Crystallography Open Database

Information card for entry 7006443

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Coordinates	7006443.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H58 K2 O2 Si6
Calculated formula	C22 H58 K2 O2 Si6
Title of publication	Alkali metal complexes of sterically hindered mono- and di-carbanions containing Si-O bonds.
Authors of publication	Bowman, Lyndsey J.; Izod, Keith; Clegg, William; Harrington, Ross W.; Smith, J. David; Eaborn, C.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2006
Journal issue	3
Pages of publication	502 - 508
a	15.3506 ± 0.0007 Å
b	11.8073 ± 0.0005 Å
c	20.1478 ± 0.0009 Å
α	90°
β	98.5763 ± 0.0007°
γ	90°
Cell volume	3610.9 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0623
Residual factor for significantly intense reflections	0.0454
Weighted residual factors for significantly intense reflections	0.1212
Weighted residual factors for all reflections included in the refinement	0.1368
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179768 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/64.	7006443.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7006443.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7006443.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7006443.cif