#------------------------------------------------------------------------------ #$Date: 2023-11-01 20:43:16 +0200 (Wed, 01 Nov 2023) $ #$Revision: 287200 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519451.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519451 _cell_angle_alpha 90.000 _cell_angle_beta 108.852 _cell_angle_gamma 90.000 _cell_length_a 9.0643 _cell_length_b 16.0149 _cell_length_c 11.2228 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file S05_Pq-Cl2_3H2O_P21_c.fcf _cod_data_source_block jw22641 _shelx_title ' jw22641_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.83 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 433.19 474.50 11.63 o 3 0 0 3.24 2.64 0.30 o 4 0 0 4606.97 4402.01 139.90 o 5 0 0 618.91 635.22 15.04 o 6 0 0 982.13 925.39 18.88 o 7 0 0 665.68 663.03 15.75 o 8 0 0 7.25 6.13 0.41 o 9 0 0 429.99 411.48 11.06 o 10 0 0 343.29 380.98 9.19 o 11 0 0 137.58 141.21 3.63 o 1 1 0 41.25 43.89 0.72 o 2 1 0 695.82 659.85 18.91 o 3 1 0 1016.99 992.91 40.09 o 4 1 0 1060.21 988.72 21.64 o 5 1 0 1126.91 1058.10 21.52 o 6 1 0 2231.30 2068.11 49.58 o 7 1 0 31.34 27.00 0.61 o 8 1 0 1787.79 1790.85 25.65 o 9 1 0 68.68 68.31 1.18 o 10 1 0 88.44 83.08 1.63 o 11 1 0 96.69 94.10 1.78 o 1 2 0 170.59 190.92 3.90 o 2 2 0 524.26 547.66 12.85 o 3 2 0 4.06 3.51 0.21 o 4 2 0 25.61 18.97 1.11 o 5 2 0 203.08 192.07 3.39 o 6 2 0 932.11 923.38 14.19 o 7 2 0 246.76 229.88 3.15 o 8 2 0 125.78 122.07 1.77 o 9 2 0 29.69 29.86 0.66 o 10 2 0 665.79 688.13 12.68 o 11 2 0 53.08 46.10 0.98 o 1 3 0 51.86 53.36 0.88 o 2 3 0 884.00 810.19 32.95 o 3 3 0 428.24 452.25 9.27 o 4 3 0 4311.70 4401.25 100.17 o 5 3 0 211.79 219.49 2.94 o 6 3 0 1.41 1.57 0.12 o 7 3 0 339.59 327.95 4.38 o 8 3 0 3.22 2.74 0.20 o 9 3 0 57.67 55.65 0.97 o 10 3 0 148.25 154.47 2.79 o 11 3 0 33.79 36.85 1.05 o 0 4 0 10.11 7.85 0.43 o 1 4 0 51.79 56.27 1.01 o 3 4 0 118.81 116.09 2.27 o 4 4 0 3400.30 3311.19 78.31 o 5 4 0 48.80 50.85 0.80 o 6 4 0 2883.77 2756.32 64.15 o 7 4 0 6.88 6.95 0.29 o 8 4 0 840.14 849.51 11.67 o 9 4 0 0.06 0.23 0.14 o 10 4 0 203.48 199.30 3.72 o 1 5 0 86.60 96.68 1.53 o 2 5 0 212.27 230.41 4.79 o 3 5 0 484.59 537.23 9.82 o 4 5 0 2479.47 2452.97 98.70 o 5 5 0 196.83 188.87 2.45 o 