#------------------------------------------------------------------------------ #$Date: 2023-01-04 15:34:53 +0200 (Wed, 04 Jan 2023) $ #$Revision: 280101 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519445.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519445 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.0589 _cell_length_b 18.8454 _cell_length_c 5.7503 _exptl_crystal_F_000 362.15 _reflns_d_resolution_high 0.8111 _cod_data_source_file 09-DBT_DBF_FLU.fcf _cod_data_source_block dbt_dbf_flu _shelx_title ' jw2307_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.82 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 21.29 21.92 1.02 o 6 0 0 391.55 417.48 8.22 o 8 0 0 6.30 5.44 0.47 o 2 1 0 7014.58 6720.03 70.49 o 4 1 0 228.27 230.20 2.39 o 6 1 0 86.18 81.84 2.34 o 8 1 0 3.21 2.47 0.24 o 0 2 0 4522.93 4149.91 61.79 o 2 2 0 907.79 914.83 5.69 o 4 2 0 71.75 74.06 1.23 o 6 2 0 11.55 14.26 1.05 o 8 2 0 3.37 3.14 0.28 o 2 3 0 2356.62 2211.79 10.91 o 4 3 0 51.54 55.67 1.50 o 6 3 0 302.49 286.44 4.19 o 8 3 0 203.84 202.43 2.27 o 0 4 0 1044.42 852.63 19.53 o 2 4 0 203.84 195.25 1.45 o 4 4 0 51.89 53.34 1.60 o 6 4 0 824.70 789.88 4.73 o 8 4 0 25.70 25.21 0.77 o 2 5 0 0.42 0.51 0.14 o 4 5 0 79.64 79.04 1.42 o 6 5 0 355.74 329.04 2.44 o 8 5 0 297.30 299.13 3.02 o 0 6 0 2146.18 2235.84 17.53 o 2 6 0 1123.96 1059.58 6.17 o 4 6 0 59.37 60.28 1.44 o 6 6 0 136.16 134.79 1.30 o 8 6 0 13.29 13.98 0.59 o 2 7 0 814.43 802.22 5.29 o 4 7 0 491.41 501.01 4.68 o 6 7 0 486.01 458.24 3.22 o 8 7 0 50.81 53.64 1.00 o 0 8 0 714.85 756.16 8.22 o 2 8 0 154.56 132.20 2.17 o 4 8 0 288.97 294.95 3.69 o 6 8 0 48.02 45.49 0.63 o 8 8 0 1.28 1.98 0.29 o 2 9 0 2167.42 2337.42 17.33 o 4 9 0 601.04 624.19 6.29 o 6 9 0 120.74 115.77 1.08 o 8 9 0 112.47 122.47 1.54 o 0 10 0 186.59 237.73 4.38 o 2 10 0 73.16 91.01 2.18 o 4 10 0 5.83 7.97 0.83 o 6 10 0 77.98 82.54 0.91 o 8 10 0 310.13 329.66 3.08 o 2 11 0 0.76 1.73 0.33 o 4 11 0 408.73 426.81 2.76 o 6 11 0 7.71 6.87 0.30 o 8 11 0 4.00 4.52 0.45 o 0 12 0 679.58 730.43 8.83 o 2 12 0 38.70 39.10 1.24 o 4 12 0 3.97 3.67 0.26 o 6 12 0 94.15 100.15 1.07 o 8 12 0 281.75 289.11 3.74 o 2 13 0 94.85 85.69 2.42 o 4 13 0 930.44 921.93 5.33 o 6 13 0 2.12 2.04 0.40 o 8 13 0 160.12 167.63 3.34 o 0 14 0 175.35 158.63 8.71 o 2 14 0 242.81 218.42 1.69 o 4 14 0 743.25 717.31 5.21 o 6 14 0 379.08 381.85 2.81 o 2 15 0 523.99 497.68 3.33 o 4 15 0 3.75 5.79 0.38 o 6 15 0 20.10 25.35 0.61 o 0 16 0 168.73 165.38 2.54 o 2 16 0 1070.13 951.22 6.00 o 4 16 0 612.35 599.01 4.40 o 6 16 0 33.81 37.48 0.69 o 2 17 0 120.15 99.35 1.27 o 4 17 0 45.78 44.46 0.86 o 6 17 0 0.83 0.79 0.25 o 0 18 0 7.20 10.99 0.83 o 2 18 0 51.87 50.64 1.66 o 4 18 0 8.71 6.50 0.38 o 6 18 0 1.41 1.67 0.28 o 2 19 0 68.77 67.56 1.13 o 4 19 0 223.75 220.45 2.03 o 0 20 0 49.58 44.27 2.08 o 