#------------------------------------------------------------------------------ #$Date: 2023-12-06 17:35:49 +0200 (Wed, 06 Dec 2023) $ #$Revision: 288090 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/94/4519479.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519479 _cell_angle_alpha 90.000 _cell_angle_beta 90.497 _cell_angle_gamma 90.000 _cell_length_a 9.3639 _cell_length_b 8.0701 _cell_length_c 10.3114 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.8004 _cod_data_source_file H4BTA_SO4_2HSO4.fcf _cod_data_source_block jw24791 _shelx_title ' jw24791_c.res in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.20 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 372.73 346.37 8.31 o 2 0 0 8731.29 8173.99 234.23 o 3 0 0 2513.90 2406.17 87.62 o 4 0 0 4993.65 4639.56 77.84 o 5 0 0 50.47 49.24 2.05 o 6 0 0 109.37 107.02 4.18 o 7 0 0 754.96 771.14 16.64 o 8 0 0 7093.11 7312.07 336.54 o 9 0 0 8.81 9.82 0.52 o 10 0 0 42.91 41.72 1.54 o 11 0 0 284.69 267.39 5.95 o 0 1 0 8.68 16.74 0.65 o 1 1 0 2019.27 1668.35 54.31 o 2 1 0 12223.92 11982.20 734.30 o 3 1 0 121.52 118.08 1.84 o 4 1 0 26.41 28.77 0.47 o 5 1 0 3107.38 3018.09 96.65 o 6 1 0 2938.65 2683.94 64.23 o 7 1 0 98.86 93.00 1.30 o 8 1 0 1.06 0.96 0.11 o 9 1 0 600.69 596.08 6.98 o 10 1 0 438.85 434.33 5.88 o 11 1 0 3.47 3.28 0.31 o 0 2 0 10110.85 10098.50 211.03 o 1 2 0 1549.89 1284.82 48.04 o 2 2 0 39.14 55.09 0.93 o 3 2 0 1033.00 1001.55 115.53 o 4 2 0 143.15 182.74 5.42 o 5 2 0 64.77 78.08 1.27 o 6 2 0 47.09 34.78 0.59 o 7 2 0 1019.08 1046.07 19.48 o 8 2 0 1435.46 1536.09 29.96 o 9 2 0 16.29 20.47 0.43 o 10 2 0 33.10 32.64 0.77 o 11 2 0 361.34 392.60 6.02 o 0 3 0 12513.40 13093.72 531.36 o 1 3 0 3.10 4.88 0.29 o 2 3 0 4213.42 3706.37 113.74 o 3 3 0 1130.37 1215.17 50.25 o 4 3 0 1970.88 2562.99 235.90 o 5 3 0 155.42 154.90 2.50 o 6 3 0 1653.71 1773.50 77.08 o 7 3 0 9.05 6.54 0.21 o 8 3 0 1111.68 1104.41 17.55 o 9 3 0 99.08 91.55 1.03 o 10 3 0 228.91 195.41 2.85 o 11 3 0 14.58 16.62 0.75 o 0 4 0 451.66 373.14 13.71 o 1 4 0 123.02 130.43 2.42 o 2 4 0 1548.35 1952.89 120.08 o 3 4 0 7.23 6.42 0.15 o 4 4 0 1366.78 1444.89 41.27 o 5 4 0 394.75 388.25 4.54 o 6 4 0 516.29 520.52 5.46 o 7 4 0 713.40 677.49 7.69 o 8 4 0 59.60 69.54 0.87 o 9 4 0 22.94 27.47 0.48 o 