#------------------------------------------------------------------------------ #$Date: 2023-11-01 20:34:29 +0200 (Wed, 01 Nov 2023) $ #$Revision: 287197 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519448.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519448 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.7562 _cell_length_b 6.3270 _cell_length_c 7.1050 _exptl_crystal_F_000 268.00 _reflns_d_resolution_high 0.8201 _cod_data_source_file S01_Pq-Cl2_Anhydre_Pnnm.fcf _cod_data_source_block jw25587 _shelx_title ' jw25587_a.res in Pnnm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 59.49 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 785.73 762.32 12.94 o 6 0 0 96.09 80.53 2.98 o 8 0 0 670.57 636.82 21.08 o 10 0 0 217.83 203.86 5.83 o 12 0 0 700.97 643.31 21.39 o 14 0 0 38.96 39.66 2.19 o 16 0 0 52.33 48.34 1.82 o 1 1 0 57.02 46.94 1.02 o 2 1 0 86.22 122.98 2.99 o 3 1 0 3260.00 3114.85 123.79 o 5 1 0 344.88 339.37 6.50 o 6 1 0 1043.55 1026.02 31.74 o 7 1 0 173.26 174.28 3.71 o 8 1 0 29.45 26.90 0.57 o 9 1 0 121.86 124.54 3.05 o 10 1 0 101.13 97.70 1.94 o 11 1 0 0.53 0.85 0.10 o 12 1 0 28.47 27.22 0.67 o 13 1 0 0.43 0.58 0.16 o 14 1 0 50.60 52.05 1.35 o 15 1 0 19.53 16.52 0.64 o 16 1 0 78.43 79.02 1.99 o 0 2 0 3380.89 3280.85 125.72 o 1 2 0 53.55 56.70 1.11 o 2 2 0 1.40 1.99 0.09 o 3 2 0 298.25 278.64 5.34 o 4 2 0 523.23 450.02 44.01 o 5 2 0 1774.96 1868.13 52.22 o 6 2 0 6.37 8.31 0.24 o 7 2 0 1297.81 1245.26 121.93 o 8 2 0 9.82 8.69 0.26 o 9 2 0 72.23 79.32 1.51 o 10 2 0 71.70 73.78 1.41 o 11 2 0 22.03 24.02 0.62 o 12 2 0 109.05 116.32 2.54 o 13 2 0 3.94 4.41 0.22 o 14 2 0 32.75 34.87 0.97 o 15 2 0 5.47 4.58 0.37 o 16 2 0 46.21 46.20 1.79 o 1 3 0 583.68 658.34 17.01 o 2 3 0 3538.85 3403.12 116.64 o 3 3 0 71.33 89.68 1.95 o 4 3 0 55.31 58.85 1.10 o 5 3 0 146.88 163.65 2.98 o 6 3 0 1290.33 1248.64 41.33 o 7 3 0 41.02 42.87 0.79 o 8 3 0 139.96 139.37 2.55 o 9 3 0 66.41 63.14 1.21 o 10 3 0 562.48 533.87 9.57 o 11 3 0 179.41 165.42 2.86 o 12 3 0 7.20 8.56 0.31 o 13 3 0 14.35 14.93 0.48 o 14 3 0 19.12 19.38 1.31 o 15 3 0 11.82 10.46 0.61 o 0 4 0 105.91 90.61 2.19 o 1 4 