#------------------------------------------------------------------------------ #$Date: 2023-01-04 15:35:06 +0200 (Wed, 04 Jan 2023) $ #$Revision: 280102 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519446.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519446 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.0529 _cell_length_b 18.8619 _cell_length_c 5.8033 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.8113 _cod_data_source_file 10-DBT_Pnma.fcf _cod_data_source_block jw23262 _shelx_title ' jw23262_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.83 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12956.96 13185.69 759.04 o 4 0 0 2.23 -4.23 13.77 o 6 0 0 43.47 37.76 16.36 o 8 0 0 94.93 78.51 8.73 o 2 1 0 4457.89 4394.43 160.85 o 4 1 0 831.02 850.73 58.94 o 6 1 0 280.94 237.88 31.63 o 8 1 0 7.27 4.50 3.14 o 0 2 0 7664.30 8205.28 667.97 o 2 2 0 1940.85 1961.51 81.55 o 4 2 0 28.27 28.75 11.82 o 6 2 0 77.55 54.53 18.54 o 8 2 0 71.10 72.24 8.18 o 2 3 0 4373.58 4264.10 175.31 o 4 3 0 516.08 540.65 56.31 o 6 3 0 394.02 318.62 50.23 o 8 3 0 150.78 152.14 14.59 o 0 4 0 184.11 200.69 23.92 o 2 4 0 615.26 542.22 27.85 o 4 4 0 71.29 60.44 11.26 o 6 4 0 1625.69 1524.51 73.10 o 8 4 0 299.06 319.13 27.95 o 2 5 0 256.91 248.33 29.80 o 4 5 0 40.99 35.34 9.60 o 6 5 0 423.09 403.36 17.67 o 8 5 0 273.58 286.55 25.36 o 0 6 0 4237.70 4400.20 259.87 o 2 6 0 1726.65 1762.56 85.45 o 4 6 0 67.61 44.16 15.20 o 6 6 0 522.99 474.82 20.28 o 8 6 0 184.80 159.29 15.95 o 2 7 0 1686.43 1662.99 101.15 o 4 7 0 1260.24 601.53 117.85 o 6 7 0 607.33 566.08 24.13 o 8 7 0 23.04 23.27 3.16 o 0 8 0 220.59 319.48 31.29 o 2 8 0 335.71 314.56 50.40 o 4 8 0 136.43 109.64 14.94 o 6 8 0 19.56 15.23 2.11 o 8 8 0 49.82 50.40 3.77 o 2 9 0 2952.00 3176.38 189.18 o 4 9 0 1046.95 761.70 151.64 o 6 9 0 240.03 232.00 9.99 o 8 9 0 29.69 33.25 3.31 o 0 10 0 5.21 51.38 11.01 o 2 10 0 2.32 8.54 11.96 o 4 10 0 15.99 21.54 11.50 o 6 10 0 309.53 287.94 12.08 o 8 10 0 416.05 392.13 19.15 o 2 11 0 87.61 117.60 16.03 o 4 11 0 903.35 954.58 37.56 o 6 11 0 112.40 106.79 5.13 o 8 11 0 5.11 6.41 1.77 o 0 12 0 1726.24 1759.19 133.25 o 2 12 0 19.16 36.43 13.31 o 4 12 0 15.60 20.23 2.60 o 6 12 0 39.41 38.99 2.99 o 8 12 0 197.93 177.16 12.88 o 2 13 0 233.44 234.12 24.59 o 4 13 0 1676.29 1844.65 68.45 o 6 13 0 83.70 83.29 4.43 o 8 13 0 242.23 210.56 10.39 o 0 14 0 882.44 920.64 104.49 o 2 14 0 544.51 485.55 22.27 o 4 14 0 565.77 595.15 23.73 o 6 14 0 285.77 281.49 11.17 o 2 15 0 674.02 647.56 37.46 o 4 15 0 164.34 170.76 8.24 o 6 15 0 0.57 0.30 1.75 o 0 16 0 343.70 356.57 22.83 o 2 16 0 948.94 928.53 45.30 o 4 16 0 387.46 372.83 19.22 o 6 16 0 101.21 102.93 6.15 o 2 17 0 351.75 321.59 20.96 o 4 17 0 16.31 15.02 2.28 o 6 17 0 13.52 13.92 1.71 o 0 18 0 11.69 20.49 4.11 o 2 18 0 49.07 54.49 5.12 o 4 18 0 0.69 2.78 1.63 o 6 18 0 50.50 48.26 3.07 o 2 19 