Crystallography Open Database

Information card for entry 7006427

Preview

Coordinates	7006427.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H51 F3 O4 P4 Ru
Calculated formula	C47 H51 F3 O4 P4 Ru
Title of publication	Stabilization of the tautomers HP(OH)2 and P(OH)3 of hypophosphorous and phosphorous acids as ligands.
Authors of publication	Akbayeva, Dina N.; Di Vaira, Massimo; Costantini, Stefano Seniori; Peruzzini, Maurizio; Stoppioni, Piero
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2006
Journal issue	2
Pages of publication	389 - 395
a	13.666 ± 0.003 Å
b	22.517 ± 0.004 Å
c	14.244 ± 0.003 Å
α	90°
β	91.91 ± 0.02°
γ	90°
Cell volume	4380.7 ± 1.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1164
Residual factor for significantly intense reflections	0.0747
Weighted residual factors for significantly intense reflections	0.206
Weighted residual factors for all reflections included in the refinement	0.2331
Goodness-of-fit parameter for all reflections included in the refinement	0.941
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179768 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/64.	7006427.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7006427.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7006427.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7006427.cif