10 4 0 21.02 18.18 0.39 o 0 5 0 2074.65 1958.52 45.71 o 1 5 0 5.53 5.63 0.19 o 2 5 0 833.86 924.40 46.58 o 3 5 0 126.15 126.87 1.52 o 4 5 0 140.44 137.40 1.99 o 5 5 0 410.90 420.06 4.79 o 6 5 0 168.95 182.14 2.14 o 7 5 0 290.02 317.56 3.66 o 8 5 0 64.66 60.02 0.80 o 9 5 0 117.73 109.68 1.56 o 10 5 0 11.40 11.21 0.34 o 0 6 0 835.38 997.64 47.74 o 1 6 0 138.02 128.92 1.61 o 2 6 0 317.99 350.80 3.89 o 3 6 0 50.26 52.48 0.63 o 4 6 0 3404.26 3003.99 161.82 o 5 6 0 52.96 50.40 0.68 o 6 6 0 92.51 98.55 1.18 o 7 6 0 81.92 69.99 0.93 o 8 6 0 65.62 61.28 0.89 o 9 6 0 41.63 45.25 1.24 o 0 7 0 3.95 2.67 0.21 o 1 7 0 49.80 40.60 0.53 o 2 7 0 289.37 283.58 3.27 o 3 7 0 114.16 105.62 1.32 o 4 7 0 338.73 344.66 3.75 o 5 7 0 53.87 50.30 0.68 o 6 7 0 140.19 140.58 2.08 o 7 7 0 36.08 44.48 0.67 o 8 7 0 10.75 17.45 0.40 o 0 8 0 118.68 100.19 1.67 o 1 8 0 296.55 267.10 2.94 o 2 8 0 263.48 258.41 2.92 o 3 8 0 119.91 130.49 1.61 o 4 8 0 20.18 18.05 0.45 o 5 8 0 52.61 40.20 0.60 o 6 8 0 53.03 51.09 0.78 o 7 8 0 125.03 132.23 2.35 o 0 9 0 52.88 53.57 1.07 o 1 9 0 71.25 65.06 0.92 o 2 9 0 142.07 142.29 1.90 o 3 9 0 166.08 165.55 2.14 o 4 9 0 53.31 55.80 0.81 o 5 9 0 58.22 57.25 1.23 o 0 10 0 90.09 103.46 2.87 o 1 10 0 0.38 0.74 0.33 o -11 1 1 30.64 28.46 0.62 o -10 1 1 18.64 19.70 0.58 o -9 1 1 0.12 0.21 0.06 o -8 1 1 0.06 1.02 0.17 o -7 1 1 196.27 193.86 2.48 o -6 1 1 6.63 7.75 0.33 o -5 1 1 12.60 12.26 0.25 o -4 1 1 2013.82 2002.57 54.35 o -3 1 1 1398.80 1184.54 42.13 o -2 1 1 110.32 112.16 2.66 o -1 1 1 166.12 140.01 5.88 o 0 1 1 320.59 252.12 13.07 o 1 1 1 27.34 23.28 0.44 o 2 1 1 49.98 49.57 0.76 o 3 1 1 1144.57 1245.31 62.79 o 4 1 1 1845.42 2321.35 99.79 o 5 1 1 4.99 4.01 0.18 o 6 1 1 0.27 0.41 0.10 o 7 1 1 342.36 346.36 4.16 o 8 1 1 5.63 7.26 0.23 o 9 1 1 11.30 11.41 0.30 o 10 1 1 27.22 24.51 0.55 o 11 1 1 40.71 38.15 0.82 o -11 2 1 11.09 10.45 0.41 o -10 2 1 64.79 66.78 1.11 o -9 2 1 55.21 57.91 0.96 o -8 2 1 27.97 30.03 0.50 o -7 2 1 12.19 12.27 0.32 o -6 2 1 557.47 596.70 11.75 o -5 2 1 1329.76 1112.33 34.91 o -4 2 1 33.88 28.15 0.65 o -3 2 1 847.96 844.12 43.76 o -2 2 1 3454.11 3972.92 100.34 o -1 2 1 0.74 0.98 0.08 o 0 2 1 110.10 90.37 1.97 o 1 2 1 271.47 305.75 9.52 o 2 2 1 2903.44 3173.70 75.94 o 3 2 1 875.68 1133.30 44.30 o 4 2 1 