Crystallography Open Database

Information card for entry 7003431

Preview

Coordinates	7003431.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H34 Cl10 N4 Ni2 O4
Calculated formula	C27 H34 Cl10 N4 Ni2 O4
Title of publication	Synthesis of nickel complexes with bidentate N,O-type ligands and application in the catalytic oligomerization of ethylene
Authors of publication	Kermagoret, Anthony; Braunstein, Pierre
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	12
Pages of publication	1564 - 1573
a	10.226 ± 0.0002 Å
b	11.526 ± 0.0002 Å
c	17.08 ± 0.0005 Å
α	89.15 ± 0.001°
β	77.95 ± 0.001°
γ	74.3 ± 0.001°
Cell volume	1893.47 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1362
Residual factor for significantly intense reflections	0.0855
Weighted residual factors for significantly intense reflections	0.2018
Weighted residual factors for all reflections included in the refinement	0.2302
Goodness-of-fit parameter for all reflections included in the refinement	0.932
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179738 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/34.	7003431.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7003431.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7003431.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7003431.cif