Crystallography Open Database

Information card for entry 7005991

Preview

Coordinates	7005991.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H70 N2 O Pb
Calculated formula	C50 H70 N2 O Pb
Title of publication	The synthesis of monomeric terminal lead aryloxides: dependence on reagents and conditions.
Authors of publication	Fulton, J. Robin; Hitchcock, Peter B.; Johnstone, Nick C.; Tam, Eric C. Y.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	31
Pages of publication	3360 - 3362
a	34.4733 ± 0.0012 Å
b	12.0183 ± 0.0004 Å
c	26.7006 ± 0.0008 Å
α	90°
β	123.008 ± 0.002°
γ	90°
Cell volume	9276.8 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0509
Residual factor for significantly intense reflections	0.0393
Weighted residual factors for significantly intense reflections	0.0871
Weighted residual factors for all reflections included in the refinement	0.0927
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179763 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/59.	7005991.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7005991.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7005991.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7005991.cif