Crystallography Open Database

Information card for entry 7005703

Preview

Coordinates	7005703.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H22 Cl3 N O2 Si2 Ti
Calculated formula	C14 H22 Cl3 N O2 Si2 Ti
SMILES	[Ti](Cl)(Cl)(Cl)N([Si](c1oc(C)cc1)(C)C)[Si](C)(C)c1oc(cc1)C
Title of publication	Deactivation pathways of ethylene polymerization catalysts derived from titanium and zirconium 1,3-bis(furyl)-1,1,3,3-tetramethyldisilazide complexes.
Authors of publication	Evans, Lloyd T. J.; Coles, Martyn P.; Geoffrey, F.; Cloke, N.; Hitchcock, Peter B.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	25
Pages of publication	2707 - 2717
a	27.1916 ± 0.0004 Å
b	11.2759 ± 0.0002 Å
c	29.9679 ± 0.0004 Å
α	90°
β	110.992 ± 0.001°
γ	90°
Cell volume	8578.6 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0673
Residual factor for significantly intense reflections	0.0397
Weighted residual factors for significantly intense reflections	0.0818
Weighted residual factors for all reflections included in the refinement	0.0917
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179761 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/57.	7005703.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7005703.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7005703.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7005703.cif