2 20 0 3.31 6.27 0.46 o 4 20 0 0.35 0.15 0.15 o 2 21 0 0.42 0.65 0.22 o 4 21 0 10.10 8.12 0.39 o 0 22 0 317.28 357.70 5.06 o 2 22 0 127.24 132.40 1.80 o 1 0 1 3550.75 3429.73 18.21 o 2 0 1 6465.80 6457.85 39.43 o 3 0 1 4713.68 4780.47 29.57 o 4 0 1 529.60 549.75 4.62 o 5 0 1 206.96 194.51 2.79 o 6 0 1 1.57 1.64 0.30 o 7 0 1 10.58 9.35 0.40 o 8 0 1 45.80 47.41 0.76 o 9 0 1 2.96 1.99 0.33 o 0 1 1 116.93 132.01 1.18 o 1 1 1 5524.09 5283.47 22.74 o 2 1 1 7712.46 8001.25 42.20 o 3 1 1 24.22 26.07 0.51 o 4 1 1 2297.19 2437.71 12.49 o 5 1 1 29.95 28.65 0.93 o 6 1 1 1.91 1.61 0.15 o 7 1 1 27.14 27.57 0.49 o 8 1 1 7.92 10.50 0.43 o 9 1 1 55.41 54.80 0.84 o 1 2 1 21.85 22.44 0.40 o 2 2 1 582.98 604.26 2.77 o 3 2 1 61.51 75.67 0.81 o 4 2 1 177.91 175.85 1.73 o 5 2 1 0.23 0.45 0.23 o 6 2 1 44.89 44.79 0.66 o 7 2 1 1.62 1.32 0.16 o 8 2 1 0.30 0.86 0.17 o 9 2 1 17.71 20.02 0.45 o 0 3 1 1227.45 1155.75 6.51 o 1 3 1 1011.26 971.30 4.44 o 2 3 1 197.78 171.65 1.14 o 3 3 1 86.23 90.50 0.85 o 4 3 1 64.78 67.70 0.86 o 5 3 1 28.84 30.58 0.92 o 6 3 1 42.96 43.42 0.46 o 7 3 1 8.09 9.04 0.35 o 8 3 1 109.02 108.59 0.89 o 9 3 1 69.61 67.63 0.80 o 1 4 1 8.85 8.08 0.29 o 2 4 1 72.55 65.82 0.70 o 3 4 1 124.28 134.45 1.16 o 4 4 1 1146.50 1159.07 6.53 o 5 4 1 22.39 25.59 0.91 o 6 4 1 114.38 115.57 0.83 o 7 4 1 30.31 31.05 0.44 o 8 4 1 3.44 3.51 0.28 o 9 4 1 2.24 1.35 0.21 o 0 5 1 573.79 524.94 3.29 o 1 5 1 122.00 123.40 0.97 o 2 5 1 40.42 40.64 0.59 o 3 5 1 157.40 162.75 1.39 o 4 5 1 11.21 13.70 0.62 o 5 5 1 358.45 365.35 3.20 o 6 5 1 0.21 0.26 0.11 o 7 5 1 68.80 67.82 0.63 o 8 5 1 220.73 212.62 1.47 o 9 5 1 0.02 0.07 0.16 o 1 6 1 333.42 325.65 1.93 o 2 6 1 306.75 336.54 1.95 o 3 6 1 266.66 294.78 1.87 o 4 6 1 535.36 501.45 3.13 o 5 6 1 10.85 10.71 0.63 o 6 6 1 57.60 59.44 0.57 o 7 6 1 4.44 4.49 0.22 o 8 6 1 68.95 70.63 0.69 o 9 6 1 10.98 11.00 0.35 o 0 7 1 1556.21 1449.12 8.06 o 1 7 1 303.26 330.49 2.01 o 2 7 1 245.24 272.66 1.72 o 3 7 1 114.00 118.34 1.10 o 4 7 1 174.77 165.99 1.49 o 5 7 1 5.92 6.18 0.50 o 6 7 1 4.12 4.54 0.21 o 7 7 1 18.59 19.29 0.42 o 8 7 1 26.27 25.44 0.42 o 9 7 1 2.39 2.24 0.19 o 1 8 1 171.45 187.58 1.43 o 2 8 1 6.88 9.96 0.39 o 3 8 1 528.22 566.63 3.25 o 4 8 1 553.56 525.98 3.19 o 5 8 1 38.62 41.25 0.50 o 6 8 1 257.19 254.10 1.46 o 7 8 1 0.89 0.76 0.13 o 8 8 1 67.36 64.14 0.67 o 9 8 1 1.07 1.38 0.16 o 0 9 1 779.92 774.51 5.52 o 1 9 1 1345.95 1484.09 6.66 o 2 9 1 7.39 11.00 0.44 o 3 9 1 17.75 17.05 0.58 o 4 9 1 75.33 76.51 1.17 o 5 9 1 20.40 22.68 0.37 o 6 9 1 0.59 0.92 0.14 o 7 9 1 0.07 0.05 0.12 o 8 9 1 4.05 4.46 0.22 o 9 9 1 0.05 0.00 0.14 o 1 10 1 60.71 77.52 0.99 o 2 10 1 18.35 20.57 0.61 o 3 10 1 31.89 41.43 0.89 o 4 10 1 118.79 110.47 1.45 o 5 10 1 23.40 23.95 0.38 o 6 10 1 386.11 397.16 2.01 o 7 10 1 4.62 4.13 0.21 o 8 10 1 86.63 89.70 0.76 o 0 11 1 85.70 