0 77.84 96.30 1.77 o 2 4 0 61.18 61.23 1.07 o 3 4 0 16.16 15.97 0.39 o 4 4 0 482.33 510.84 10.76 o 5 4 0 70.99 69.99 1.42 o 6 4 0 165.89 164.67 2.99 o 7 4 0 59.75 60.28 1.17 o 8 4 0 182.74 188.79 4.13 o 9 4 0 105.61 105.74 2.02 o 10 4 0 255.91 240.48 5.15 o 11 4 0 48.32 40.79 0.93 o 12 4 0 22.35 25.90 0.76 o 13 4 0 9.05 5.25 0.31 o 14 4 0 121.93 107.69 3.14 o 1 5 0 172.53 178.27 3.01 o 2 5 0 328.71 344.65 6.17 o 3 5 0 38.08 47.77 0.94 o 4 5 0 19.53 22.88 0.49 o 5 5 0 314.11 323.13 5.80 o 6 5 0 289.21 286.65 7.34 o 7 5 0 1.11 0.17 0.11 o 8 5 0 10.66 14.27 0.44 o 9 5 0 15.45 17.94 0.51 o 10 5 0 44.12 43.35 1.11 o 11 5 0 10.12 11.21 0.63 o 12 5 0 32.99 38.03 1.05 o 0 6 0 72.95 72.82 1.94 o 1 6 0 34.80 36.79 0.88 o 2 6 0 7.16 6.32 0.24 o 3 6 0 0.26 0.31 0.10 o 4 6 0 73.48 82.84 1.62 o 5 6 0 120.44 112.62 2.16 o 6 6 0 33.83 34.82 0.93 o 7 6 0 3.59 5.03 0.28 o 8 6 0 149.93 148.70 3.33 o 9 6 0 84.08 76.43 1.74 o 10 6 0 32.10 31.70 1.28 o 1 7 0 164.88 157.41 4.57 o 2 7 0 95.05 92.13 2.08 o 3 7 0 48.83 53.37 1.43 o 4 7 0 3.36 1.98 0.23 o 5 7 0 15.53 16.50 0.82 o 6 7 0 97.21 96.71 2.63 o 7 7 0 22.16 27.54 1.10 o 1 0 1 1522.32 1487.13 68.24 o 3 0 1 453.16 477.94 9.46 o 5 0 1 504.65 448.63 9.40 o 7 0 1 728.82 647.00 22.66 o 9 0 1 54.53 54.91 2.13 o 11 0 1 117.32 105.14 2.56 o 13 0 1 47.87 48.64 1.29 o 15 0 1 37.60 42.69 1.14 o 0 1 1 1166.40 1120.38 98.94 o 1 1 1 1807.10 1749.86 69.36 o 2 1 1 805.38 772.56 17.06 o 4 1 1 1284.16 1381.82 33.32 o 5 1 1 619.56 571.54 18.75 o 6 1 1 6.78 6.33 0.15 o 7 1 1 241.84 230.42 3.03 o 8 1 1 161.63 167.51 2.41 o 9 1 1 1138.00 1013.09 27.46 o 10 1 1 4.81 4.98 0.14 o 11 1 1 6.07 7.28 0.19 o 12 1 1 21.14 20.06 0.37 o 13 1 1 174.89 177.22 3.01 o 14 1 1 21.03 21.91 0.50 o 15 1 1 0.02 0.44 0.12 o 16 1 1 20.63 20.55 0.52 o 1 2 1 1140.45 1172.92 21.37 o 2 2 1 48.15 45.21 0.63 o 3 2 1 1580.96 1653.17 31.02 o 4 2 1 5.60 8.81 0.16 o 5 2 1 598.30 584.73 13.69 o 6 2 1 501.05 547.91 9.74 o 7 2 1 1686.91 1612.26 63.89 o 8 2 1 39.16 42.42 0.59 o 9 2 1 97.02 103.49 1.36 o 10 2 1 2.70 2.55 0.12 o 11 2 1 440.02 421.60 5.52 o 12 2 1 11.20 12.29 0.31 o 13 2 1 1.70 2.24 0.15 o 14 2 1 9.82 