0 216.59 211.79 12.15 o 4 19 0 367.08 341.27 13.34 o 0 20 0 142.53 165.10 11.74 o 2 20 0 40.39 56.48 4.78 o 4 20 0 1.69 0.74 2.11 o 2 21 0 12.38 19.95 2.97 o 4 21 0 38.83 28.46 3.01 o 0 22 0 334.83 368.61 32.72 o 2 22 0 147.51 149.47 8.29 o 1 0 1 3199.85 3426.14 115.16 o 2 0 1 10891.58 11755.25 553.84 o 3 0 1 5513.44 5958.30 200.44 o 4 0 1 2.74 -2.65 3.41 o 5 0 1 532.23 547.04 32.16 o 6 0 1 19.34 8.01 3.35 o 7 0 1 8.35 7.42 2.91 o 8 0 1 32.34 36.91 5.32 o 9 0 1 5.37 17.31 5.32 o 0 1 1 538.17 560.23 27.38 o 1 1 1 4763.65 5311.44 137.44 o 2 1 1 8540.50 9059.80 234.24 o 3 1 1 135.19 145.82 6.06 o 4 1 1 2170.75 2496.93 66.82 o 5 1 1 5.50 10.66 3.64 o 6 1 1 99.54 89.26 7.80 o 7 1 1 39.34 30.18 2.56 o 8 1 1 25.62 26.49 2.62 o 9 1 1 78.15 78.65 6.41 o 1 2 1 31.50 34.45 2.97 o 2 2 1 1605.62 1579.14 41.74 o 3 2 1 181.67 185.30 7.04 o 4 2 1 906.66 937.68 26.55 o 5 2 1 40.42 46.52 4.76 o 6 2 1 168.86 156.54 6.69 o 7 2 1 0.28 -1.19 1.19 o 8 2 1 3.79 5.75 2.51 o 9 2 1 0.66 12.82 3.95 o 0 3 1 2984.06 2917.85 106.28 o 1 3 1 1615.57 1614.91 47.98 o 2 3 1 11.59 15.46 2.86 o 3 3 1 138.59 136.34 8.01 o 4 3 1 186.95 192.08 11.82 o 5 3 1 7.97 2.18 4.90 o 6 3 1 13.23 12.34 1.67 o 7 3 1 13.44 13.13 1.66 o 8 3 1 242.65 262.96 10.53 o 9 3 1 55.24 56.95 5.25 o 1 4 1 64.62 63.60 4.00 o 2 4 1 17.65 10.65 2.47 o 3 4 1 326.16 346.48 15.17 o 4 4 1 2358.47 2420.13 92.47 o 5 4 1 99.13 94.85 9.05 o 6 4 1 381.01 374.76 13.48 o 7 4 1 11.32 9.74 1.60 o 8 4 1 23.65 19.91 2.00 o 9 4 1 18.19 13.95 2.18 o 0 5 1 1624.11 1668.74 81.13 o 1 5 1 22.96 20.33 3.79 o 2 5 1 25.31 12.60 2.74 o 3 5 1 227.46 229.87 16.05 o 4 5 1 75.44 85.18 8.82 o 5 5 1 300.13 348.04 21.24 o 6 5 1 61.34 54.93 3.54 o 7 5 1 54.67 50.17 2.98 o 8 5 1 330.95 351.90 13.81 o 9 5 1 0.63 -0.16 1.81 o 1 6 1 392.43 455.15 17.85 o 2 6 1 896.01 908.40 30.90 o 3 6 1 462.71 499.94 22.88 o 4 6 1 1289.51 1265.67 57.07 o 5 6 1 58.87 55.67 18.23 o 6 6 1 230.04 208.43 6.92 o 7 6 1 1.10 2.47 1.40 o 8 6 1 14.42 14.90 1.82 o 9 6 1 22.36 18.52 2.69 o 0 7 1 2846.01 2982.97 162.39 o 1 7 1 532.73 607.95 26.11 o 2 7 1 701.63 704.83 25.06 o 3 7 1 158.43 165.97 15.39 o 4 7 1 63.61 59.32 6.80 o 5 7 1 20.37 18.51 8.52 o 6 7 1 57.37 45.53 2.26 o 7 7 1 42.71 41.12 2.46 o 8 7 1 146.57 164.56 9.04 o 9 7 1 7.87 8.93 2.11 o 1 8 1 79.21 99.78 9.45 o 2 8 1 93.61 75.43 8.93 o 3 8 1 284.13 326.53 20.29 o 4 8 1 1061.33 977.34 56.23 o 5 8 1 10.29 11.40 1.33 o 6 8 1 328.06 322.29 9.63 o 7 8 1 7.00 7.15 1.37 o 8 8 1 20.30 18.29 1.82 o 9 8 1 2.54 1.56 1.64 o 0 9 1 1844.24 1920.96 84.05 o 1 9 1 1506.21 1777.23 69.16 o 2 9 1 67.17 57.79 5.40 o 3 9 1 78.25 77.09 6.50 o 4 9 1 153.22 148.53 20.64 o 5 9 1 21.32 21.36 1.63 o 6 9 1 117.90 110.76 4.42 o 7 9 1 9.41 9.11 1.40 o 8 9 1 127.35 143.53 5.85 o 9 9 1 0.90 2.14 1.54 o 1 10 1 9.37 23.47 5.68 o 2 10 1 131.91 117.61 12.62 o 3 10 1 1.49 -5.45 5.45 o 4 10 1 455.99 391.28 32.39 