Crystallography Open Database

Information card for entry 7001681

Preview

Coordinates	7001681.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H116 Hf2 N8 O89 P2 W22
Calculated formula	C24 Hf2 N6 O89 P2 W22
Title of publication	Synthesis and structure of dinuclear hafnium(IV) and zirconium(IV) complexes sandwiched between 2 mono-lacunary α-Keggin polyoxometalates
Authors of publication	Nomiya, Kenji; Saku, Yoshio; Yamada, Shingo; Takahashi, Wataru; Sekiya, Hiromi; Shinohara, Akira; Ishimaru, Megumi; Sakai, Yoshitaka
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	28
Pages of publication	5504 - 5511
a	11.796 ± 0.0014 Å
b	20.774 ± 0.003 Å
c	23.084 ± 0.003 Å
α	78.921 ± 0.002°
β	79.47 ± 0.002°
γ	88.6 ± 0.002°
Cell volume	5457.5 ± 1.2 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1053
Residual factor for significantly intense reflections	0.0674
Weighted residual factors for significantly intense reflections	0.1834
Weighted residual factors for all reflections included in the refinement	0.2221
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179714 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/16.	7001681.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7001681.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7001681.cif
1143	2010-05-03	cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition.	7001681.cif