92.58 1.60 o 1 11 1 127.49 145.05 1.49 o 2 11 1 53.00 60.95 1.18 o 3 11 1 44.36 41.62 1.07 o 4 11 1 45.44 47.66 0.81 o 5 11 1 17.02 17.55 0.37 o 6 11 1 358.90 372.10 1.88 o 7 11 1 66.99 66.86 0.65 o 8 11 1 17.97 17.45 0.46 o 1 12 1 0.40 0.36 0.23 o 2 12 1 422.76 415.79 3.17 o 3 12 1 2.66 2.25 0.17 o 4 12 1 37.01 38.78 0.55 o 5 12 1 8.99 7.37 0.25 o 6 12 1 107.31 114.41 0.88 o 7 12 1 105.51 104.72 0.89 o 8 12 1 194.25 192.17 1.75 o 0 13 1 62.73 58.89 1.47 o 1 13 1 187.02 168.04 2.14 o 2 13 1 601.78 589.12 3.39 o 3 13 1 0.05 0.15 0.13 o 4 13 1 101.03 100.92 0.81 o 5 13 1 213.50 220.55 1.35 o 6 13 1 136.21 144.09 1.04 o 7 13 1 64.97 70.54 0.75 o 8 13 1 1.53 2.05 0.31 o 1 14 1 93.03 84.92 0.70 o 2 14 1 9.41 11.85 0.31 o 3 14 1 142.99 137.43 0.93 o 4 14 1 4.24 3.56 0.21 o 5 14 1 3.36 4.38 0.22 o 6 14 1 53.67 52.60 0.62 o 7 14 1 139.81 143.70 1.17 o 0 15 1 1717.43 1562.17 10.45 o 1 15 1 3.59 7.49 0.26 o 2 15 1 435.58 415.76 1.95 o 3 15 1 181.74 150.69 1.38 o 4 15 1 36.57 31.64 0.52 o 5 15 1 138.80 144.29 1.10 o 6 15 1 120.56 117.74 0.96 o 7 15 1 16.89 16.48 0.46 o 1 16 1 3.54 2.84 0.19 o 2 16 1 140.18 123.88 0.90 o 3 16 1 47.59 48.22 0.65 o 4 16 1 172.30 169.68 1.18 o 5 16 1 174.93 181.54 1.24 o 6 16 1 31.94 32.52 0.49 o 7 16 1 43.01 40.26 1.29 o 0 17 1 727.99 647.44 4.67 o 1 17 1 19.11 20.61 0.45 o 2 17 1 46.44 40.57 0.53 o 3 17 1 32.86 28.22 0.46 o 4 17 1 0.80 0.71 0.15 o 5 17 1 0.94 1.32 0.16 o 6 17 1 31.39 28.32 0.44 o 1 18 1 0.02 0.27 0.15 o 2 18 1 7.23 7.74 0.27 o 3 18 1 0.39 0.10 0.13 o 4 18 1 75.82 79.83 0.76 o 5 18 1 1.18 0.65 0.12 o 6 18 1 9.85 7.33 0.27 o 0 19 1 5.84 6.81 0.47 o 1 19 1 99.68 92.41 0.89 o 2 19 1 14.88 11.62 0.38 o 3 19 1 35.82 38.23 0.50 o 4 19 1 6.05 6.53 0.23 o 5 19 1 10.50 12.18 0.31 o 1 20 1 0.23 0.29 0.15 o 2 20 1 57.91 51.58 0.76 o 3 20 1 1.11 0.85 0.16 o 4 20 1 23.78 28.71 0.69 o 0 21 1 54.05 68.21 0.91 o 1 21 1 5.76 7.50 0.29 o 2 21 1 52.61 57.85 1.24 o 3 21 1 1.09 0.50 0.16 o 4 21 1 10.17 10.06 0.51 o 1 22 1 17.09 17.24 0.41 o 2 22 1 22.69 25.39 0.46 o 0 0 2 2022.40 2096.24 18.85 o 1 0 2 146.78 153.44 1.67 o 2 0 2 151.18 144.75 1.56 o 3 0 2 2890.04 3097.50 18.45 o 4 0 2 198.27 209.43 2.49 o 5 0 2 775.07 775.27 6.51 o 6 0 2 1117.59 1114.41 6.49 o 7 0 2 37.55 41.94 0.71 o 8 0 2 19.79 23.55 0.55 o 9 0 2 37.06 37.85 0.78 o 1 1 2 185.78 206.84 1.36 o 2 1 2 64.28 66.91 0.73 o 3 1 2 0.31 0.80 0.17 o 4 1 2 1669.93 1709.93 8.67 o 5 1 2 740.28 736.74 4.44 o 6 1 2 27.24 26.85 0.41 o 7 1 2 303.05 299.31 1.52 o 8 1 2 49.27 43.49 0.54 o 9 1 2 81.94 81.81 0.85 o 0 2 2 813.03 859.16 6.06 o 1 2 2 132.30 129.05 0.94 o 2 2 2 360.02 369.05 2.11 o 3 2 2 31.29 37.75 0.66 o 4 2 2 70.52 81.17 1.05 o 5 2 2 187.91 193.49 1.95 o 6 2 2 4.00 4.30 0.19 o 7 2 2 54.14 52.57 0.55 o 8 2 2 150.77 158.27 1.14 o 9 2 2 1.63 2.31 0.20 o 1 3 2 44.08 45.62 0.61 o 2 