6 5 0 43.19 46.65 0.88 o 7 5 0 222.80 214.20 3.11 o 8 5 0 78.91 77.74 1.30 o 9 5 0 13.03 13.43 0.41 o 10 5 0 17.42 20.45 0.54 o 1 6 0 11.60 13.88 0.32 o 2 6 0 4831.25 4686.84 219.52 o 3 6 0 354.42 394.41 7.27 o 4 6 0 3776.58 3684.80 148.20 o 5 6 0 119.05 127.55 1.71 o 6 6 0 902.10 886.50 12.08 o 7 6 0 4.16 3.17 0.24 o 8 6 0 399.24 423.77 6.28 o 9 6 0 141.99 145.55 2.37 o 10 6 0 8.50 5.55 0.35 o 1 7 0 5.05 3.28 0.14 o 2 7 0 133.69 156.24 3.12 o 3 7 0 229.40 223.54 2.97 o 4 7 0 1160.37 1198.35 14.00 o 5 7 0 285.19 290.92 3.70 o 6 7 0 317.89 310.05 4.37 o 7 7 0 0.83 0.74 0.15 o 8 7 0 463.20 469.16 6.91 o 9 7 0 35.73 33.88 0.87 o 10 7 0 1.99 0.45 0.22 o 0 8 0 619.02 788.59 22.74 o 1 8 0 48.36 43.84 1.02 o 2 8 0 77.12 95.84 1.34 o 3 8 0 113.64 104.16 1.34 o 4 8 0 187.42 179.55 2.45 o 5 8 0 184.76 191.13 2.48 o 6 8 0 283.15 290.54 4.12 o 7 8 0 49.36 39.89 1.40 o 8 8 0 12.77 18.23 0.55 o 9 8 0 23.83 23.20 0.69 o 10 8 0 196.92 196.55 3.79 o 1 9 0 291.02 279.42 4.74 o 2 9 0 316.03 292.74 3.68 o 3 9 0 254.33 233.56 2.85 o 4 9 0 660.23 654.67 8.10 o 5 9 0 261.29 273.13 3.70 o 6 9 0 420.95 456.29 7.21 o 7 9 0 443.93 435.64 6.95 o 8 9 0 100.35 131.67 2.49 o 9 9 0 116.93 121.34 2.24 o 10 9 0 309.58 331.70 6.17 o 0 10 0 4513.82 3528.61 148.06 o 1 10 0 421.29 430.29 5.14 o 2 10 0 5515.40 4797.95 192.85 o 3 10 0 505.82 490.14 5.83 o 4 10 0 2591.26 2514.42 45.47 o 5 10 0 17.91 17.40 0.40 o 6 10 0 1708.84 1663.88 33.86 o 7 10 0 27.35 24.76 0.63 o 8 10 0 75.10 85.93 1.70 o 9 10 0 43.25 42.76 0.95 o 1 11 0 73.89 74.54 0.98 o 2 11 0 231.35 235.51 2.89 o 3 11 0 30.97 26.61 0.48 o 4 11 0 915.48 926.98 11.42 o 5 11 0 86.15 85.84 1.31 o 6 11 0 449.92 438.38 6.96 o 7 11 0 279.65 297.93 5.18 o 8 11 0 320.53 311.14 5.38 o 9 11 0 74.17 82.57 1.48 o 0 12 0 127.89 97.79 1.70 o 1 12 0 266.54 270.89 3.19 o 2 12 0 16.63 17.41 0.62 o 3 12 0 999.34 994.72 12.83 o 4 12 0 936.48 950.81 12.94 o 5 12 0 6.59 7.53 0.33 o 6 12 0 441.49 429.76 6.79 o 7 12 0 7.34 7.32 0.34 o 8 12 0 230.22 231.38 3.74 o 9 12 0 1.27 0.55 0.17 o 1 13 0 0.39 0.31 0.11 o 2 13 0 43.90 43.51 0.71 o 3 13 0 200.17 202.48 2.69 o 4 13 0 767.18 800.24 10.95 o 5 13 0 32.83 35.58 0.81 o 6 13 0 54.33 60.99 1.28 o 7 13 0 125.90 136.81 2.51 o 8 13 0 20.19 