9.79 0.75 o 1 4 6 51.66 57.77 1.07 o 2 4 6 12.50 13.06 0.30 o 3 4 6 69.23 79.46 1.09 o 4 4 6 0.07 0.09 0.04 o 1 5 6 33.50 32.93 0.66 o 2 5 6 12.48 12.58 0.39 o 3 5 6 77.84 81.39 1.12 o 4 5 6 31.66 32.04 0.45 o 0 6 6 292.76 291.95 7.41 o 1 6 6 42.03 41.08 0.84 o 2 6 6 22.37 20.71 0.43 o 3 6 6 0.72 0.23 0.08 o 4 6 6 0.04 0.15 0.04 o 1 7 6 10.82 9.72 0.26 o 2 7 6 10.78 8.24 0.23 o 3 7 6 76.38 84.07 1.15 o 4 7 6 29.06 34.26 0.90 o 0 8 6 71.41 68.88 2.88 o 1 8 6 13.13 12.28 0.30 o 2 8 6 36.77 34.49 0.63 o 3 8 6 1.73 1.11 0.09 o 1 9 6 34.48 37.07 0.78 o 2 9 6 7.55 7.21 0.19 o 3 9 6 91.16 96.20 1.43 o 0 10 6 9.88 9.98 0.47 o 1 10 6 8.12 8.84 0.22 o 2 10 6 20.13 20.93 0.38 o 1 11 6 4.57 4.87 0.14 o 2 11 6 4.03 4.64 0.13 o 0 12 6 22.89 16.81 0.52 o