o 5 10 1 51.51 45.06 2.28 o 6 10 1 378.05 380.34 11.24 o 7 10 1 7.45 7.11 1.25 o 8 10 1 40.88 44.51 4.19 o 0 11 1 25.98 20.22 8.60 o 1 11 1 231.70 279.51 14.64 o 2 11 1 223.56 205.74 14.37 o 3 11 1 69.11 76.22 12.99 o 4 11 1 30.56 32.06 1.90 o 5 11 1 9.35 9.95 1.39 o 6 11 1 592.95 588.23 16.74 o 7 11 1 8.90 11.99 1.34 o 8 11 1 137.45 140.46 5.90 o 1 12 1 1.48 5.30 5.93 o 2 12 1 908.25 894.71 48.85 o 3 12 1 1.53 2.25 3.28 o 4 12 1 14.37 13.03 1.46 o 5 12 1 15.04 14.31 1.61 o 6 12 1 104.34 101.82 6.21 o 7 12 1 79.14 77.91 3.46 o 8 12 1 145.49 135.32 5.60 o 0 13 1 423.64 452.94 38.55 o 1 13 1 198.13 222.64 18.93 o 2 13 1 1220.00 1159.59 47.52 o 3 13 1 1.39 3.31 1.43 o 4 13 1 183.50 189.59 6.47 o 5 13 1 294.02 299.77 8.78 o 6 13 1 288.87 278.64 9.10 o 7 13 1 183.72 182.06 6.09 o 8 13 1 22.35 20.75 1.88 o 1 14 1 40.84 43.81 2.76 o 2 14 1 137.37 134.39 5.70 o 3 14 1 62.75 60.61 3.11 o 4 14 1 54.88 49.38 2.84 o 5 14 1 5.71 6.22 1.51 o 6 14 1 71.09 69.60 3.38 o 7 14 1 119.58 117.30 4.97 o 0 15 1 2122.52 2274.66 108.32 o 1 15 1 3.46 7.97 1.70 o 2 15 1 695.84 683.02 21.10 o 3 15 1 124.10 110.38 4.28 o 4 15 1 18.96 17.68 1.79 o 5 15 1 167.84 173.53 5.86 o 6 15 1 7.26 4.65 1.42 o 7 15 1 64.39 61.78 3.23 o 1 16 1 0.13 0.35 1.60 o 2 16 1 19.51 19.08 2.13 o 3 16 1 71.07 70.56 4.23 o 4 16 1 334.25 328.79 10.73 o 5 16 1 136.00 137.43 4.92 o 6 16 1 105.88 108.99 6.04 o 7 16 1 31.05 31.87 2.42 o 0 17 1 852.17 873.44 42.81 o 1 17 1 3.51 4.52 1.62 o 2 17 1 67.64 62.44 3.41 o 3 17 1 3.18 1.99 1.67 o 4 17 1 24.02 23.72 2.32 o 5 17 1 1.58 1.58 1.31 o 6 17 1 0.59 -0.08 1.09 o 1 18 1 0.02 1.19 1.65 o 2 18 1 41.24 42.33 2.98 o 3 18 1 0.35 -0.87 1.47 o 4 18 1 215.08 209.99 7.35 o 5 18 1 1.02 0.51 1.06 o 6 18 1 47.76 40.94 2.43 o 0 19 1 93.23 99.40 6.92 o 1 19 1 171.36 145.05 5.84 o 2 19 1 42.99 45.75 2.78 o 3 19 1 45.20 43.43 2.55 o 4 19 1 0.03 -0.42 1.20 o 5 19 1 10.41 9.59 1.20 o 1 20 1 1.29 2.43 1.90 o 2 20 1 107.43 109.37 5.53 o 3 20 1 0.84 0.64 1.67 o 4 20 1 95.25 101.21 4.22 o 0 21 1 145.24 169.28 9.60 o 1 21 1 1.14 0.82 1.68 o 2 21 1 82.69 91.47 4.76 o 3 21 1 1.29 -1.12 1.34 o 4 21 1 4.77 6.14 4.36 o 1 22 1 14.37 15.97 2.80 o 2 22 1 52.84 52.41 3.29 o 0 23 1 25.86 18.54 6.82 o 0 0 2 3660.41 3778.00 155.74 o 1 0 2 2.29 1.67 2.57 o 2 0 2 74.80 94.86 7.25 o 3 0 2 1880.93 2200.29 76.51 o 4 0 2 2.66 7.64 6.75 o 5 0 2 1419.76 1599.60 57.83 o 6 0 2 618.32 659.36 32.32 o 7 0 2 355.64 389.57 19.58 o 8 0 2 44.90 65.58 4.56 o 9 0 2 146.32 181.86 16.91 o 1 1 2 38.65 60.80 3.38 o 2 1 2 198.22 217.30 7.54 o 3 1 2 23.48 11.39 2.62 o 4 1 2 2976.03 3221.39 78.44 o 5 1 2 731.80 800.27 22.91 o 6 1 2 242.29 244.00 8.45 o 7 1 2 338.30 351.60 12.66 o 8 1 2 106.41 124.48 9.00 o 9 1 2 71.33 107.30 9.64 o 0 2 2 1970.41 2131.19 102.18 o 1 2 2 579.50 589.71 17.07 o 2 2 2 680.66 771.41 23.14 o 3 2 2 0.34 2.05 2.41 o 4 2 2 4.19 7.65 3.24 o 5 2 2 328.57 