22.59 0.60 o 0 14 0 1.87 4.17 0.51 o 1 14 0 98.97 98.73 1.36 o 2 14 0 1093.97 1093.00 13.47 o 3 14 0 56.16 57.81 1.04 o 4 14 0 1718.27 1792.16 23.06 o 5 14 0 0.12 0.10 0.15 o 6 14 0 407.35 427.80 7.29 o 7 14 0 22.83 22.42 0.59 o 8 14 0 237.96 239.76 4.14 o 1 15 0 6.72 7.12 0.29 o 2 15 0 237.52 241.33 3.24 o 3 15 0 111.99 112.38 1.82 o 4 15 0 48.41 53.23 1.16 o 5 15 0 2.53 2.11 0.33 o 6 15 0 62.15 69.67 1.56 o 7 15 0 5.23 5.23 0.34 o 0 16 0 232.85 263.49 5.66 o 1 16 0 3.85 3.16 0.31 o 2 16 0 2373.23 2322.61 38.30 o 3 16 0 128.27 130.30 2.44 o 4 16 0 506.62 514.18 9.54 o 5 16 0 3.81 3.43 0.32 o 6 16 0 128.55 125.67 2.51 o 7 16 0 2.15 2.45 0.30 o 1 17 0 103.33 96.71 2.09 o 2 17 0 288.91 295.51 5.62 o 3 17 0 129.67 128.77 2.61 o 4 17 0 120.48 121.56 2.50 o 5 17 0 56.49 57.44 1.31 o 6 17 0 43.50 41.01 0.99 o 0 18 0 50.13 47.33 2.92 o 1 18 0 211.47 212.04 4.63 o 2 18 0 5.62 7.34 0.72 o 3 18 0 77.02 78.39 2.72 o 4 18 0 4.70 4.83 0.97 o 5 18 0 5.59 5.89 0.50 o 1 19 0 6.94 6.85 0.56 o 2 19 0 241.73 234.85 5.79 o 3 19 0 46.66 44.92 1.44 o 4 19 0 330.54 349.20 8.43 o 0 20 0 1026.13 981.07 40.09 o 1 20 0 174.65 178.27 5.55 o 2 20 0 798.74 769.09 22.29 o 3 20 0 19.50 17.59 0.85 o -11 1 1 224.63 218.44 3.81 o -10 1 1 2.76 2.92 0.24 o -9 1 1 101.65 99.03 1.83 o -8 1 1 159.85 164.34 3.02 o -7 1 1 647.55 620.48 9.03 o -6 1 1 203.99 201.45 3.27 o -5 1 1 1419.54 1352.44 31.52 o -4 1 1 7.77 10.75 0.46 o -3 1 1 283.38 266.98 6.88 o -2 1 1 453.92 472.29 9.59 o -1 1 1 37.16 32.59 1.16 o 0 1 1 20.07 24.21 0.58 o 2 1 1 323.52 336.55 6.91 o 3 1 1 42.65 62.83 1.09 o 4 1 1 61.61 58.71 1.07 o 5 1 1 311.14 257.67 3.85 o 6 1 1 90.38 84.11 1.54 o 7 1 1 4642.27 4390.28 151.56 o 8 1 1 0.26 0.16 0.12 o 9 1 1 317.14 311.34 4.18 o 10 1 1 70.76 77.55 1.53 o -11 2 1 1.73 2.05 0.40 o -10 2 1 8.07 8.48 0.38 o -9 2 1 261.68 247.04 4.05 o -8 2 1 1088.85 1068.95 14.56 o -7 2 1 2070.14 2015.83 30.79 o -6 2 1 629.32 596.08 9.36 o -5 2 1 43.27 59.58 1.31 o -4 2 1 218.51 239.68 4.53 o -3 2 1 3366.98 3300.64 78.86 o -2 2 1 12.51 11.13 0.39 o 0 2 1 6.32 6.15 0.30 o 2 2 1 342.99 360.29 6.58 o 3 2 1 54.60 35.62 1.00 o 4 2 1 0.69 0.53 0.14 o 5 2 1 17.11 7.33 0.28 o 6 2 1 4.70 4.45 0.23 o 7 2 1 140.76 150.58 2.13 o 8 2 1 68.02 67.24 