3 2 362.39 390.68 2.20 o 3 3 2 13.58 17.17 0.47 o 4 3 2 62.46 57.75 0.93 o 5 3 2 5.01 5.20 0.43 o 6 3 2 2.00 1.78 0.15 o 7 3 2 156.60 165.40 1.10 o 8 3 2 86.06 98.43 0.84 o 9 3 2 36.24 35.42 0.50 o 0 4 2 832.86 850.03 5.25 o 1 4 2 855.10 901.62 4.42 o 2 4 2 107.27 103.30 0.96 o 3 4 2 706.65 755.74 3.92 o 4 4 2 80.72 93.02 1.13 o 5 4 2 9.74 8.50 0.53 o 6 4 2 193.22 183.35 1.07 o 7 4 2 1.03 1.66 0.17 o 8 4 2 32.93 34.71 0.47 o 9 4 2 44.77 41.63 0.49 o 1 5 2 1.95 1.52 0.20 o 2 5 2 1508.98 1565.13 7.32 o 3 5 2 0.24 1.07 0.20 o 4 5 2 218.75 241.06 1.95 o 5 5 2 25.94 22.53 0.46 o 6 5 2 144.95 135.75 0.87 o 7 5 2 29.68 29.84 0.49 o 8 5 2 13.61 14.04 0.34 o 9 5 2 4.28 4.44 0.18 o 0 6 2 5.41 4.80 0.44 o 1 6 2 655.60 689.68 3.82 o 2 6 2 208.54 195.32 1.92 o 3 6 2 7.93 11.77 0.49 o 4 6 2 94.70 96.73 1.21 o 5 6 2 5.35 4.48 0.18 o 6 6 2 6.83 8.32 0.26 o 7 6 2 11.54 12.62 0.32 o 8 6 2 18.35 18.16 0.39 o 9 6 2 8.37 8.59 0.23 o 1 7 2 41.66 39.53 0.67 o 2 7 2 51.21 43.85 0.91 o 3 7 2 9.88 8.48 0.44 o 4 7 2 7.29 7.87 0.43 o 5 7 2 10.22 11.01 0.28 o 6 7 2 121.49 110.06 0.77 o 7 7 2 5.64 5.42 0.25 o 8 7 2 22.00 23.54 0.41 o 9 7 2 16.69 15.55 0.41 o 0 8 2 1384.84 1504.01 9.30 o 1 8 2 98.99 102.92 1.14 o 2 8 2 1095.42 1116.66 5.62 o 3 8 2 170.91 170.34 1.63 o 4 8 2 34.79 33.00 0.88 o 5 8 2 33.80 30.10 0.38 o 6 8 2 75.90 75.62 0.66 o 7 8 2 23.90 22.34 0.40 o 8 8 2 11.12 11.60 0.32 o 1 9 2 123.06 124.96 1.32 o 2 9 2 1.63 0.15 0.19 o 3 9 2 57.22 62.14 1.19 o 4 9 2 0.86 1.01 0.16 o 5 9 2 94.49 95.00 0.72 o 6 9 2 37.33 34.94 0.50 o 7 9 2 30.99 29.90 0.46 o 8 9 2 87.44 88.86 0.78 o 0 10 2 155.31 192.45 2.17 o 1 10 2 168.91 162.18 1.59 o 2 10 2 3.16 3.80 0.33 o 3 10 2 675.18 671.44 4.17 o 4 10 2 0.01 0.06 0.10 o 5 10 2 275.66 264.03 1.39 o 6 10 2 2.10 1.65 0.18 o 7 10 2 3.37 3.92 0.21 o 8 10 2 17.97 17.51 0.49 o 1 11 2 24.27 27.08 0.78 o 2 11 2 0.07 0.25 0.23 o 3 11 2 106.58 92.08 0.71 o 4 11 2 533.72 525.16 2.59 o 5 11 2 11.27 10.79 0.32 o 6 11 2 124.87 120.78 0.94 o 7 11 2 37.18 37.42 0.51 o 8 11 2 0.95 1.24 0.18 o 0 12 2 782.23 768.72 10.28 o 1 12 2 93.02 93.27 1.39 o 2 12 2 13.88 14.08 0.34 o 3 12 2 18.38 19.17 0.37 o 4 12 2 122.52 116.19 0.85 o 5 12 2 190.24 178.17 1.27 o 6 12 2 21.77 19.80 0.44 o 7 12 2 32.81 33.26 0.46 o 8 12 2 31.14 34.09 1.27 o 1 13 2 6.12 6.05 0.25 o 2 13 2 286.11 280.67 1.55 o 3 13 2 169.88 160.38 1.05 o 4 13 2 71.36 70.09 0.65 o 5 13 2 130.55 137.69 1.02 o 6 13 2 73.17 72.27 0.74 o 7 13 2 4.41 3.22 0.20 o 0 14 2 1141.60 1127.72 6.96 o 1 14 2 171.25 154.78 1.15 o 2 14 2 296.74 281.12 1.57 o 3 14 2 18.54 18.60 0.38 o 4 14 2 1.63 2.52 0.18 o 5 14 2 2.90 3.50 0.21 o 6 14 2 26.25 28.97 0.64 o 7 14 2 54.09 49.27 0.60 o 1 15 2 183.25 175.75 1.23 o 2 15 2 40.04 35.89 0.51 o 3 15 2 188.87 203.14 1.22 o 4 15 2 0.38 0.37 0.13 o 5 15 2 15.63 19.31 0.49 o 6 15 2 44.77 