Crystallography Open Database

Information card for entry 7004962

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Coordinates	7004962.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H52 Ga2
Calculated formula	C30 H52 Ga2
Title of publication	The reactions of dialkylgallium hydrides with tert-butylethynylbenzenes‒a systematic investigation into the course of hydrogallation reactions.
Authors of publication	Uhl, Werner; Claesener, Michael; Haddadpour, Sima; Jasper, Beate; Hepp, Alexander
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	4
Pages of publication	417 - 423
a	27.889 ± 0.008 Å
b	12.053 ± 0.003 Å
c	19.249 ± 0.005 Å
α	90°
β	111.919 ± 0.006°
γ	90°
Cell volume	6003 ± 3 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	3
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.2311
Residual factor for significantly intense reflections	0.0857
Weighted residual factors for significantly intense reflections	0.1384
Weighted residual factors for all reflections included in the refinement	0.1841
Goodness-of-fit parameter for all reflections included in the refinement	0.944
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179753 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/49.	7004962.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7004962.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7004962.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7004962.cif