1.17 o 9 2 1 148.78 151.54 2.28 o 10 2 1 138.48 145.19 2.62 o -11 3 1 3.44 2.43 0.29 o -10 3 1 21.05 21.93 0.64 o -9 3 1 153.40 151.09 2.99 o -8 3 1 23.01 20.53 0.50 o -7 3 1 550.43 575.10 8.42 o -6 3 1 514.84 519.52 7.58 o -5 3 1 2326.68 2198.80 62.68 o -4 3 1 70.09 61.84 2.29 o -2 3 1 483.06 505.12 10.25 o -1 3 1 382.81 487.28 8.84 o 0 3 1 449.36 483.55 19.69 o 2 3 1 1385.48 1401.97 23.43 o 3 3 1 4108.07 3624.53 84.12 o 4 3 1 141.48 127.25 2.09 o 6 3 1 1.66 1.64 0.14 o 7 3 1 1168.98 1169.33 15.05 o 8 3 1 4.63 5.14 0.29 o 9 3 1 489.08 478.25 9.25 o 10 3 1 10.07 11.13 0.41 o -11 4 1 705.40 768.52 14.00 o -10 4 1 5.11 6.05 0.34 o -9 4 1 147.17 143.91 2.32 o -8 4 1 370.02 377.24 5.30 o -7 4 1 615.22 595.19 8.19 o -6 4 1 649.34 635.15 8.70 o -5 4 1 60.43 46.50 0.78 o -4 4 1 619.69 636.33 12.20 o -3 4 1 191.61 180.55 3.39 o -2 4 1 29.89 26.43 0.67 o 0 4 1 0.14 0.64 0.20 o 1 4 1 413.45 397.68 7.23 o 2 4 1 230.06 246.05 4.57 o 3 4 1 8577.39 8343.69 375.99 o 4 4 1 49.69 64.34 0.84 o 5 4 1 1058.12 1077.10 13.20 o 6 4 1 703.58 697.51 9.05 o 7 4 1 274.06 288.48 3.89 o 8 4 1 628.22 621.99 8.13 o 9 4 1 142.95 141.30 2.12 o 10 4 1 56.95 53.41 1.14 o -11 5 1 394.48 393.05 7.25 o -10 5 1 123.01 131.38 2.64 o -9 5 1 451.84 442.96 6.54 o -8 5 1 5.27 4.81 0.31 o -7 5 1 260.57 268.81 3.83 o -6 5 1 10.37 10.98 0.31 o -5 5 1 270.74 287.42 4.00 o -4 5 1 10.55 9.16 0.24 o -3 5 1 4444.60 4543.43 103.43 o -2 5 1 389.12 420.70 7.67 o -1 5 1 686.52 676.09 14.19 o 0 5 1 1392.07 1515.55 41.43 o 1 5 1 562.99 550.12 9.98 o 2 5 1 796.30 792.28 13.09 o 3 5 1 972.87 1112.15 22.54 o 4 5 1 61.74 56.16 0.76 o 5 5 1 0.81 1.06 0.12 o 6 5 1 187.76 176.27 2.33 o 7 5 1 251.55 230.48 3.15 o 8 5 1 153.91 155.37 2.47 o 9 5 1 454.35 450.43 7.10 o 10 5 1 0.99 0.70 0.19 o -10 6 1 23.06 17.86 0.67 o -9 6 1 131.09 131.55 2.15 o -8 6 1 131.21 139.32 2.14 o -7 6 1 203.62 232.58 3.35 o -6 6 1 286.10 269.89 3.82 o -5 6 1 581.27 446.51 6.14 o -4 6 1 492.92 482.02 6.61 o -3 6 1 2223.86 2317.37 56.01 o -2 6 1 33.18 27.08 0.74 o -1 6 1 1768.57 1511.83 61.06 o 0 6 1 4.67 5.21 0.45 o 1 6 1 275.41 277.81 5.72 o 2 6 1 0.49 1.21 0.12 o 3 6 1 19.20 30.67 0.50 o 4 6 1 295.56 291.98 3.40 o 5 6 1 1054.44 1134.64 13.91 o 6 6 1 411.77 417.78 5.53 