9.82 0.34 o 15 2 1 69.62 71.52 1.38 o 16 2 1 4.05 3.87 0.34 o 0 3 1 63.63 57.79 1.07 o 1 3 1 239.80 226.45 2.85 o 2 3 1 212.50 240.69 3.04 o 3 3 1 42.45 38.54 0.58 o 4 3 1 34.62 30.87 0.51 o 5 3 1 361.26 340.28 4.84 o 6 3 1 1.12 1.16 0.10 o 7 3 1 64.50 69.13 0.96 o 8 3 1 17.21 19.54 0.32 o 9 3 1 96.14 90.27 1.17 o 10 3 1 121.32 118.64 1.63 o 11 3 1 15.90 15.17 0.28 o 12 3 1 19.95 21.80 0.40 o 13 3 1 145.73 145.90 2.37 o 14 3 1 6.05 4.61 0.22 o 15 3 1 0.19 0.31 0.24 o 1 4 1 565.42 586.87 8.33 o 2 4 1 611.60 647.38 10.77 o 3 4 1 296.93 293.40 3.71 o 4 4 1 16.47 16.64 0.30 o 5 4 1 64.26 66.16 0.89 o 6 4 1 84.23 89.14 1.19 o 7 4 1 164.86 162.97 2.40 o 8 4 1 3.04 4.20 0.15 o 9 4 1 42.74 43.49 0.73 o 10 4 1 14.62 17.40 0.34 o 11 4 1 73.36 74.19 1.10 o 12 4 1 16.67 14.36 0.38 o 13 4 1 22.83 19.55 0.49 o 14 4 1 71.19 68.21 1.69 o 0 5 1 169.04 172.49 2.96 o 1 5 1 429.89 433.30 4.98 o 2 5 1 1.45 1.33 0.08 o 3 5 1 47.54 48.52 0.70 o 4 5 1 41.71 41.50 0.58 o 5 5 1 339.32 341.68 4.53 o 6 5 1 71.38 68.10 1.11 o 7 5 1 0.39 1.44 0.11 o 8 5 1 82.55 82.59 1.22 o 9 5 1 158.41 156.73 2.22 o 10 5 1 3.55 3.88 0.21 o 11 5 1 5.37 6.90 0.33 o 12 5 1 50.45 55.64 1.34 o 1 6 1 74.15 73.94 0.95 o 2 6 1 72.68 74.21 1.04 o 3 6 1 327.36 324.46 4.66 o 4 6 1 11.56 9.64 0.24 o 5 6 1 15.24 15.11 0.31 o 6 6 1 50.08 54.62 0.89 o 7 6 1 50.67 48.85 0.90 o 8 6 1 9.99 8.11 0.34 o 9 6 1 0.04 0.46 0.17 o 10 6 1 10.08 11.57 0.45 o 0 7 1 1.41 1.93 0.30 o 1 7 1 53.14 50.46 1.71 o 2 7 1 0.82 0.65 0.14 o 3 7 1 9.39 8.14 0.31 o 4 7 1 62.68 65.22 1.28 o 5 7 1 18.59 16.57 0.47 o 6 7 1 0.37 0.60 0.20 o 2 0 2 650.39 666.47 31.19 o 4 0 2 1004.55 886.53 29.58 o 6 0 2 1018.13 934.02 31.01 o 8 0 2 697.64 705.71 19.16 o 10 0 2 117.51 131.65 3.17 o 12 0 2 298.37 305.21 8.39 o 14 0 2 63.65 66.57 1.51 o 16 0 2 8.71 9.84 0.52 o 1 1 2 15.22 17.15 0.22 o 3 1 2 228.64 258.20 3.14 o 4 1 2 65.16 70.64 0.92 o 5 1 2 11.24 8.47 0.13 o 6 1 2 626.73 601.53 8.91 o 7 1 2 1.43 1.28 0.06 o 8 1 2 10.12 6.93 0.13 o 9 1 2 28.54 31.30 0.49 o 10 1 2 129.04 114.48 1.68 o 11 1 2 1.54 2.16 0.13 o 12 1 2 64.93 65.93 1.17 o 13 1 2 15.78 18.13 0.40 o 14 1 2 145.63 151.95 2.60 