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Information card for entry 7003521
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| Coordinates | 7003521.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | (2-(dimethylphosphinoyl)ethyl)-hydroxy-dimethylphosphonium trichloridogermanate(ii) |
|---|---|
| Chemical name | (2-(dimethylphosphinoyl)ethyl)-hydroxy-dimethylphosphonium trichloridogermanate(II) |
| Formula | C6 H17 Cl3 Ge O2 P2 |
| Calculated formula | C6 H17 Cl3 Ge O2 P2 |
| SMILES | [Ge](Cl)(Cl)[Cl-].P(=O)(C)(C)CC[P+](O)(C)C |
| Title of publication | Complexes of germanium(iv) fluoride with phosphane ligands: structural and spectroscopic authentication of germanium(iv) phosphane complexes |
| Authors of publication | Davis, Martin F.; Levason, William; Reid, Gillian; Webster, Michael |
| Journal of publication | Dalton Transactions |
| Year of publication | 2008 |
| Journal issue | 17 |
| Pages of publication | 2261 - 2269 |
| a | 9.0978 ± 0.0015 Å |
| b | 9.2599 ± 0.0015 Å |
| c | 11.1713 ± 0.0015 Å |
| α | 66.397 ± 0.01° |
| β | 89.283 ± 0.01° |
| γ | 60.695 ± 0.01° |
| Cell volume | 731.9 ± 0.2 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0358 |
| Residual factor for significantly intense reflections | 0.0281 |
| Weighted residual factors for significantly intense reflections | 0.0555 |
| Weighted residual factors for all reflections included in the refinement | 0.059 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.088 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179739 (current) | 2016-03-25 | cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/35. |
7003521.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7003521.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7003521.cif |
| 1173 | 2010-05-16 | cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing. | 7003521.cif |
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