o 7 6 1 1215.50 1112.69 14.35 o 8 6 1 233.69 235.64 3.60 o 9 6 1 321.87 309.93 5.36 o 10 6 1 246.38 255.20 4.83 o -10 7 1 1.25 1.86 0.29 o -9 7 1 30.01 33.12 0.77 o -8 7 1 0.39 1.33 0.18 o -7 7 1 34.74 55.55 0.97 o -6 7 1 129.76 129.16 2.09 o -5 7 1 1076.42 970.67 12.48 o -4 7 1 5.35 6.69 0.21 o -3 7 1 498.42 426.68 5.54 o -2 7 1 79.88 77.53 1.98 o 0 7 1 731.95 784.04 18.42 o 2 7 1 405.09 410.69 6.35 o 4 7 1 128.72 135.42 1.66 o 5 7 1 1797.40 1837.87 26.34 o 6 7 1 34.52 37.94 0.68 o 7 7 1 2221.90 2075.65 44.24 o 8 7 1 9.77 8.33 0.33 o 9 7 1 255.19 254.70 4.83 o 10 7 1 118.94 126.69 2.80 o -10 8 1 175.78 190.58 3.69 o -9 8 1 99.35 100.75 2.09 o -8 8 1 1.41 0.89 0.19 o -7 8 1 3.32 2.05 0.36 o -6 8 1 27.58 28.18 0.62 o -5 8 1 687.04 717.97 9.80 o -4 8 1 377.90 373.38 4.91 o -3 8 1 115.08 131.90 1.73 o -2 8 1 47.20 38.65 0.64 o -1 8 1 0.09 1.90 0.36 o 0 8 1 133.41 149.12 3.76 o 1 8 1 295.78 335.32 5.23 o 2 8 1 10.46 10.46 0.37 o 3 8 1 120.98 122.22 1.56 o 4 8 1 584.61 599.52 6.83 o 5 8 1 324.39 349.19 4.24 o 6 8 1 157.94 149.06 2.12 o 7 8 1 79.62 81.86 1.40 o 8 8 1 28.42 27.64 0.74 o 9 8 1 38.91 49.31 1.16 o -10 9 1 14.25 14.37 0.57 o -9 9 1 145.08 154.21 2.80 o -8 9 1 95.60 101.32 1.96 o -7 9 1 35.20 56.70 1.14 o -6 9 1 232.42 231.64 3.55 o -5 9 1 369.48 351.11 5.20 o -4 9 1 43.60 47.00 0.72 o -3 9 1 3410.29 3283.64 59.11 o -2 9 1 15.61 15.88 0.36 o -1 9 1 58.54 61.52 1.59 o 0 9 1 59.73 66.17 1.13 o 1 9 1 1030.88 993.92 11.16 o 2 9 1 20.77 21.43 0.35 o 3 9 1 11.77 8.32 0.25 o 4 9 1 0.32 0.25 0.09 o 5 9 1 668.96 659.49 8.61 o 6 9 1 36.66 40.84 0.84 o 7 9 1 531.91 503.56 8.55 o 8 9 1 32.77 31.68 0.84 o 9 9 1 386.04 399.29 6.77 o -10 10 1 39.11 37.15 1.02 o -9 10 1 48.79 41.06 0.94 o -8 10 1 4.45 6.80 0.36 o -7 10 1 4.46 1.17 0.17 o -6 10 1 0.61 1.50 0.20 o -5 10 1 101.78 113.55 1.84 o -4 10 1 54.69 54.58 0.87 o -3 10 1 0.56 1.94 0.19 o -2 10 1 3.38 3.62 0.17 o -1 10 1 2589.33 2840.47 56.91 o 0 10 1 50.57 53.84 0.81 o 1 10 1 166.53 210.08 2.30 o 2 10 1 10.85 11.58 0.25 o 3 10 1 1359.30 1311.46 16.05 o 4 10 1 96.28 95.69 1.45 o 5 10 1 288.87 289.51 4.14 o 6 10 1 67.69 64.76 1.20 o 7 10 1 16.91 14.86 0.52 o 8 10 1 73.31 73.19 1.46 o 9 10 1 23.69 24.95 0.68 o -9 11 1 539.38 547.55 8.53 o -8 11 1 1.95 2.60 0.25 o -7 11 1 270.50 286.38 5.47 o -6 11 1 1.49 0.48 0.19 o -5 11 1 48.41 59.67 1.17 o -4 11 1 207.80 198.14 2.73 o -3 11 1 99.54 105.10 1.52 o -2 11 1 12.18 12.71 0.29 o -1 11 1 12.46 20.24 0.39 o 0 11 1 131.94 120.69 1.43 o 1 11 1 616.21 674.66 7.38 o 2 11 1 110.43 103.69 1.39 o 3 11 1 26.92 23.01 0.43 o 4 11 1 10.16 10.16 0.30 o 5 11 1 7.25 7.86 0.31 o 6 11 1 195.48 185.06 3.07 o 7 11 1 80.32 89.67 2.26 o 8 11 1 33.13 33.22 0.80 o 9 11 1 218.55 235.86 4.82 o -9 12 1 214.50 202.85 3.53 o -8 12 1 86.56 83.03 1.66 o -7 12 1 142.72 150.03 2.55 o -6 12 1 185.43 179.17 2.99 o -5 12 1 207.66 201.57 3.13 o -4 12 1 27.21 27.24 0.58 o -3 12 1 2207.22 2201.72 36.27 o -2 12 1 8.43 8.96 0.26 o -1 12 1 1.20 0.49 0.10 o 0 12 1 50.45 48.14 0.67 o 1 12 1 19.56 24.21 0.46 o 2 12 1 0.18 0.10 0.09 o 3 12 1 105.96 95.57 1.49 o 4 12 1 171.53 177.05 2.49 o 5 12 1 662.12 655.06 11.09 o 6 12 1 56.18 65.48 1.64 o 7 12 1 85.98 80.37 1.49 o 8 12 1 46.17 52.86 1.01 o -8 13 1 69.66 69.80 1.38 o -7 13 1 317.51 329.50 5.69 o -6 13 1 2.70 2.87 0.23 o -5 13 1 112.14 109.54 1.96 o -4 13 1 55.30 63.25 1.58 o -3 13 1 8.48 9.55 0.33 o -2 13 1 33.05 32.02 0.57 o -1 13 1 3042.51 2835.30 34.46 o 0 13 1 542.98 526.84 7.00 o 1 13 1 3035.31 2950.51 39.67 o 2 13 1 348.30 351.00 4.31 o 3 13 1 5163.94 4844.99 112.94 o 4 13 1 12.48 14.26 0.66 o 5 13 1 1400.62 1479.68 22.67 o 6 13 1 32.23 35.04 0.83 o 7 13 1 204.56 197.54 4.33 o 8 13 1 3.39 3.79 0.30 o -8 14 1 36.72 35.88 0.83 o -7 14 1 140.79 137.87 2.83 o -6 14 1 239.51 244.98 4.30 o -5 14 1 1884.34 1957.31 35.39 o -4 14 1 137.55 141.57 2.31 o -3 14 1 1.15 1.33 0.18 o -2 14 1 1.98 1.95 0.15 o -1 14 1 10.61 10.12 0.27 o 0 14 1 3.50 2.97 0.16 o 1 14 1 35.13 35.04 0.64 o 2 14 1 200.29 207.10 2.89 o 3 14 1 303.32 327.18 5.71 o 4 14 1 305.70 318.05 4.82 o 5 14 1 2.23 3.66 0.35 o 6 14 1 149.68 159.14 3.53 o 7 14 1 381.48 430.66 7.99 o -7 15 1 241.02 270.65 4.67 o -6 15 1 70.27 74.04 1.82 o -5 15 1 383.61 384.93 6.59 o -4 15 1 237.85 254.24 4.45 o -3 15 1 61.84 65.29 1.42 o -2 15 1 339.02 348.64 5.95 o -1 15 1 78.89 76.51 1.31 o 0 15 1 265.27 269.68 3.69 o 1 15 1 95.68 94.46 1.46 o 2 15 1 2.10 2.55 0.27 o 3 15 1 83.22 89.93 1.63 o 4 15 1 4.84 4.42 0.34 o 5 15 1 