o 15 1 2 39.36 41.72 0.76 o 16 1 2 29.69 31.29 0.72 o 0 2 2 452.84 429.07 9.01 o 1 2 2 60.09 67.64 0.95 o 2 2 2 271.06 288.30 4.29 o 3 2 2 74.37 76.11 1.12 o 4 2 2 711.80 706.01 14.73 o 5 2 2 35.91 40.00 0.51 o 6 2 2 71.41 61.86 0.89 o 7 2 2 47.87 54.58 0.76 o 8 2 2 238.89 221.40 2.92 o 9 2 2 15.17 13.69 0.25 o 10 2 2 1.02 1.01 0.10 o 11 2 2 73.51 77.32 1.14 o 12 2 2 53.64 52.99 0.91 o 13 2 2 40.71 44.48 0.79 o 14 2 2 18.10 18.26 0.42 o 15 2 2 0.02 0.10 0.17 o 1 3 2 58.39 57.68 0.78 o 2 3 2 1269.38 1270.80 59.48 o 3 3 2 134.47 144.43 2.09 o 4 3 2 3.68 2.04 0.10 o 5 3 2 244.77 250.80 3.61 o 6 3 2 243.43 238.76 3.45 o 7 3 2 394.71 402.36 5.50 o 8 3 2 341.68 337.10 4.44 o 9 3 2 72.32 68.65 1.03 o 10 3 2 300.06 297.79 4.86 o 11 3 2 83.90 86.03 1.32 o 12 3 2 77.54 74.53 1.23 o 13 3 2 1.24 1.38 0.15 o 14 3 2 28.48 30.12 0.72 o 0 4 2 665.79 642.50 14.47 o 1 4 2 1.51 1.46 0.07 o 2 4 2 15.99 17.08 0.28 o 3 4 2 191.90 183.13 2.81 o 4 4 2 1202.01 1127.10 40.93 o 5 4 2 42.26 40.10 0.64 o 6 4 2 20.02 23.34 0.42 o 7 4 2 4.07 3.19 0.13 o 8 4 2 431.27 424.02 6.22 o 9 4 2 36.08 38.08 0.65 o 10 4 2 68.66 68.80 1.08 o 11 4 2 2.08 1.99 0.16 o 12 4 2 32.78 33.74 0.87 o 13 4 2 0.06 0.16 0.17 o 1 5 2 44.09 47.17 0.68 o 2 5 2 27.91 27.20 0.47 o 3 5 2 57.42 56.87 0.92 o 4 5 2 0.98 1.17 0.10 o 5 5 2 38.42 42.97 0.89 o 6 5 2 125.73 127.81 1.93 o 7 5 2 36.02 35.50 0.65 o 8 5 2 43.05 42.67 0.75 o 9 5 2 27.25 29.24 0.58 o 10 5 2 26.34 27.13 0.70 o 11 5 2 1.69 1.77 0.18 o 12 5 2 32.96 27.93 0.73 o 0 6 2 180.09 176.00 3.25 o 1 6 2 188.39 193.39 2.74 o 2 6 2 32.61 36.79 0.63 o 3 6 2 168.07 176.04 2.57 o 4 6 2 77.60 77.09 1.15 o 5 6 2 44.85 48.33 0.80 o 6 6 2 8.44 7.31 0.24 o 7 6 2 18.70 20.56 0.57 o 8 6 2 74.71 70.64 1.23 o 9 6 2 78.66 87.54 1.59 o 1 7 2 27.20 27.57 0.64 o 2 7 2 85.33 84.27 1.47 o 3 7 2 34.78 33.97 0.59 o 4 7 2 22.70 24.27 0.57 o 5 7 2 0.41 0.67 0.19 o 1 0 3 1712.43 1491.11 47.54 o 3 0 3 561.54 532.29 8.82 o 5 0 3 1770.94 1788.70 83.42 o 7 0 3 98.70 80.05 1.78 o 9 0 3 33.16 34.93 0.86 o 11 0 3 149.20 159.27 3.43 o 13 0 3 0.44 0.44 0.16 o 15 0 3 41.61 39.78 1.00 o 0 1 3 58.25 51.76 0.98 o 1 1 3 65.61 53.28 