45.57 0.91 o 7 15 2 31.01 30.40 0.43 o 0 16 2 25.38 24.29 0.71 o 1 16 2 251.70 223.96 1.48 o 2 16 2 121.33 112.58 0.93 o 3 16 2 1.06 1.83 0.15 o 4 16 2 81.06 79.82 0.70 o 5 16 2 17.20 18.10 0.42 o 6 16 2 16.94 20.33 0.37 o 1 17 2 49.17 44.98 0.62 o 2 17 2 219.61 217.87 1.50 o 3 17 2 80.44 81.43 0.70 o 4 17 2 13.79 12.84 0.39 o 5 17 2 29.76 36.77 0.48 o 6 17 2 96.41 88.53 0.94 o 0 18 2 25.15 18.20 0.81 o 1 18 2 28.84 33.75 0.78 o 2 18 2 48.70 45.29 0.57 o 3 18 2 3.26 2.26 0.18 o 4 18 2 4.17 7.42 0.31 o 5 18 2 6.22 7.26 0.27 o 1 19 2 4.86 5.96 0.26 o 2 19 2 11.17 10.29 0.41 o 3 19 2 4.78 5.27 0.26 o 4 19 2 0.09 0.20 0.13 o 0 20 2 121.79 109.95 1.52 o 1 20 2 59.98 60.38 0.67 o 2 20 2 26.67 31.08 0.62 o 3 20 2 5.08 6.35 0.38 o 4 20 2 0.04 -0.14 0.14 o 1 21 2 0.97 1.51 0.21 o 2 21 2 46.42 55.06 0.75 o 3 21 2 2.88 2.50 0.29 o 0 22 2 0.40 1.24 0.29 o 1 22 2 12.29 10.26 0.87 o 1 0 3 170.49 182.87 2.16 o 2 0 3 286.34 285.65 3.29 o 3 0 3 10.04 13.07 0.68 o 4 0 3 6.41 5.35 0.53 o 5 0 3 17.56 20.55 0.60 o 6 0 3 571.67 576.23 3.58 o 7 0 3 382.49 382.13 2.65 o 8 0 3 432.48 445.00 3.75 o 9 0 3 168.04 141.25 3.34 o 0 1 3 0.11 0.04 0.24 o 1 1 3 107.63 130.25 1.25 o 2 1 3 98.42 102.16 1.08 o 3 1 3 0.75 0.69 0.21 o 4 1 3 94.79 97.59 1.28 o 5 1 3 310.18 309.14 1.46 o 6 1 3 390.34 382.69 1.84 o 7 1 3 270.42 257.63 1.40 o 8 1 3 20.51 20.32 0.56 o 1 2 3 31.43 27.09 0.66 o 2 2 3 19.31 19.27 0.61 o 3 2 3 251.84 259.87 2.28 o 4 2 3 0.25 0.88 0.26 o 5 2 3 299.26 283.13 1.37 o 6 2 3 234.29 248.88 1.27 o 7 2 3 71.74 67.48 0.62 o 8 2 3 152.03 158.96 1.14 o 0 3 3 1085.47 1097.92 7.95 o 1 3 3 252.57 267.29 1.96 o 2 3 3 25.35 31.40 0.73 o 3 3 3 0.92 1.51 0.25 o 4 3 3 103.86 94.71 1.36 o 5 3 3 163.15 168.11 1.00 o 6 3 3 29.52 26.46 0.41 o 7 3 3 156.95 158.64 1.02 o 8 3 3 12.25 10.62 0.33 o 1 4 3 90.68 112.02 1.16 o 2 4 3 166.61 171.82 1.48 o 3 4 3 9.80 6.80 0.39 o 4 4 3 146.45 132.98 1.84 o 5 4 3 160.14 160.50 1.01 o 6 4 3 69.69 77.61 0.67 o 7 4 3 0.13 0.00 0.12 o 8 4 3 2.83 2.82 0.17 o 0 5 3 884.14 898.86 6.95 o 1 5 3 1227.01 1310.42 6.37 o 2 5 3 25.24 30.97 0.84 o 3 5 3 236.06 228.57 2.08 o 4 5 3 10.50 12.74 0.31 o 5 5 3 14.81 17.30 0.35 o 6 5 3 31.42 31.05 0.47 o 7 5 3 21.91 22.01 0.38 o 8 5 3 15.81 14.93 0.35 o 1 6 3 23.58 16.69 0.56 o 2 6 3 9.52 8.81 0.43 o 3 6 3 0.20 0.37 0.23 o 4 6 3 138.63 129.31 0.89 o 5 6 3 16.75 15.55 0.35 o 6 6 3 6.98 9.66 0.28 o 7 6 3 15.16 14.14 0.35 o 8 6 3 2.31 2.40 0.18 o 0 7 3 727.33 716.45 8.27 o 1 7 3 0.29 0.96 0.53 o 2 7 3 214.90 213.26 2.29 o 3 7 3 54.39 50.94 1.11 o 4 7 3 89.96 82.38 0.63 o 5 7 3 1.29 0.88 0.14 o 6 7 3 43.17 38.35 0.47 o 7 7 3 50.99 49.10 0.55 o 8 7 3 24.78 21.32 0.37 o 1 8 3 43.69 46.68 0.92 o 2 8 3 14.12 14.24 0.64 o 3 8 3 153.90 157.71 1.06 o 4 8 3 29.01 22.64 0.37 o 5 8 3 123.60 129.33 0.91 o 6 8 3 13.67 12.18 0.31 o 7 8 3 0.22 