377.99 17.26 o 6 2 2 109.23 98.88 3.58 o 7 2 2 219.41 231.63 8.08 o 8 2 2 244.72 268.53 10.80 o 9 2 2 15.71 23.23 6.61 o 1 3 2 109.70 102.73 5.78 o 2 3 2 908.06 1017.44 31.24 o 3 3 2 54.86 36.22 3.77 o 4 3 2 16.80 19.84 3.88 o 5 3 2 30.11 18.42 6.29 o 6 3 2 38.19 36.38 1.97 o 7 3 2 150.86 168.65 6.85 o 8 3 2 56.44 70.95 6.19 o 9 3 2 22.31 19.55 2.44 o 0 4 2 245.99 336.04 16.30 o 1 4 2 2285.31 2380.14 69.74 o 2 4 2 407.25 436.71 18.01 o 3 4 2 991.64 1163.64 42.77 o 4 4 2 105.53 120.94 10.41 o 5 4 2 2.45 5.27 5.77 o 6 4 2 394.76 375.36 12.45 o 7 4 2 26.56 27.17 2.16 o 8 4 2 123.76 148.38 6.47 o 9 4 2 4.68 2.50 1.85 o 1 5 2 1.20 -0.35 2.55 o 2 5 2 2553.48 2770.29 87.46 o 3 5 2 48.19 29.82 5.33 o 4 5 2 790.37 818.53 32.84 o 5 5 2 95.27 79.80 4.09 o 6 5 2 197.28 184.86 6.76 o 7 5 2 34.10 31.46 2.07 o 8 5 2 5.07 5.15 1.41 o 9 5 2 3.17 3.67 1.40 o 0 6 2 374.82 337.36 17.02 o 1 6 2 1381.39 1552.53 50.13 o 2 6 2 502.62 521.57 20.38 o 3 6 2 46.86 55.83 6.58 o 4 6 2 91.21 112.32 11.72 o 5 6 2 1.11 0.08 1.33 o 6 6 2 17.25 14.90 1.56 o 7 6 2 11.73 12.39 1.48 o 8 6 2 8.86 10.96 1.46 o 9 6 2 28.26 32.37 3.03 o 1 7 2 2.73 2.26 3.32 o 2 7 2 215.05 201.61 15.12 o 3 7 2 179.65 172.96 15.04 o 4 7 2 158.05 142.41 17.16 o 5 7 2 134.12 129.89 4.48 o 6 7 2 157.38 149.97 5.45 o 7 7 2 0.21 -0.22 1.14 o 8 7 2 10.06 12.14 1.78 o 9 7 2 21.22 21.40 3.95 o 0 8 2 2061.77 2337.10 141.26 o 1 8 2 289.80 288.88 24.59 o 2 8 2 1576.21 1673.42 54.89 o 3 8 2 172.05 163.13 18.30 o 4 8 2 19.26 13.17 8.85 o 5 8 2 22.51 20.81 1.59 o 6 8 2 291.56 284.61 9.22 o 7 8 2 33.30 35.10 2.19 o 8 8 2 98.20 113.71 8.00 o 1 9 2 196.49 191.82 14.30 o 2 9 2 175.69 140.44 13.45 o 3 9 2 350.16 340.57 31.51 o 4 9 2 40.53 32.46 2.25 o 5 9 2 4.30 1.79 1.09 o 6 9 2 67.02 64.03 3.05 o 7 9 2 3.99 3.26 1.29 o 8 9 2 49.67 53.53 3.06 o 0 10 2 286.15 355.08 36.74 o 1 10 2 486.36 505.08 25.78 o 2 10 2 94.59 91.91 14.97 o 3 10 2 767.81 782.95 48.73 o 4 10 2 0.06 0.75 1.16 o 5 10 2 190.92 181.80 6.36 o 6 10 2 70.02 69.16 2.97 o 7 10 2 0.53 -1.08 1.08 o 8 10 2 74.10 79.69 3.54 o 1 11 2 84.87 87.56 11.76 o 2 11 2 63.63 50.70 9.04 o 3 11 2 289.83 279.93 9.61 o 4 11 2 836.11 820.17 24.36 o 5 11 2 96.77 94.68 4.29 o 6 11 2 194.59 186.56 6.07 o 7 11 2 4.37 2.83 1.03 o 8 11 2 2.46 3.16 1.43 o 0 12 2 1686.77 1592.70 140.07 o 1 12 2 146.72 145.65 13.24 o 2 12 2 25.76 24.53 2.68 o 3 12 2 22.80 24.86 1.89 o 4 12 2 149.61 152.68 5.29 o 5 12 2 53.06 47.27 2.56 o 6 12 2 0.64 2.01 1.28 o 7 12 2 2.36 2.32 1.29 o 8 12 2 79.00 80.82 4.67 o 1 13 2 41.17 35.96 2.36 o 2 13 2 151.39 160.27 6.33 o 3 13 2 410.46 420.53 12.28 o 4 13 2 241.64 229.72 7.38 o 5 13 2 315.52 314.32 10.21 o 6 13 2 137.50 137.06 5.02 o 7 13 2 0.72 2.07 1.29 o 0 14 2 1628.41 1677.55 79.80 o 1 14 2 154.49 146.75 5.55 o 2 14 2 397.26 384.70 12.20 o 3 14 2 62.41 60.21 3.15 o 4 14 2 13.13 16.42 1.66 o 5 14 2 33.20 35.43 2.17 o 6 14 2 