Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7002654
Preview
| Coordinates | 7002654.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | 1-chloro-3-triflouromethanesolfonato-2,4- bis(tris(trimethylsilyl)silyl)-cyclo-1,3-diphospha-2,4-diazane |
|---|---|
| Chemical name | 1-chloro-3-triflouromethanesolfonato-2,4-bis[tris(trimethylsilyl)silyl]-cyclo- 1,3-diphospha-2,4-diazane |
| Formula | C19 H54 Cl F3 N2 O3 P2 S Si8 |
| Calculated formula | C19 H54 Cl F3 N2 O3 P2 S Si8 |
| Title of publication | Hypersilylated cyclodiphosphadiazanes and cyclodiphosphadiazenium salts |
| Authors of publication | Kuzora, René; Schulz, Axel; Villinger, Alexander; Wustrack, Ronald |
| Journal of publication | Dalton Transactions |
| Year of publication | 2009 |
| Journal issue | 42 |
| Pages of publication | 9304 |
| a | 18.508 ± 0.004 Å |
| b | 13.008 ± 0.003 Å |
| c | 18.329 ± 0.004 Å |
| α | 90° |
| β | 108.4 ± 0.03° |
| γ | 90° |
| Cell volume | 4187.1 ± 1.8 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 9 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0617 |
| Residual factor for significantly intense reflections | 0.0494 |
| Weighted residual factors for significantly intense reflections | 0.1306 |
| Weighted residual factors for all reflections included in the refinement | 0.1371 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179730 (current) | 2016-03-25 | cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/26. |
7002654.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7002654.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7002654.cif |
| 1143 | 2010-05-03 | cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition. |
7002654.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.