0.41 0.14 o 8 8 3 21.39 20.40 0.34 o 0 9 3 158.99 138.34 2.32 o 1 9 3 159.77 149.10 1.58 o 2 9 3 242.16 237.81 2.28 o 3 9 3 1.61 0.88 0.14 o 4 9 3 189.86 186.68 1.09 o 5 9 3 49.89 46.77 0.51 o 6 9 3 32.93 32.50 0.50 o 7 9 3 38.83 37.46 0.53 o 8 9 3 13.77 9.65 0.25 o 1 10 3 26.20 27.12 0.70 o 2 10 3 217.26 212.10 1.33 o 3 10 3 5.04 4.44 0.22 o 4 10 3 10.56 7.51 0.25 o 5 10 3 15.79 18.71 0.37 o 6 10 3 1.07 0.46 0.14 o 7 10 3 0.27 0.76 0.13 o 0 11 3 103.98 102.64 1.21 o 1 11 3 677.16 652.56 2.95 o 2 11 3 95.20 98.35 0.84 o 3 11 3 425.77 394.20 2.04 o 4 11 3 175.84 162.43 1.11 o 5 11 3 18.25 20.74 0.43 o 6 11 3 0.17 0.59 0.15 o 7 11 3 2.10 2.07 0.18 o 1 12 3 122.61 110.30 0.90 o 2 12 3 553.66 515.28 2.62 o 3 12 3 31.65 41.70 0.52 o 4 12 3 7.57 6.60 0.26 o 5 12 3 8.03 5.92 0.23 o 6 12 3 0.71 1.91 0.17 o 7 12 3 45.30 44.86 0.59 o 0 13 3 182.57 186.65 1.82 o 1 13 3 52.09 53.49 0.63 o 2 13 3 21.39 20.43 0.46 o 3 13 3 85.58 88.90 1.19 o 4 13 3 111.99 101.59 0.82 o 5 13 3 1.04 2.81 0.18 o 6 13 3 17.79 21.85 0.42 o 7 13 3 8.65 6.96 0.27 o 1 14 3 59.26 62.04 0.81 o 2 14 3 217.24 227.32 1.56 o 3 14 3 255.69 275.25 1.59 o 4 14 3 58.69 64.17 0.83 o 5 14 3 162.19 165.11 1.10 o 6 14 3 1.35 2.12 0.17 o 0 15 3 1.53 3.31 0.38 o 1 15 3 12.78 11.14 0.37 o 2 15 3 9.68 10.26 0.34 o 3 15 3 187.17 178.10 1.18 o 4 15 3 6.24 6.27 0.25 o 5 15 3 32.55 32.25 0.63 o 6 15 3 8.90 11.67 0.29 o 1 16 3 55.57 55.08 0.78 o 2 16 3 20.33 20.41 0.47 o 3 16 3 0.32 0.68 0.16 o 4 16 3 283.22 297.77 1.86 o 5 16 3 88.27 88.78 0.77 o 0 17 3 17.21 15.09 0.80 o 1 17 3 88.34 95.18 1.21 o 2 17 3 31.96 38.26 0.58 o 3 17 3 0.15 0.20 0.12 o 4 17 3 1.24 2.53 0.26 o 5 17 3 0.74 0.53 0.13 o 1 18 3 25.28 32.29 0.66 o 2 18 3 4.76 3.89 0.24 o 3 18 3 55.96 63.59 0.68 o 4 18 3 100.49 111.23 2.44 o 0 19 3 21.57 21.47 0.66 o 1 19 3 0.57 0.48 0.15 o 2 19 3 5.42 2.93 0.27 o 3 19 3 92.37 106.93 1.13 o 1 20 3 20.44 18.83 0.38 o 2 20 3 5.28 4.73 0.26 o 0 21 3 25.03 30.11 0.74 o 0 0 4 17.99 16.38 1.48 o 1 0 4 14.42 12.85 0.77 o 2 0 4 178.76 169.18 2.62 o 3 0 4 111.70 114.11 1.16 o 4 0 4 182.66 176.05 1.55 o 5 0 4 30.38 32.66 0.69 o 6 0 4 33.92 30.82 0.74 o 7 0 4 17.47 19.77 0.57 o 8 0 4 232.81 220.87 2.07 o 1 1 4 2.01 1.68 0.27 o 2 1 4 0.73 1.51 0.29 o 3 1 4 251.73 233.77 1.30 o 4 1 4 244.20 250.06 1.38 o 5 1 4 142.01 139.85 0.97 o 6 1 4 26.58 27.64 0.49 o 7 1 4 36.26 37.49 0.48 o 8 1 4 14.36 10.68 0.28 o 0 2 4 78.91 83.58 1.92 o 1 2 4 2.42 2.85 0.33 o 2 2 4 91.24 86.47 1.22 o 3 2 4 116.14 113.65 0.82 o 4 2 4 3.48 2.34 0.18 o 5 2 4 111.01 104.22 0.78 o 6 2 4 18.95 19.73 0.42 o 7 2 4 5.11 6.02 0.26 o 8 2 4 13.88 13.13 0.35 o 1 3 4 327.77 320.55 2.53 o 2 3 4 207.35 203.54 1.57 o 3 3 4 314.35 292.14 1.59 o 4 3 4 134.20 132.01 0.90 o 5 3 4 0.22 0.02 0.14 o 6 3 4 26.37 25.42 0.42 o 7 3 4 9.40 10.32 0.28 o 8 3 4 0.88 0.43 0.17 o 0 