79.89 84.58 3.46 o 7 14 2 84.20 82.56 3.03 o 1 15 2 183.86 184.69 6.75 o 2 15 2 158.96 148.96 5.66 o 3 15 2 346.34 351.19 12.24 o 4 15 2 54.38 55.07 2.73 o 5 15 2 96.03 95.28 3.86 o 6 15 2 49.29 52.96 2.45 o 7 15 2 26.01 31.25 6.34 o 0 16 2 4.13 6.75 2.30 o 1 16 2 48.15 47.64 2.82 o 2 16 2 133.47 120.84 5.33 o 3 16 2 6.90 7.37 1.93 o 4 16 2 61.56 53.71 3.04 o 5 16 2 20.28 20.41 2.02 o 6 16 2 85.60 88.40 5.90 o 1 17 2 60.21 53.67 3.17 o 2 17 2 375.11 365.10 12.16 o 3 17 2 129.34 129.29 8.55 o 4 17 2 60.97 62.34 3.45 o 5 17 2 48.68 56.50 3.87 o 6 17 2 62.77 62.76 3.34 o 0 18 2 108.64 96.78 6.15 o 1 18 2 132.09 138.67 5.90 o 2 18 2 109.93 103.43 4.06 o 3 18 2 36.95 29.62 2.31 o 4 18 2 4.05 6.50 1.59 o 5 18 2 9.06 8.75 1.43 o 1 19 2 0.20 0.39 1.42 o 2 19 2 0.94 0.56 1.43 o 3 19 2 37.71 40.46 2.49 o 4 19 2 12.66 15.23 1.48 o 0 20 2 217.21 213.73 13.89 o 1 20 2 94.46 95.92 6.49 o 2 20 2 72.59 77.70 5.89 o 3 20 2 11.09 10.98 1.67 o 4 20 2 0.13 -0.08 1.38 o 1 21 2 4.07 3.83 1.51 o 2 21 2 94.44 116.51 9.75 o 3 21 2 12.89 11.01 2.10 o 0 22 2 15.60 12.87 2.98 o 1 22 2 45.32 45.73 4.12 o 1 0 3 222.89 322.46 28.87 o 2 0 3 714.37 804.08 30.84 o 3 0 3 240.86 248.05 13.87 o 4 0 3 7.19 5.32 5.82 o 5 0 3 25.74 22.69 2.17 o 6 0 3 313.66 342.29 18.51 o 7 0 3 295.21 358.26 21.23 o 8 0 3 517.48 490.26 24.12 o 9 0 3 104.06 174.09 17.18 o 0 1 3 11.81 18.23 4.23 o 1 1 3 39.06 24.97 4.18 o 2 1 3 240.95 239.07 9.85 o 3 1 3 10.33 11.86 3.83 o 4 1 3 101.46 114.61 8.17 o 5 1 3 357.30 355.15 9.84 o 6 1 3 1068.09 1071.36 28.19 o 7 1 3 569.04 571.28 18.41 o 8 1 3 62.77 85.21 11.25 o 9 1 3 109.99 167.68 17.18 o 1 2 3 162.15 200.40 9.11 o 2 2 3 11.17 7.34 3.66 o 3 2 3 967.37 937.49 28.14 o 4 2 3 59.52 55.04 6.81 o 5 2 3 674.46 649.61 16.54 o 6 2 3 231.69 248.60 7.08 o 7 2 3 72.57 84.97 5.28 o 8 2 3 125.72 120.48 5.43 o 0 3 3 2076.03 2384.47 115.06 o 1 3 3 893.06 917.45 27.47 o 2 3 3 125.21 141.61 7.29 o 3 3 3 60.79 54.00 5.16 o 4 3 3 141.46 136.57 10.13 o 5 3 3 94.31 88.16 3.02 o 6 3 3 78.26 71.23 2.75 o 7 3 3 29.49 24.61 1.50 o 8 3 3 49.61 52.41 3.25 o 1 4 3 1.52 3.72 3.02 o 2 4 3 115.44 141.92 8.49 o 3 4 3 227.74 197.40 9.19 o 4 4 3 323.56 272.66 14.30 o 5 4 3 416.94 397.32 11.53 o 6 4 3 130.70 142.86 4.78 o 7 4 3 9.22 11.89 1.19 o 8 4 3 1.91 2.62 1.55 o 0 5 3 2183.88 2383.39 114.42 o 1 5 3 2415.82 2625.42 69.88 o 2 5 3 303.87 310.86 15.72 o 3 5 3 467.82 408.57 17.60 o 4 5 3 13.21 14.53 1.70 o 5 5 3 4.29 3.67 1.12 o 6 5 3 0.35 1.39 0.96 o 7 5 3 124.53 130.66 5.00 o 8 5 3 47.78 53.63 4.40 o 1 6 3 126.08 112.49 6.05 o 2 6 3 9.75 1.34 5.01 o 3 6 3 131.52 126.18 10.01 o 4 6 3 224.73 206.15 6.06 o 5 6 3 30.55 25.88 1.60 o 6 6 3 29.79 28.03 1.78 o 7 6 3 49.97 47.25 2.59 o 8 6 3 10.19 9.14 1.19 o 0 7 3 1029.76 1003.37 44.28 o 1 7 3 85.24 82.77 7.70 o 2 7 3 371.27 357.49 18.56 o 3 7 3 125.34 116.68 18.65 o 4 7 3 47.76 40.27 2.00 o 5 7 3 30.42 29.77 