273.99 290.13 5.50 o 6 15 1 19.70 21.46 0.66 o 7 15 1 14.85 16.16 0.55 o -7 16 1 53.86 46.09 1.38 o -6 16 1 32.11 31.43 0.85 o -5 16 1 37.12 39.91 1.03 o -4 16 1 219.83 226.83 4.39 o -3 16 1 20.28 22.94 0.71 o -2 16 1 195.24 203.37 3.67 o -1 16 1 136.90 128.66 2.32 o 0 16 1 10.90 8.99 0.39 o 1 16 1 26.17 21.98 0.62 o 2 16 1 3.90 3.56 0.27 o 3 16 1 86.69 84.75 1.69 o 4 16 1 104.60 108.54 2.29 o 5 16 1 191.48 194.31 6.50 o 6 16 1 192.14 202.02 4.37 o -6 17 1 52.53 55.87 1.44 o -5 17 1 167.19 173.92 3.41 o -4 17 1 64.65 67.31 1.52 o -3 17 1 548.98 544.20 11.29 o -2 17 1 150.29 154.14 3.14 o -1 17 1 983.24 965.25 17.67 o 0 17 1 66.04 63.91 1.37 o 1 17 1 230.16 256.47 4.52 o 2 17 1 134.52 135.26 2.50 o 3 17 1 192.08 188.06 3.80 o 4 17 1 155.72 150.21 3.95 o 5 17 1 159.78 169.26 3.69 o 6 17 1 7.46 5.67 0.50 o -5 18 1 0.19 0.09 0.19 o -4 18 1 19.83 20.42 0.75 o -3 18 1 11.53 12.39 0.71 o -2 18 1 36.42 38.49 1.14 o -1 18 1 206.91 198.79 3.94 o 0 18 1 4.52 3.23 0.39 o 1 18 1 71.77 62.44 1.48 o 2 18 1 27.46 26.20 0.87 o 3 18 1 0.18 0.49 0.35 o 4 18 1 23.34 23.10 0.76 o 5 18 1 2.12 3.14 0.74 o -4 19 1 1.78 1.29 0.45 o -3 19 1 25.14 22.85 0.84 o -2 19 1 0.41 0.23 0.24 o -1 19 1 325.97 312.79 7.71 o 0 19 1 0.46 0.32 0.22 o 1 19 1 21.23 26.51 1.01 o 2 19 1 26.02 25.68 0.98 o 3 19 1 95.13 91.15 2.47 o 4 19 1 40.54 36.46 1.21 o -3 20 1 7.02 7.01 0.93 o -2 20 1 13.52 13.60 1.06 o -1 20 1 7.94 6.74 1.43 o 0 20 1 29.09 26.06 1.31 o 1 20 1 5.03 4.08 0.60 o 2 20 1 0.09 -0.30 0.39 o -11 0 2 12.95 14.77 0.76 o -10 0 2 186.99 183.14 4.09 o -9 0 2 41.12 42.85 1.47 o -7 0 2 178.42 177.24 5.60 o -5 0 2 272.12 240.02 5.08 o -4 0 2 3075.17 2839.50 80.99 o -3 0 2 598.88 647.58 18.56 o -2 0 2 1607.11 1987.19 139.57 o -1 0 2 455.12 538.32 21.68 o 1 0 2 1408.46 1642.73 80.95 o 3 0 2 116.39 147.05 4.44 o 5 0 2 33.76 32.85 0.80 o 6 0 2 2344.11 2294.56 41.41 o 7 0 2 982.82 936.16 17.07 o 8 0 2 478.24 480.09 9.98 o 9 0 2 162.14 164.79 3.60 o 10 0 2 0.66 1.56 0.38 o -11 1 2 74.30 74.63 1.47 o -10 1 2 256.79 252.49 4.99 o -9 1 2 258.43 252.77 4.17 o -8 1 2 6.93 7.94 0.50 o -7 1 2 236.06 231.03 3.51 o -6 1 2 1387.01 1444.63 22.09 o -5 1 2 108.88 92.34 1.72 o -4 1 2 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