82.11 69.83 1.89 o 5 2 1 1090.93 1233.43 39.63 o 6 2 1 654.63 685.64 12.35 o 7 2 1 55.98 52.51 0.78 o 8 2 1 7.53 8.46 0.27 o 9 2 1 129.07 130.14 1.64 o 10 2 1 40.27 39.32 0.63 o 11 2 1 10.33 9.40 0.43 o -11 3 1 125.34 128.62 2.44 o -10 3 1 0.37 0.71 0.13 o -9 3 1 4.75 6.55 0.26 o -8 3 1 45.51 47.48 0.83 o -7 3 1 63.56 66.76 0.96 o -6 3 1 55.17 47.81 0.76 o -5 3 1 121.20 140.77 2.23 o -4 3 1 3951.29 4059.45 61.42 o -3 3 1 639.90 541.45 46.91 o -2 3 1 7.72 11.74 0.23 o -1 3 1 465.39 487.04 12.47 o 0 3 1 233.50 316.32 9.05 o 1 3 1 52.28 48.04 0.80 o 2 3 1 109.45 131.50 1.87 o 3 3 1 381.97 414.04 8.85 o 4 3 1 3480.31 3115.72 131.07 o 5 3 1 217.34 242.15 3.27 o 6 3 1 46.81 44.61 0.63 o 7 3 1 155.92 157.31 1.97 o 8 3 1 9.92 15.12 0.26 o 9 3 1 2.49 1.93 0.15 o 10 3 1 6.56 6.09 0.25 o 11 3 1 80.85 79.18 1.34 o -10 4 1 165.74 169.11 2.35 o -9 4 1 40.08 44.00 0.63 o -8 4 1 35.96 32.39 0.47 o -7 4 1 1.44 1.82 0.12 o -6 4 1 465.71 496.22 4.97 o -5 4 1 226.65 236.32 2.65 o -4 4 1 172.84 175.80 2.55 o -3 4 1 455.17 477.11 28.12 o -2 4 1 675.30 509.84 23.98 o -1 4 1 201.41 241.49 4.52 o 0 4 1 39.90 63.11 0.93 o 1 4 1 34.38 35.38 0.62 o 2 4 1 395.52 375.57 12.80 o 3 4 1 357.35 424.65 12.39 o 4 4 1 74.57 71.55 0.99 o 5 4 1 207.13 226.90 2.54 o 6 4 1 416.29 433.97 4.68 o 7 4 1 68.17 69.79 0.86 o 8 4 1 2.12 1.73 0.15 o 9 4 1 141.95 161.16 1.98 o 10 4 1 103.28 110.23 1.37 o -10 5 1 25.62 22.95 0.65 o -9 5 1 13.33 14.50 0.31 o -8 5 1 89.32 96.81 1.13 o -7 5 1 18.60 21.41 0.34 o -6 5 1 341.96 338.27 3.52 o -5 5 1 8.45 6.00 0.16 o -4 5 1 1736.86 1425.37 39.96 o -3 5 1 180.29 165.93 2.02 o -2 5 1 593.36 563.13 15.65 o -1 5 1 20.70 24.10 0.42 o 0 5 1 276.27 225.02 3.65 o 1 5 1 110.13 119.32 1.65 o 2 5 1 608.11 598.30 28.73 o 3 5 1 342.91 354.81 4.59 o 4 5 1 1873.48 1553.04 39.91 o 5 5 1 43.22 39.41 0.56 o 6 5 1 263.42 261.08 3.22 o 7 5 1 118.56 136.23 1.65 o 8 5 1 75.28 81.26 1.13 o 9 5 1 56.75 54.62 0.80 o 10 5 1 17.53 16.79 0.51 o -9 6 1 124.06 125.96 2.03 o -8 6 1 59.00 57.21 0.99 o -7 6 1 32.92 29.40 0.47 o -6 6 1 359.42 375.22 4.30 o -5 6 1 228.32 227.02 2.72 o -4 6 1 776.35 824.63 11.39 o -3 6 1 155.06 145.15 1.63 o -2 6 1 1478.91 1429.38 68.21 o -1 6 1 55.30 51.46 0.66 o 0 6 1 804.53 839.10 18.23 o 1 6 1 170.78 165.74 2.11 o 2 6 1 1394.49 