1.92 o 6 7 3 1.98 2.56 1.04 o 7 7 3 141.80 152.16 5.62 o 8 7 3 44.16 44.74 2.68 o 1 8 3 178.42 178.30 13.08 o 2 8 3 98.79 98.84 9.60 o 3 8 3 596.25 553.56 31.61 o 4 8 3 256.65 225.64 6.69 o 5 8 3 413.94 383.10 11.28 o 6 8 3 4.85 5.98 1.21 o 7 8 3 13.10 14.35 1.41 o 8 8 3 49.71 40.25 2.58 o 0 9 3 441.05 308.23 69.18 o 1 9 3 632.32 569.07 51.97 o 2 9 3 239.30 232.48 15.56 o 3 9 3 42.81 34.89 2.17 o 4 9 3 90.60 89.29 4.16 o 5 9 3 11.25 10.60 1.30 o 6 9 3 23.95 18.79 1.58 o 7 9 3 1.39 0.18 1.02 o 8 9 3 13.74 13.34 1.20 o 1 10 3 4.34 1.42 9.43 o 2 10 3 285.44 260.06 8.43 o 3 10 3 46.03 50.64 3.07 o 4 10 3 151.33 136.60 5.07 o 5 10 3 155.34 163.90 5.44 o 6 10 3 7.20 7.97 1.34 o 7 10 3 7.32 6.92 1.11 o 0 11 3 1.74 0.39 4.85 o 1 11 3 1374.42 1312.15 43.96 o 2 11 3 201.73 197.13 6.67 o 3 11 3 425.10 412.42 12.28 o 4 11 3 153.18 156.04 5.10 o 5 11 3 0.39 -0.29 1.81 o 6 11 3 13.25 14.84 1.41 o 7 11 3 45.79 44.28 2.32 o 1 12 3 152.67 150.63 6.01 o 2 12 3 922.20 896.86 26.68 o 3 12 3 208.88 222.10 6.73 o 4 12 3 76.29 79.52 3.17 o 5 12 3 34.33 39.75 2.28 o 6 12 3 5.96 8.14 1.27 o 7 12 3 59.87 58.12 2.69 o 0 13 3 222.96 226.37 16.76 o 1 13 3 3.17 5.83 1.69 o 2 13 3 23.18 18.69 2.07 o 3 13 3 60.68 63.92 2.93 o 4 13 3 82.84 82.75 3.94 o 5 13 3 14.39 11.60 1.46 o 6 13 3 73.61 73.82 3.29 o 7 13 3 76.36 65.55 3.35 o 1 14 3 116.95 121.51 5.55 o 2 14 3 463.51 477.68 16.58 o 3 14 3 456.76 478.71 14.01 o 4 14 3 213.53 218.90 7.39 o 5 14 3 275.44 268.73 9.44 o 6 14 3 26.45 28.45 1.78 o 0 15 3 0.74 1.25 2.25 o 1 15 3 24.45 21.09 2.02 o 2 15 3 14.75 21.34 1.98 o 3 15 3 83.71 87.91 4.64 o 4 15 3 8.23 9.22 1.58 o 5 15 3 93.56 91.70 3.85 o 6 15 3 1.42 1.98 1.02 o 1 16 3 19.00 19.15 2.05 o 2 16 3 21.12 23.12 2.12 o 3 16 3 19.51 21.81 2.07 o 4 16 3 353.26 337.83 14.76 o 5 16 3 137.82 125.94 7.42 o 0 17 3 122.80 125.14 8.72 o 1 17 3 336.26 325.08 11.46 o 2 17 3 2.73 2.47 1.55 o 3 17 3 19.57 27.26 2.05 o 4 17 3 12.35 13.53 2.06 o 5 17 3 3.65 3.29 1.67 o 1 18 3 47.27 55.59 3.04 o 2 18 3 20.00 17.47 1.83 o 3 18 3 139.15 141.17 5.94 o 4 18 3 147.05 137.42 6.39 o 0 19 3 63.62 65.20 9.06 o 1 19 3 35.74 37.48 2.86 o 2 19 3 25.41 25.50 3.76 o 3 19 3 113.45 118.25 6.52 o 1 20 3 32.69 34.20 3.05 o 2 20 3 25.28 14.32 3.14 o 0 21 3 83.51 103.19 9.82 o 0 0 4 119.99 107.69 17.18 o 1 0 4 321.47 356.53 23.69 o 2 0 4 276.32 312.05 25.06 o 3 0 4 12.56 18.61 3.56 o 4 0 4 564.44 537.36 22.71 o 5 0 4 5.62 6.99 1.53 o 6 0 4 74.25 77.79 4.90 o 7 0 4 19.72 28.76 2.66 o 8 0 4 302.33 255.71 15.50 o 1 1 4 88.52 94.00 7.37 o 2 1 4 0.80 -2.20 4.68 o 3 1 4 901.87 791.47 22.01 o 4 1 4 443.14 403.38 12.24 o 5 1 4 628.35 598.37 16.00 o 6 1 4 60.65 67.33 2.52 o 7 1 4 2.28 3.77 0.83 o 8 1 4 4.91 7.13 1.30 o 0 2 4 103.82 134.77 12.24 o 1 2 4 296.92 281.60 18.35 o 2 2 4 88.78 101.59 8.11 o 3 2 4 328.21 270.36 7.88 o 4 2 4 6.51 7.60 1.18 o 5 2 4 34.49 35.97 2.12 o 6 2 4 6.45 