0.73 o 2 1 3 185.07 218.05 2.58 o 3 1 3 13.27 5.28 0.12 o 4 1 3 55.70 64.97 0.93 o 5 1 3 1167.51 1174.60 27.43 o 6 1 3 16.26 20.96 0.27 o 7 1 3 43.09 42.48 0.56 o 8 1 3 5.46 7.74 0.23 o 9 1 3 744.22 739.08 10.46 o 10 1 3 36.68 41.68 0.70 o 11 1 3 5.69 5.49 0.18 o 12 1 3 2.32 2.72 0.16 o 13 1 3 46.85 49.79 0.87 o 14 1 3 62.94 63.04 1.17 o 15 1 3 19.27 21.15 0.51 o 1 2 3 1984.93 2044.00 77.15 o 2 2 3 349.02 366.12 5.21 o 3 2 3 616.29 605.60 9.88 o 4 2 3 17.16 14.10 0.24 o 5 2 3 349.16 383.70 4.84 o 6 2 3 46.08 45.37 0.64 o 7 2 3 613.77 581.51 8.25 o 8 2 3 7.70 9.34 0.19 o 9 2 3 0.55 1.05 0.08 o 10 2 3 141.70 142.18 2.00 o 11 2 3 490.18 500.98 7.48 o 12 2 3 140.56 141.63 2.29 o 13 2 3 0.11 0.12 0.12 o 14 2 3 4.85 4.77 0.33 o 15 2 3 85.07 84.73 1.95 o 0 3 3 69.51 57.19 1.50 o 1 3 3 436.61 404.42 5.51 o 2 3 3 0.59 0.51 0.07 o 3 3 3 95.51 75.13 1.14 o 4 3 3 53.30 66.41 1.11 o 5 3 3 761.31 785.84 11.69 o 6 3 3 17.29 16.61 0.36 o 7 3 3 372.21 372.56 5.90 o 8 3 3 146.66 149.58 2.20 o 9 3 3 37.43 36.80 0.72 o 10 3 3 0.19 0.02 0.09 o 11 3 3 8.40 8.95 0.27 o 12 3 3 2.32 2.19 0.15 o 13 3 3 41.03 40.62 0.87 o 14 3 3 3.31 2.27 0.24 o 1 4 3 105.28 106.79 1.47 o 2 4 3 77.28 73.95 1.14 o 3 4 3 32.54 30.61 0.54 o 4 4 3 307.18 308.13 4.63 o 5 4 3 50.66 49.40 0.90 o 6 4 3 296.63 309.79 4.70 o 7 4 3 75.48 70.76 1.16 o 8 4 3 1.27 1.17 0.12 o 9 4 3 15.29 14.55 0.33 o 10 4 3 65.43 68.74 1.37 o 11 4 3 91.47 91.81 1.78 o 12 4 3 0.02 -0.01 0.14 o 13 4 3 3.03 3.83 0.32 o 0 5 3 959.14 947.02 18.17 o 1 5 3 601.19 592.77 8.45 o 2 5 3 92.17 93.35 1.44 o 3 5 3 207.67 213.09 3.29 o 4 5 3 121.85 127.21 2.00 o 5 5 3 319.00 314.26 4.76 o 6 5 3 4.06 5.32 0.20 o 7 5 3 35.20 37.45 0.67 o 8 5 3 22.62 23.85 0.50 o 9 5 3 101.55 104.55 1.86 o 10 5 3 7.16 6.97 0.33 o 11 5 3 10.70 8.82 0.37 o 1 6 3 13.33 11.08 0.30 o 2 6 3 33.42 35.88 0.62 o 3 6 3 265.78 257.95 4.12 o 4 6 3 34.04 32.74 0.59 o 5 6 3 3.43 3.17 0.18 o 6 6 3 27.42 26.11 0.50 o 7 6 3 68.59 69.50 1.17 o 8 6 3 2.03 2.65 0.29 o 0 7 3 77.93 77.31 2.30 o 1 7 3 29.75 29.46 0.70 o 2 7 3 6.00 5.52 0.43 o 3 7 3 9.42 10.30 0.58 o 4 7 3 87.92 87.19 2.21 o 0 0 4 1834.15 1680.00 78.69 