1486.01 71.01 o 3 6 1 95.98 83.44 1.03 o 4 6 1 715.71 738.38 11.21 o 5 6 1 198.72 206.66 2.36 o 6 6 1 285.42 296.37 3.63 o 7 6 1 81.08 78.50 1.07 o 8 6 1 13.67 14.35 0.33 o 9 6 1 186.00 196.51 2.81 o -8 7 1 219.63 230.53 3.43 o -7 7 1 73.81 71.32 1.27 o -6 7 1 140.74 131.03 1.68 o -5 7 1 13.35 11.34 0.26 o -4 7 1 569.45 578.32 7.90 o -3 7 1 203.05 191.18 2.24 o -2 7 1 303.29 302.97 3.59 o -1 7 1 26.45 26.46 0.40 o 0 7 1 1070.80 1147.12 54.94 o 1 7 1 3.60 4.96 0.19 o 2 7 1 403.00 407.88 5.33 o 3 7 1 398.00 389.30 4.58 o 4 7 1 495.51 516.14 6.61 o 5 7 1 69.67 61.65 0.81 o 6 7 1 55.82 50.23 0.77 o 7 7 1 176.77 173.53 2.31 o 8 7 1 104.55 114.60 1.62 o -7 8 1 68.70 76.84 1.24 o -6 8 1 395.44 398.35 5.36 o -5 8 1 16.89 16.49 0.32 o -4 8 1 144.62 138.10 1.71 o -3 8 1 14.75 15.53 0.39 o -2 8 1 635.60 661.07 7.72 o -1 8 1 107.17 105.49 1.26 o 0 8 1 12.39 14.52 0.29 o 1 8 1 452.65 457.26 5.22 o 2 8 1 684.64 722.27 9.28 o 3 8 1 16.07 13.62 0.31 o 4 8 1 167.82 164.87 2.14 o 5 8 1 109.83 106.62 1.53 o 6 8 1 295.21 289.48 3.65 o 7 8 1 3.37 4.25 0.21 o -5 9 1 38.57 36.62 0.65 o -4 9 1 411.44 412.53 5.15 o -3 9 1 98.43 93.01 1.26 o -2 9 1 12.50 14.82 0.35 o -1 9 1 135.13 139.31 1.89 o 0 9 1 781.05 839.21 10.78 o 1 9 1 78.13 79.24 1.06 o 2 9 1 15.48 16.75 0.33 o 3 9 1 117.60 109.61 1.41 o 4 9 1 316.99 307.88 4.02 o 5 9 1 25.96 23.84 0.51 o -1 10 1 148.56 136.68 2.31 o 0 10 1 0.46 0.22 0.07 o 1 10 1 213.65 212.88 4.26 o -11 0 2 132.52 129.50 4.87 o -10 0 2 7.62 7.12 0.66 o -9 0 2 9.44 6.40 0.44 o -8 0 2 398.85 414.15 8.26 o -7 0 2 3458.46 3255.63 43.51 o -6 0 2 6.22 7.12 0.37 o -5 0 2 21.03 19.09 0.53 o -4 0 2 26.18 44.44 1.32 o -3 0 2 17.72 31.40 0.99 o -2 0 2 30.70 51.19 0.87 o -1 0 2 8719.99 8983.83 467.28 o 0 0 2 3244.76 4267.98 292.89 o 1 0 2 4831.56 5796.24 515.33 o 2 0 2 2.80 6.11 0.22 o 3 0 2 6169.70 7567.80 534.36 o 4 0 2 198.75 242.81 5.95 o 5 0 2 2792.14 3086.06 148.77 o 6 0 2 50.69 60.08 1.93 o 7 0 2 3614.32 3381.23 195.09 o 8 0 2 142.10 130.37 2.64 o 9 0 2 1.55 0.82 0.18 o 10 0 2 12.92 10.91 0.60 o 11 0 2 417.86 420.29 11.67 o -11 1 2 0.04 0.23 0.11 o -10 1 2 612.36 612.86 8.53 o -9 1 2 634.84 671.09 10.78 o -8 1 2 832.50 876.71 12.70 o -7 1 2 473.71 488.83 6.52 o -6 1 2 1694.95 1388.99 34.81 o -5 1 2 131.86 176.65 2.60 o -4 1 