Crystallography Open Database

Information card for entry 7003255

Preview

Coordinates	7003255.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C61 H88 Cl4 O14 P Si7 V
Calculated formula	C60.99 H86 Cl4 O14 P Si7 V
Title of publication	V2O5/SiO2 surface inspired, silsesquioxane-derived oxovanadium complexes and their properties
Authors of publication	Ohde, Christian; Brandt, Marcus; Limberg, Christian; Döbler, Jens; Ziemer, Burckhard; Sauer, Joachim
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	3
Pages of publication	326
a	10.292 ± 0.003 Å
b	14.543 ± 0.004 Å
c	24.244 ± 0.006 Å
α	87.33 ± 0.03°
β	88.66 ± 0.03°
γ	85.85 ± 0.03°
Cell volume	3614.6 ± 1.7 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2055
Residual factor for significantly intense reflections	0.1085
Weighted residual factors for significantly intense reflections	0.2673
Weighted residual factors for all reflections included in the refinement	0.3183
Goodness-of-fit parameter for all reflections included in the refinement	0.913
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179736 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/32.	7003255.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7003255.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7003255.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7003255.cif