4 4 4.95 7.73 0.67 o 1 4 4 81.20 69.61 1.09 o 2 4 4 142.83 136.89 0.98 o 3 4 4 650.94 675.58 3.24 o 4 4 4 78.09 82.55 0.73 o 5 4 4 89.64 84.54 0.87 o 6 4 4 0.82 0.84 0.14 o 7 4 4 0.21 0.35 0.14 o 8 4 4 4.69 3.42 0.32 o 1 5 4 55.99 57.50 1.12 o 2 5 4 20.81 19.99 0.41 o 3 5 4 42.35 41.85 0.60 o 4 5 4 129.15 110.82 1.29 o 5 5 4 17.47 14.28 0.37 o 6 5 4 1.37 1.71 0.17 o 7 5 4 12.45 12.71 0.42 o 0 6 4 84.02 87.74 1.25 o 1 6 4 106.34 103.26 0.96 o 2 6 4 319.39 301.05 1.73 o 3 6 4 0.33 2.01 0.16 o 4 6 4 62.56 64.19 0.77 o 5 6 4 4.95 3.95 0.23 o 6 6 4 79.09 71.40 0.66 o 7 6 4 2.67 3.06 0.17 o 1 7 4 0.31 0.37 0.15 o 2 7 4 52.51 53.18 0.58 o 3 7 4 40.59 44.47 0.50 o 4 7 4 14.01 8.81 0.30 o 5 7 4 152.88 144.98 1.00 o 6 7 4 0.04 0.01 0.13 o 7 7 4 47.90 39.15 0.50 o 0 8 4 24.42 21.14 0.64 o 1 8 4 0.49 0.42 0.13 o 2 8 4 51.38 40.85 0.54 o 3 8 4 9.00 7.50 0.29 o 4 8 4 53.28 50.72 0.57 o 5 8 4 62.07 58.16 0.59 o 6 8 4 18.88 23.27 0.45 o 7 8 4 36.99 38.97 0.51 o 1 9 4 23.85 23.55 0.50 o 2 9 4 1.34 2.79 0.20 o 3 9 4 17.48 21.30 0.46 o 4 9 4 11.93 14.20 0.36 o 5 9 4 15.61 13.80 0.36 o 6 9 4 0.13 0.03 0.13 o 7 9 4 101.00 98.92 1.05 o 0 10 4 731.95 720.19 4.65 o 1 10 4 232.26 227.19 1.42 o 2 10 4 143.04 128.12 1.00 o 3 10 4 84.32 90.52 0.91 o 4 10 4 10.42 9.09 0.32 o 5 10 4 2.63 3.20 0.22 o 6 10 4 16.63 16.49 0.46 o 7 10 4 10.36 12.38 1.14 o 1 11 4 40.96 34.07 0.50 o 2 11 4 146.07 145.54 1.15 o 3 11 4 7.50 6.94 0.29 o 4 11 4 0.12 -0.02 0.14 o 5 11 4 50.83 50.10 0.84 o 6 11 4 1.05 0.94 0.16 o 0 12 4 274.33 257.88 2.11 o 1 12 4 646.63 659.08 3.03 o 2 12 4 9.50 5.53 0.28 o 3 12 4 4.60 2.14 0.20 o 4 12 4 3.74 4.22 0.26 o 5 12 4 0.03 0.48 0.17 o 6 12 4 4.68 6.06 0.27 o 1 13 4 85.42 82.79 0.74 o 2 13 4 1.18 3.27 0.26 o 3 13 4 0.35 0.47 0.17 o 4 13 4 131.54 154.15 1.31 o 5 13 4 193.58 200.81 1.39 o 6 13 4 36.71 37.09 0.75 o 0 14 4 42.42 45.83 1.01 o 1 14 4 46.54 52.64 0.60 o 2 14 4 81.18 86.46 0.88 o 3 14 4 19.52 17.42 0.43 o 4 14 4 51.87 51.90 0.61 o 5 14 4 59.07 65.50 0.71 o 1 15 4 16.39 16.62 0.38 o 2 15 4 9.06 10.14 0.36 o 3 15 4 1.17 0.55 0.16 o 4 15 4 20.72 16.39 0.48 o 5 15 4 4.58 5.94 0.32 o 0 16 4 3.09 4.54 0.43 o 1 16 4 17.88 20.54 0.44 o 2 16 4 2.67 2.66 0.21 o 3 16 4 53.29 55.16 0.64 o 4 16 4 33.71 35.29 0.68 o 1 17 4 5.70 5.20 0.25 o 2 17 4 15.88 19.82 0.42 o 3 17 4 1.00 0.97 0.15 o 0 18 4 23.57 36.00 0.83 o 1 18 4 149.07 172.44 2.01 o 2 18 4 8.72 8.04 0.29 o 1 19 4 1.71 3.02 0.26 o 1 0 5 118.77 113.38 1.39 o 2 0 5 119.12 119.56 1.42 o 3 0 5 15.19 15.32 0.53 o 4 0 5 0.53 0.51 0.20 o 5 0 5 0.31 0.41 0.18 o 6 0 5 6.67 5.75 0.31 o 7 0 5 84.34 91.43 1.31 o 0 1 5 386.73 379.70 3.33 o 1 1 5 125.31 118.73 1.08 o 2 1 5 50.21 46.65 0.66 o 3 1 5 138.40 131.98 1.02 o 4 1 5 3.44 2.76 0.18 o 5 1 5 26.70 30.45 0.41 o 6 1 5 45.78 54.47 0.56 o 7 1 5 10.01 9.32 0.39 o 1 2 5 14.75 19.81 