2 2.49 1.38 0.08 o -3 1 2 1020.46 1169.30 76.06 o -2 1 2 7568.41 8750.70 523.28 o -1 1 2 3732.89 4211.58 227.34 o 0 1 2 11282.83 13038.56 699.87 o 1 1 2 7551.49 8404.41 679.34 o 2 1 2 5217.88 6191.70 473.78 o 3 1 2 2291.64 2321.03 68.90 o 4 1 2 108.61 136.74 2.42 o 5 1 2 1658.22 1662.98 59.51 o 6 1 2 968.01 946.64 22.18 o 7 1 2 174.29 151.92 2.11 o 8 1 2 422.25 429.58 5.43 o 9 1 2 567.58 570.82 7.57 o 10 1 2 210.73 203.48 2.83 o 11 1 2 113.68 113.12 1.76 o -11 2 2 1.29 3.17 0.26 o -10 2 2 119.68 109.51 1.78 o -9 2 2 24.24 24.55 0.49 o -8 2 2 1938.58 2183.86 73.51 o -7 2 2 301.70 298.78 3.76 o -6 2 2 200.98 207.55 3.09 o -5 2 2 625.21 678.35 18.76 o -4 2 2 2574.65 2192.04 71.56 o -3 2 2 2994.50 3168.39 59.85 o -2 2 2 471.69 470.20 29.37 o -1 2 2 3524.43 4080.81 90.12 o 0 2 2 11597.81 13156.86 430.58 o 1 2 2 413.63 390.13 15.12 o 2 2 2 4.81 1.39 0.09 o 3 2 2 325.48 296.18 6.40 o 4 2 2 1211.37 1176.24 34.94 o 5 2 2 393.47 445.24 8.73 o 6 2 2 51.03 39.83 0.60 o 7 2 2 517.46 540.66 6.71 o 8 2 2 1205.95 1208.10 29.07 o 9 2 2 7.47 8.01 0.34 o 10 2 2 2.22 2.96 0.25 o 11 2 2 74.83 68.85 1.20 o -11 3 2 11.36 16.89 0.43 o -10 3 2 231.73 224.65 2.85 o -9 3 2 124.48 129.02 1.63 o -8 3 2 0.36 0.58 0.11 o -7 3 2 65.91 58.34 0.83 o -6 3 2 558.38 545.93 7.93 o -5 3 2 4.23 2.69 0.22 o -4 3 2 702.36 740.13 35.30 o -3 3 2 1321.93 1337.42 63.49 o -2 3 2 348.71 310.33 6.06 o -1 3 2 453.10 533.49 13.53 o 0 3 2 1755.75 1661.30 69.63 o 1 3 2 320.74 283.80 7.94 o 2 3 2 19.47 26.28 0.54 o 3 3 2 343.59 377.82 9.17 o 4 3 2 1593.92 1395.63 62.53 o 5 3 2 1359.06 1440.73 51.45 o 6 3 2 451.28 425.59 4.60 o 7 3 2 188.15 164.75 1.84 o 8 3 2 32.89 29.32 0.88 o 9 3 2 221.06 228.38 2.86 o 10 3 2 41.34 38.27 0.62 o 11 3 2 93.79 110.64 2.34 o -10 4 2 22.29 18.24 0.54 o -9 4 2 1.94 2.63 0.14 o -8 4 2 618.50 569.09 5.97 o -7 4 2 66.06 79.74 0.91 o -6 4 2 12.54 15.03 0.27 o -5 4 2 318.81 326.10 3.72 o -4 4 2 1086.41 839.25 36.65 o -3 4 2 17.13 26.02 0.51 o -2 4 2 418.44 417.69 10.00 o -1 4 2 468.18 433.30 15.48 o 0 4 2 2969.79 2762.82 98.54 o 1 4 2 79.71 101.51 1.46 o 2 4 2 1.69 4.64 0.21 o 3 4 2 1043.26 829.38 28.98 o 4 4 2 512.70 528.53 8.47 o 5 4 2 24.98 32.25 0.44 o 6 4 2 17.65 18.31 0.40 o 7 4 2 272.72 313.55 3.85 o 8 4 2 404.07 380.16 4.78 o 9 4 2 39.37 39.00 