Crystallography Open Database

Information card for entry 7006387

Preview

Coordinates	7006387.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	tris-((mu2-(1R,4R)-1,7,7-trimethylbicyclo(2.2.1)heptane-2-one oximato-O)dimethylaluminium)
Formula	C36 H66 Al3 N3 O3
Calculated formula	C36 H66 Al3 N3 O3
Title of publication	Organoaluminium complexes with sterically demanding oximato ligands: does a bulky and rigid ligand backbone change the aggregation motif?
Authors of publication	Ullrich, Matthias; Mitzel, Norbert W.; Bergander, Klaus; Fröhlich, Roland
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2006
Journal issue	5
Pages of publication	714 - 721
a	13.7886 ± 0.0013 Å
b	20.1732 ± 0.0019 Å
c	14.6935 ± 0.0014 Å
α	90°
β	97.182 ± 0.002°
γ	90°
Cell volume	4055.1 ± 0.7 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.1141
Residual factor for significantly intense reflections	0.0794
Weighted residual factors for significantly intense reflections	0.1566
Weighted residual factors for all reflections included in the refinement	0.1713
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179767 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/63.	7006387.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7006387.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7006387.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7006387.cif