Crystallography Open Database

Information card for entry 7003280

Preview

Coordinates	7003280.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H47 N3 Na P Si2
Calculated formula	C25 H47 N3 Na P Si2
SMILES	P1([Na]2([N](c5cccc4cccc1c54)(C)C)[N](C)(C)CC[N]2(C)C)C([Si](C)(C)C)[Si](C)(C)C
Title of publication	Alkali metal complexes of a naphthylamine-substituted phosphanide
Authors of publication	Izod, Keith; Stewart, John C.; Clegg, William; Harrington, Ross W.
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	3
Pages of publication	363
a	9.795 ± 0.003 Å
b	26.617 ± 0.009 Å
c	12.301 ± 0.004 Å
α	90°
β	108.43 ± 0.005°
γ	90°
Cell volume	3042.5 ± 1.7 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1079
Residual factor for significantly intense reflections	0.0894
Weighted residual factors for significantly intense reflections	0.2263
Weighted residual factors for all reflections included in the refinement	0.2461
Goodness-of-fit parameter for all reflections included in the refinement	1.108
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179736 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/32.	7003280.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7003280.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7003280.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7003280.cif