o 2 0 4 95.88 103.87 2.09 o 4 0 4 519.29 516.94 9.19 o 6 0 4 424.70 476.29 8.48 o 8 0 4 425.31 419.34 7.48 o 10 0 4 92.14 88.12 1.77 o 12 0 4 178.80 180.25 3.87 o 14 0 4 51.94 52.57 1.43 o 1 1 4 12.91 12.91 0.37 o 2 1 4 1449.17 1487.51 41.42 o 3 1 4 116.34 155.01 2.49 o 4 1 4 18.39 15.36 0.28 o 5 1 4 3.66 3.78 0.15 o 6 1 4 394.96 395.49 4.80 o 7 1 4 0.31 0.27 0.06 o 8 1 4 4.74 4.99 0.14 o 9 1 4 15.92 16.79 0.33 o 10 1 4 96.14 99.14 1.75 o 11 1 4 2.31 1.99 0.12 o 12 1 4 42.08 42.38 0.70 o 13 1 4 11.62 10.67 0.34 o 14 1 4 92.87 89.23 1.71 o 0 2 4 159.24 123.80 2.26 o 1 2 4 13.28 16.28 0.37 o 2 2 4 75.05 84.95 1.29 o 3 2 4 8.30 5.63 0.15 o 4 2 4 346.08 328.86 4.97 o 5 2 4 40.42 41.88 0.61 o 6 2 4 20.75 24.35 0.34 o 7 2 4 22.97 23.60 0.40 o 8 2 4 158.14 157.35 2.41 o 9 2 4 10.43 10.69 0.27 o 10 2 4 0.48 0.44 0.10 o 11 2 4 47.38 46.85 0.85 o 12 2 4 28.33 26.83 0.58 o 13 2 4 30.78 29.02 0.58 o 14 2 4 13.87 13.79 1.27 o 1 3 4 63.53 68.73 1.06 o 2 3 4 627.25 640.05 9.54 o 3 3 4 75.32 77.00 1.18 o 4 3 4 0.24 0.04 0.07 o 5 3 4 132.57 136.47 2.53 o 6 3 4 129.50 129.80 2.29 o 7 3 4 207.52 215.26 3.94 o 8 3 4 241.51 248.57 3.96 o 9 3 4 45.30 42.16 0.73 o 10 3 4 200.01 198.73 3.22 o 11 3 4 45.97 49.36 0.95 o 12 3 4 57.54 56.90 1.18 o 13 3 4 0.78 0.46 0.19 o 0 4 4 346.45 343.63 10.04 o 1 4 4 2.26 1.82 0.13 o 2 4 4 14.81 14.52 0.30 o 3 4 4 106.43 102.82 1.56 o 4 4 4 753.20 764.65 11.98 o 5 4 4 22.88 23.98 0.59 o 6 4 4 7.72 7.42 0.24 o 7 4 4 2.07 2.48 0.14 o 8 4 4 300.70 310.47 4.70 o 9 4 4 22.35 20.72 0.43 o 10 4 4 34.28 33.06 0.68 o 11 4 4 3.11 3.55 0.29 o 12 4 4 21.25 20.16 1.38 o 1 5 4 38.52 35.68 0.75 o 2 5 4 20.97 19.63 0.43 o 3 5 4 38.62 38.72 0.70 o 4 5 4 0.09 0.13 0.09 o 5 5 4 16.50 15.01 0.36 o 6 5 4 68.03 66.43 1.11 o 7 5 4 21.34 22.75 0.50 o 8 5 4 26.16 25.53 0.52 o 9 5 4 13.80 12.39 0.41 o 10 5 4 16.04 17.23 0.68 o 0 6 4 88.78 87.79 2.18 o 1 6 4 133.10 127.97 2.32 o 2 6 4 16.11 14.54 0.45 o 3 6 4 127.01 117.37 2.10 o 4 6 4 39.66 43.79 0.79 o 5 6 4 26.87 28.14 0.54 o 6 6 4 8.79 8.53 0.32 o 7 6 4 11.57 11.05 0.48 o 1 0 5 12.71 9.06 0.25 o 3 0 5 216.63 225.82 4.43 o 5 0 5 83.96 98.18 1.84 o 7 0 5 