0.45 o 2 2 5 178.20 171.70 1.28 o 3 2 5 39.16 39.51 0.56 o 4 2 5 14.30 12.89 0.33 o 5 2 5 11.36 11.35 0.37 o 6 2 5 0.56 0.48 0.15 o 0 3 5 20.52 20.88 0.57 o 1 3 5 777.20 815.39 4.20 o 2 3 5 4.59 5.21 0.25 o 3 3 5 7.13 4.88 0.23 o 4 3 5 79.28 74.41 0.71 o 5 3 5 1.32 1.11 0.15 o 6 3 5 19.81 16.66 0.35 o 1 4 5 48.41 54.02 0.64 o 2 4 5 3.37 3.26 0.21 o 3 4 5 4.25 3.83 0.23 o 4 4 5 17.11 14.90 0.39 o 5 4 5 127.16 135.15 1.08 o 6 4 5 14.46 12.21 0.30 o 0 5 5 241.23 239.44 2.21 o 1 5 5 39.92 42.87 0.57 o 2 5 5 13.15 18.62 0.39 o 3 5 5 0.09 0.06 0.14 o 4 5 5 10.08 10.13 0.34 o 5 5 5 19.25 17.90 0.43 o 6 5 5 67.05 60.43 0.62 o 1 6 5 33.50 32.14 0.65 o 2 6 5 79.14 75.04 0.73 o 3 6 5 191.14 177.22 1.15 o 4 6 5 26.12 22.60 0.54 o 5 6 5 93.01 88.03 0.84 o 6 6 5 4.50 8.04 0.25 o 0 7 5 62.02 57.78 1.90 o 1 7 5 7.94 6.26 0.28 o 2 7 5 9.96 8.32 0.32 o 3 7 5 4.19 3.86 0.20 o 4 7 5 21.73 16.00 0.43 o 5 7 5 25.84 36.12 0.52 o 6 7 5 7.88 8.25 0.27 o 1 8 5 1.27 1.06 0.21 o 2 8 5 2.59 1.28 0.16 o 3 8 5 29.10 23.88 0.43 o 4 8 5 1.01 0.71 0.16 o 5 8 5 48.90 47.46 0.70 o 6 8 5 0.11 0.40 0.16 o 0 9 5 10.23 7.08 0.59 o 1 9 5 3.88 4.12 0.28 o 2 9 5 41.07 39.89 0.55 o 3 9 5 12.27 12.96 0.32 o 4 9 5 8.55 8.76 0.43 o 5 9 5 6.97 8.03 0.28 o 1 10 5 27.13 27.33 0.55 o 2 10 5 0.07 0.10 0.14 o 3 10 5 141.05 145.29 1.18 o 4 10 5 62.59 70.02 0.74 o 5 10 5 86.45 93.43 0.88 o 0 11 5 106.99 103.37 2.71 o 1 11 5 3.88 2.45 0.20 o 2 11 5 162.41 173.62 2.00 o 3 11 5 94.96 98.48 0.88 o 4 11 5 14.24 14.90 0.38 o 5 11 5 44.79 46.02 0.60 o 1 12 5 156.43 151.76 1.38 o 2 12 5 8.04 5.31 0.25 o 3 12 5 113.57 110.04 0.87 o 4 12 5 25.66 22.93 0.50 o 0 13 5 0.02 -0.25 0.39 o 1 13 5 23.59 30.24 0.56 o 2 13 5 0.27 0.11 0.14 o 3 13 5 200.00 212.02 1.60 o 4 13 5 36.17 34.05 0.59 o 1 14 5 12.28 9.43 0.35 o 2 14 5 0.24 0.01 0.17 o 3 14 5 9.96 12.84 0.33 o 0 15 5 19.86 18.08 0.98 o 1 15 5 37.93 36.11 0.69 o 2 15 5 40.66 45.47 1.38 o 1 16 5 1.07 1.18 0.20 o 0 0 6 7.83 5.54 0.50 o 1 0 6 288.23 282.24 2.76 o 2 0 6 84.67 84.74 1.35 o 3 0 6 0.13 0.33 0.23 o 4 0 6 82.31 98.37 1.22 o 5 0 6 37.08 43.64 0.73 o 1 1 6 29.33 28.93 0.57 o 2 1 6 60.26 64.74 0.83 o 3 1 6 1.08 2.17 0.19 o 4 1 6 0.07 0.14 0.13 o 5 1 6 22.83 29.42 0.72 o 0 2 6 199.80 220.23 2.31 o 1 2 6 212.40 210.68 1.64 o 2 2 6 1.75 2.14 0.21 o 3 2 6 50.95 54.75 0.66 o 4 2 6 55.38 61.80 0.71 o 5 2 6 4.75 4.71 0.25 o 1 3 6 9.48 10.77 0.35 o 2 3 6 159.05 170.20 1.30 o 3 3 6 0.90 1.43 0.16 o 4 3 6 27.02 27.74 0.47 o 5 3 6 1.13 0.71 0.23 o 0 4 6 85.14 93.14 1.37 o 1 4 6 22.34 20.56 0.39 o 2 4 6 53.26 50.76 0.69 o 3 4 6 68.38 75.33 0.87 o 4 4 6 1.03 0.71 0.13 o 5 4 6 6.80 6.71 0.40 o 1 5 6 37.55 36.50 0.73 o 2 5 6 27.65 25.80 0.53 o 3 5 6 32.66 38.42 0.55 o 4 5 6 14.39 14.60 0.38 o 0 6 6 232.27 217.25 2.13 o 1 6 6 0.28 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