0.62 o 10 4 2 23.26 23.92 0.51 o -10 5 2 125.61 106.26 2.19 o -9 5 2 3.54 3.08 0.18 o -8 5 2 11.54 16.68 0.29 o -7 5 2 21.09 16.19 0.27 o -6 5 2 440.86 453.04 4.77 o -5 5 2 631.89 644.93 7.49 o -4 5 2 649.24 665.09 12.05 o -3 5 2 1993.30 1731.46 50.92 o -2 5 2 2080.22 2134.30 101.69 o -1 5 2 432.18 474.76 13.14 o 0 5 2 533.36 523.73 14.52 o 1 5 2 39.01 31.17 0.57 o 2 5 2 867.54 943.21 53.50 o 3 5 2 317.62 320.05 4.14 o 4 5 2 411.38 432.44 5.61 o 5 5 2 1622.06 1676.74 76.49 o 6 5 2 598.90 631.29 8.44 o 7 5 2 162.39 146.55 1.82 o 8 5 2 0.41 0.97 0.13 o 9 5 2 23.45 25.63 0.46 o -9 6 2 6.36 6.28 0.32 o -8 6 2 3.56 6.67 0.28 o -7 6 2 31.87 26.98 0.47 o -6 6 2 93.13 80.80 1.02 o -5 6 2 327.43 329.41 3.78 o -4 6 2 39.15 35.59 0.84 o -3 6 2 483.98 490.45 6.64 o -2 6 2 40.74 36.48 0.51 o -1 6 2 224.92 211.91 2.39 o 0 6 2 32.42 32.58 0.53 o 1 6 2 53.59 54.00 0.74 o 2 6 2 348.91 343.21 4.15 o 3 6 2 1492.68 1697.95 46.90 o 4 6 2 105.20 101.56 1.59 o 5 6 2 20.54 23.77 0.44 o 6 6 2 23.98 21.00 0.44 o 7 6 2 161.75 140.90 1.99 o 8 6 2 1.59 1.30 0.19 o 9 6 2 14.55 13.56 0.34 o -8 7 2 22.75 26.15 0.68 o -7 7 2 6.84 6.01 0.24 o -6 7 2 9.39 10.59 0.28 o -5 7 2 68.78 65.44 0.85 o -4 7 2 1.06 0.73 0.09 o -3 7 2 1067.30 1085.76 19.59 o -2 7 2 28.08 29.04 0.51 o -1 7 2 212.46 185.65 2.13 o 0 7 2 244.86 199.33 2.47 o 1 7 2 7.47 9.04 0.28 o 2 7 2 25.08 25.36 0.43 o 3 7 2 343.85 337.90 3.88 o 4 7 2 19.48 18.27 0.35 o 5 7 2 230.77 235.38 2.82 o 6 7 2 8.09 7.13 0.26 o 7 7 2 14.22 15.78 0.35 o 8 7 2 53.22 63.60 1.13 o -6 8 2 1.82 1.35 0.14 o -5 8 2 138.90 135.56 1.67 o -4 8 2 148.92 138.92 1.72 o -3 8 2 26.77 24.46 0.41 o -2 8 2 17.38 15.53 0.31 o -1 8 2 62.80 62.45 0.82 o 0 8 2 96.33 84.89 1.13 o 1 8 2 40.01 36.30 0.56 o 2 8 2 95.20 85.85 1.12 o 3 8 2 24.77 26.92 0.45 o 4 8 2 81.24 81.11 1.11 o 5 8 2 18.39 16.73 0.36 o 6 8 2 0.67 0.39 0.10 o -4 9 2 352.25 369.30 5.22 o -3 9 2 0.93 0.20 0.12 o -2 9 2 15.28 15.26 0.50 o -1 9 2 23.15 17.70 0.38 o 0 9 2 368.51 346.27 4.22 o 1 9 2 15.42 16.32 0.32 o 2 9 2 42.88 41.41 0.60 o 3 9 2 31.89 42.66 0.67 o 4 9 2 352.63 355.86 4.78 o -11 1 3 0.85 0.85 0.14 o -10 1 3 4.80 4.91 0.23 o -9 1 3 5.38 4.34 0.20 o -8 1 3 4.75 5.71 0.24 o -7 1 3 1.70 2.01 0.14 o -6 1 3 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