234.74 240.11 5.85 o 9 0 5 18.13 17.70 0.47 o 11 0 5 43.89 44.85 3.60 o 13 0 5 9.19 11.70 1.27 o 0 1 5 71.67 74.13 2.22 o 1 1 5 419.92 423.20 5.56 o 2 1 5 72.94 74.11 1.12 o 3 1 5 612.56 619.71 7.54 o 4 1 5 151.71 159.24 2.32 o 5 1 5 205.25 206.46 2.99 o 6 1 5 2.85 3.14 0.13 o 7 1 5 48.36 52.43 1.05 o 8 1 5 37.56 33.96 0.66 o 9 1 5 315.86 328.07 6.39 o 10 1 5 0.64 0.46 0.13 o 11 1 5 1.43 0.80 0.15 o 12 1 5 7.54 8.84 0.53 o 13 1 5 68.51 70.73 3.61 o 1 2 5 257.28 265.22 3.84 o 2 2 5 21.95 20.49 0.50 o 3 2 5 396.06 401.13 5.75 o 4 2 5 5.41 2.91 0.13 o 5 2 5 91.52 84.47 1.25 o 6 2 5 75.40 81.16 1.35 o 7 2 5 479.40 502.01 7.93 o 8 2 5 6.61 8.79 0.30 o 9 2 5 24.18 25.12 0.60 o 10 2 5 1.69 1.76 0.21 o 11 2 5 161.23 168.70 5.39 o 12 2 5 4.01 3.33 0.33 o 0 3 5 12.67 13.49 0.68 o 1 3 5 126.62 140.99 2.48 o 2 3 5 33.78 30.19 0.60 o 3 3 5 28.91 36.73 0.70 o 4 3 5 13.89 13.06 0.41 o 5 3 5 167.57 169.18 2.63 o 6 3 5 1.14 1.38 0.16 o 7 3 5 28.15 28.46 0.67 o 8 3 5 12.48 13.99 0.40 o 9 3 5 30.63 29.30 0.75 o 10 3 5 34.80 37.41 1.07 o 11 3 5 5.06 5.77 0.46 o 12 3 5 10.09 9.95 0.66 o 1 4 5 194.61 186.77 3.25 o 2 4 5 148.08 144.17 2.55 o 3 4 5 113.79 119.91 2.01 o 4 4 5 3.24 2.10 0.16 o 5 4 5 16.15 16.37 0.45 o 6 4 5 30.44 27.90 0.66 o 7 4 5 66.02 68.22 1.28 o 8 4 5 1.57 1.21 0.18 o 9 4 5 11.12 12.92 0.49 o 10 4 5 3.14 2.51 0.29 o 0 5 5 76.42 64.70 2.98 o 1 5 5 146.50 134.96 2.77 o 2 5 5 0.00 0.02 0.14 o 3 5 5 13.58 13.04 0.42 o 4 5 5 19.27 17.16 0.52 o 5 5 5 137.45 136.16 2.87 o 6 5 5 22.99 24.39 0.60 o 7 5 5 0.05 -0.11 0.23 o 8 5 5 41.73 45.47 1.30 o 1 6 5 40.00 42.51 1.17 o 2 6 5 25.12 28.70 0.78 o 3 6 5 137.46 132.71 2.94 o 4 6 5 3.60 4.33 0.39 o 0 0 6 2615.41 2357.40 103.65 o 2 0 6 41.00 42.90 0.81 o 4 0 6 578.07 572.87 9.57 o 6 0 6 5.03 6.46 0.30 o 8 0 6 133.88 132.85 3.25 o 10 0 6 49.63 49.87 2.68 o 12 0 6 158.49 151.61 10.29 o 1 1 6 0.16 0.20 0.09 o 2 1 6 47.09 50.16 0.81 o 3 1 6 117.10 123.41 1.85 o 4 1 6 266.63 286.33 4.35 o 5 1 6 19.80 19.59 0.36 o 6 1 6 205.99 209.13 3.21 o 7 1 6 11.38 10.65 0.29 o 8 1 6 10.53 13.23 0.36 o 9 1 6 19.49 17.56 0.36 o 10 1 6 37.78 36.72 0.97 o 11 1 6 0.49 0.06 0.20 o 