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Information card for entry 7003527
Preview
| Coordinates | 7003527.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | ((tmeda)Li(Me3SiNCPhCHC(NSiMe3)C6H4C(NSiMe3)NCPhCHSiMe3)Li(tmeda)) |
|---|---|
| Formula | C48 H84 Li2 N8 Si4 |
| Calculated formula | C48 H84 Li2 N8 Si4 |
| SMILES | [Li]12([N]([Si](C)(C)C)=C(C=C(N1[Si](C)(C)C)c1cc(ccc1)C1=[N]([Li]3(N1C(=C[Si](C)(C)C)c1ccccc1)[N](CC[N]3(C)C)(C)C)[Si](C)(C)C)c1ccccc1)[N](CC[N]2(C)C)(C)C |
| Title of publication | Synthesis and structures of some new types of lithium β-diketiminates |
| Authors of publication | Wei, Xue-Hong; Farwell, James D.; Hitchcock, Peter B.; Lappert, Michael F. |
| Journal of publication | Dalton Transactions |
| Year of publication | 2008 |
| Journal issue | 8 |
| Pages of publication | 1073 - 1080 |
| a | 18.5001 ± 0.0003 Å |
| b | 14.7798 ± 0.0003 Å |
| c | 21.7209 ± 0.0005 Å |
| α | 90° |
| β | 98.215 ± 0.001° |
| γ | 90° |
| Cell volume | 5878.2 ± 0.2 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0819 |
| Residual factor for significantly intense reflections | 0.0605 |
| Weighted residual factors for significantly intense reflections | 0.1424 |
| Weighted residual factors for all reflections included in the refinement | 0.1577 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179739 (current) | 2016-03-25 | cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/35. |
7003527.cif |
| 171654 | 2015-12-20 | cod/ (antanas@echidna.ibt.lt) Removing surrounding qoutes ("'") from the _chemical_name_common tag values in multiple entries in ranges 7, 8. |
7003527.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7003527.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7003527.cif |
| 1173 | 2010-05-16 | cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing. | 7003527.cif |
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