5.02 0.95 o 7 2 4 56.83 67.48 2.47 o 8 2 4 24.69 22.85 2.08 o 1 3 4 526.51 498.00 29.38 o 2 3 4 560.61 569.82 21.36 o 3 3 4 869.19 770.46 21.45 o 4 3 4 223.75 208.28 6.34 o 5 3 4 97.36 88.27 2.98 o 6 3 4 13.63 15.74 1.15 o 7 3 4 26.40 27.43 1.57 o 8 3 4 7.63 6.22 1.21 o 0 4 4 24.94 24.52 7.09 o 1 4 4 499.71 434.77 20.21 o 2 4 4 321.84 310.38 9.31 o 3 4 4 779.69 732.90 23.08 o 4 4 4 184.64 183.08 6.00 o 5 4 4 27.81 21.62 1.37 o 6 4 4 7.34 8.51 1.00 o 7 4 4 59.11 64.89 2.57 o 8 4 4 0.36 -0.58 2.11 o 1 5 4 163.41 164.93 10.90 o 2 5 4 57.89 61.68 3.47 o 3 5 4 535.83 496.79 13.38 o 4 5 4 65.94 58.75 2.58 o 5 5 4 313.56 286.71 8.10 o 6 5 4 5.84 4.10 0.94 o 7 5 4 35.11 33.83 2.07 o 0 6 4 225.31 206.16 10.22 o 1 6 4 420.81 361.45 11.23 o 2 6 4 355.61 346.81 10.63 o 3 6 4 1.21 2.38 1.52 o 4 6 4 38.57 40.70 1.94 o 5 6 4 33.82 27.96 1.58 o 6 6 4 115.03 104.93 3.44 o 7 6 4 58.13 63.25 2.84 o 1 7 4 11.42 9.09 1.56 o 2 7 4 118.58 118.42 4.68 o 3 7 4 333.09 330.97 10.28 o 4 7 4 5.58 7.00 1.13 o 5 7 4 489.50 478.83 13.62 o 6 7 4 1.07 3.29 0.87 o 7 7 4 78.95 69.18 2.80 o 0 8 4 10.23 9.70 2.30 o 1 8 4 249.55 231.05 7.90 o 2 8 4 48.53 37.69 2.25 o 3 8 4 6.66 3.72 1.27 o 4 8 4 38.88 36.86 1.88 o 5 8 4 143.57 128.96 4.17 o 6 8 4 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14 4 121.74 128.83 5.18 o 3 14 4 0.55 -0.22 1.82 o 4 14 4 148.07 144.37 6.08 o 5 14 4 103.76 106.72 5.83 o 1 15 4 40.71 41.38 2.37 o 2 15 4 18.06 19.70 1.79 o 3 15 4 55.02 54.97 2.97 o 4 15 4 17.11 13.96 1.58 o 0 16 4 0.14 -0.53 1.66 o 1 16 4 155.51 180.42 7.31 o 2 16 4 14.57 14.55 1.96 o 3 16 4 131.10 141.87 13.84 o 4 16 4 27.77 32.86 4.09 o 1 17 4 30.34 29.40 1.96 o 2 17 4 28.17 31.74 1.95 o 3 17 4 45.29 55.33 3.47 o 0 18 4 0.31 1.93 1.63 o 1 18 4 344.11 371.81 15.61 o 2 18 4 34.81 35.26 2.68 o 1 19 4 0.09 -1.55 2.25 o 1 0 5 299.22 276.89 14.19 o 2 0 5 318.30 285.69 12.59 o 3 0 5 327.74 304.44 13.30 o 4 0 5 0.86 0.08 1.22 o 5 0 5 58.51 76.93 4.15 o 6 0 5 0.29 7.78 6.67 o 7 0 5 119.26 141.07 8.66 o 0 1 5 690.39 675.00 28.29 o 1 1 5 926.75 827.78 28.26 o 2 1 5 93.31 83.94 3.38 o 3 1 5 438.51 389.13 11.80 o 4 1 5 5.50 4.79 0.99 o 5 1 5 39.95 42.00 2.03 o 6 1 5 96.36 97.10 3.32 o 7 1 5 116.31 125.60 6.44 o 1 2 5 1.88 2.98 1.12 o 2 2 5 112.52 115.77 4.21 o 3 2 5 9.15 9.75 1.20 o 4 2 5 3.94 5.00 0.95 o 5 2 5 135.10 150.40 5.19 o 6 2 5 0.68 2.39 0.84 o 7 2 5 76.73 78.49 5.16 o 0 3 5 15.58 22.88 8.11 o 1 3 5 2060.11 1868.87 58.02 o 2 3 5 16.20 18.53 1.43 o 3 3 5 32.01 29.79 1.65 o 4 3 5 36.88 34.17 1.74 o 5 3 5 82.51 84.87 3.29 o 6 3 5 27.27 25.59 1.35 o 1 4 5 3.64 5.44 1.29 o 2 4 5 3.92 5.93 1.15 o 3 4 5 152.16 140.20 4.76 o 4 4 5 27.05 28.10 1.60 o 5 4 5 442.05 444.91 13.18 o 6 4 5 6.79 4.83 0.84 o 0 5 5 187.51 191.94 13.49 o 1 5 5 213.80 191.26 7.40 o 2 5 5 1.50 2.90 1.18 o 3 5 5 15.56 12.23 1.29 o 4 5 5 0.67 2.19 0.93 o 5 5 5 9.43 10.12 1.11 o 6 5 5 90.76 