0 2 6 373.29 405.30 9.69 o 1 2 6 10.61 9.34 0.47 o 2 2 6 0.61 0.95 0.11 o 3 2 6 21.41 22.91 0.55 o 4 2 6 140.55 160.35 2.49 o 5 2 6 172.09 165.23 2.55 o 6 2 6 0.78 0.25 0.10 o 7 2 6 179.94 175.44 3.25 o 8 2 6 15.13 15.65 0.55 o 9 2 6 11.00 10.90 0.83 o 10 2 6 25.64 26.19 0.85 o 11 2 6 7.49 6.64 0.71 o 1 3 6 58.89 51.09 1.23 o 2 3 6 424.36 414.74 7.01 o 3 3 6 4.90 3.63 0.30 o 4 3 6 5.85 6.58 0.22 o 5 3 6 16.99 16.77 0.37 o 6 3 6 252.97 251.10 4.97 o 7 3 6 3.19 2.09 0.26 o 8 3 6 27.77 29.93 0.78 o 9 3 6 16.95 16.94 0.68 o 10 3 6 139.15 138.18 4.06 o 0 4 6 26.68 30.60 1.11 o 1 4 6 3.08 2.78 0.24 o 2 4 6 8.90 7.95 0.30 o 3 4 6 1.24 0.73 0.16 o 4 4 6 87.81 90.70 1.78 o 5 4 6 24.78 23.46 0.65 o 6 4 6 31.35 29.90 0.71 o 7 4 6 12.79 10.37 0.43 o 8 4 6 42.15 41.42 1.07 o 1 5 6 46.41 43.27 1.32 o 2 5 6 93.60 97.04 2.47 o 3 5 6 12.26 12.11 0.51 o 4 5 6 3.26 2.46 0.32 o 5 5 6 74.59 69.20 1.65 o 1 0 7 15.44 16.28 0.46 o 3 0 7 86.55 93.65 1.79 o 5 0 7 29.62 32.00 0.77 o 7 0 7 87.41 92.47 1.92 o 9 0 7 5.97 5.29 0.38 o 0 1 7 32.05 29.63 0.98 o 1 1 7 160.50 175.05 2.48 o 2 1 7 21.86 22.99 0.41 o 3 1 7 249.57 259.78 3.46 o 4 1 7 80.38 82.03 1.26 o 5 1 7 61.80 66.17 1.11 o 6 1 7 0.01 0.15 0.10 o 7 1 7 16.21 16.04 0.36 o 8 1 7 19.30 16.12 0.43 o 9 1 7 148.68 147.18 7.03 o 1 2 7 89.63 92.84 1.50 o 2 2 7 1.61 2.19 0.22 o 3 2 7 160.18 157.60 2.80 o 4 2 7 1.46 0.71 0.15 o 5 2 7 52.28 47.90 0.83 o 6 2 7 45.64 41.86 1.26 o 7 2 7 183.50 178.35 4.50 o 8 2 7 11.17 9.40 0.46 o 0 3 7 4.29 5.58 0.51 o 1 3 7 31.95 37.76 0.79 o 2 3 7 14.02 11.33 0.38 o 3 3 7 6.53 8.15 0.34 o 4 3 7 12.08 8.44 0.36 o 5 3 7 53.90 58.16 2.13 o 6 3 7 0.00 0.16 0.24 o 7 3 7 4.35 3.77 0.39 o 1 4 7 83.95 76.69 1.88 o 2 4 7 73.13 58.12 1.56 o 3 4 7 50.77 51.58 1.59 o 4 4 7 0.20 0.96 0.48 o 0 0 8 205.83 204.76 5.75 o 2 0 8 6.64 6.54 0.36 o 4 0 8 71.41 71.88 1.85 o 6 0 8 58.98 64.37 3.17 o 1 1 8 0.65 0.36 0.19 o 2 1 8 183.26 188.47 3.76 o 3 1 8 8.89 8.32 0.32 o 4 1 8 4.19 4.05 0.25 o 5 1 8 0.09 0.29 0.19 o 6 1 8 61.24 57.82 2.41 o 0 2 8 34.24 30.48 1.02 o 1 2 8 0.02 -0.18 0.30 o 2 2 8 10.92 11.91 0.66 o 3 2 8 3.58 2.44 0.36 o 4 2 8 49.83 49.58 1.39 o