82.12 3.29 o 1 6 5 213.13 211.33 7.92 o 2 6 5 33.86 32.81 2.11 o 3 6 5 688.36 656.30 19.48 o 4 6 5 51.05 46.61 2.09 o 5 6 5 296.52 293.04 8.85 o 6 6 5 0.29 0.66 0.93 o 0 7 5 15.06 13.60 2.11 o 1 7 5 83.78 88.38 3.80 o 2 7 5 36.62 32.30 2.53 o 3 7 5 21.79 25.85 1.74 o 4 7 5 65.49 54.54 2.81 o 5 7 5 100.54 120.81 4.52 o 6 7 5 0.02 -0.34 0.88 o 1 8 5 28.90 28.26 2.01 o 2 8 5 13.29 11.59 1.49 o 3 8 5 209.41 200.79 6.41 o 4 8 5 0.04 0.79 0.87 o 5 8 5 223.25 226.53 8.00 o 6 8 5 0.08 -0.84 0.84 o 0 9 5 33.76 33.57 2.73 o 1 9 5 211.60 206.44 7.22 o 2 9 5 29.84 26.31 1.93 o 3 9 5 3.37 3.76 1.39 o 4 9 5 0.40 1.35 0.98 o 5 9 5 33.45 36.91 2.21 o 1 10 5 62.34 61.45 2.96 o 2 10 5 0.76 1.54 1.29 o 3 10 5 530.38 554.05 18.87 o 4 10 5 35.93 35.94 2.14 o 5 10 5 396.00 421.69 15.64 o 0 11 5 35.88 37.43 3.33 o 1 11 5 33.12 41.87 2.11 o 2 11 5 131.08 146.52 5.29 o 3 11 5 101.89 113.80 4.56 o 4 11 5 35.62 39.41 2.38 o 5 11 5 26.57 27.67 1.66 o 1 12 5 273.16 277.08 8.53 o 2 12 5 5.41 8.17 1.29 o 3 12 5 441.33 450.40 16.91 o 4 12 5 36.97 41.14 2.36 o 0 13 5 20.97 22.05 2.43 o 1 13 5 196.56 217.73 6.78 o 2 13 5 0.18 -0.79 1.09 o 3 13 5 358.29 359.43 13.55 o 4 13 5 25.56 24.83 1.60 o 1 14 5 55.06 53.32 2.36 o 2 14 5 0.36 1.18 1.28 o 3 14 5 111.62 123.91 4.99 o 0 15 5 18.08 16.30 1.92 o 1 15 5 227.23 240.47 10.34 o 2 15 5 49.46 54.42 2.90 o 3 15 5 40.77 42.37 3.27 o 1 16 5 7.83 8.32 1.28 o 0 0 6 4.81 4.67 2.07 o 1 0 6 1347.44 1233.06 71.86 o 2 0 6 162.67 174.19 15.06 o 3 0 6 73.46 77.37 4.24 o 4 0 6 160.74 164.42 7.46 o 5 0 6 23.42 32.33 8.49 o 1 1 6 0.42 4.44 1.76 o 2 1 6 202.01 183.41 7.57 o 3 1 6 124.08 128.16 4.66 o 4 1 6 13.44 15.34 1.46 o 5 1 6 181.27 198.74 6.85 o 0 2 6 247.30 257.85 16.05 o 1 2 6 525.79 521.09 21.98 o 2 2 6 3.80 4.16 1.26 o 3 2 6 182.36 170.73 5.91 o 4 2 6 71.06 75.02 3.01 o 5 2 6 0.30 4.20 1.40 o 1 3 6 151.82 155.32 6.70 o 2 3 6 264.24 260.20 10.09 o 3 3 6 259.27 243.70 8.69 o 4 3 6 167.79 167.87 6.48 o 5 3 6 44.44 49.80 2.35 o 0 4 6 16.07 17.61 2.79 o 1 4 6 109.41 122.38 6.15 o 2 4 6 35.37 35.59 2.32 o 3 4 6 109.05 109.60 4.70 o 4 4 6 2.59 2.95 1.03 o 5 4 6 48.62 50.45 2.54 o 1 5 6 70.16 70.36 3.61 o 2 5 6 35.53 35.43 2.06 o 3 5 6 214.19 223.32 7.91 o 4 5 6 40.41 44.43 2.08 o 0 6 6 561.70 613.14 36.34 o 1 6 6 208.36 205.38 8.20 o 2 6 6 52.82 55.33 2.71 o 3 6 6 0.63 0.97 1.00 o 4 6 6 0.06 0.62 0.87 o 1 7 6 23.88 23.56 2.43 o 2 7 6 18.10 14.88 1.38 o 3 7 6 207.76 227.11 8.75 o 4 7 6 47.06 54.97 2.55 o 0 8 6 122.80 131.52 7.41 o 1 8 6 72.21 76.74 3.36 o 2 8 6 62.77 58.04 2.67 o 3 8 6 9.23 5.00 1.01 o 4 8 6 41.01 41.92 3.08 o 1 9 6 108.64 116.88 4.55 o 2 9 6 8.22 8.00 1.12 o 3 9 6 253.65 272.60 10.23 o 0 10 6 21.32 25.10 2.89 o 1 10 6 38.48 48.93 3.49 o 2 10 6 36.46 37.71 1.88 o 3 10 6 12.27 13.92 1.42 o 1 11 6 14.73 18.51 1.47 o 2 11 6 10.58 11.41 1.10 o 0 12 6 21.37 17.25 2.17 o 1 12 6 286.84 299.91 14.56 o