Crystallography Open Database

Information card for entry 7008137

Preview

Coordinates	7008137.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	AsBr4(+)(Al(OR)4)(-) (R = C(CF3)3)
Chemical name	AsBr4(+)[Al(OR)4](-) (R = C(CF3)3)
Formula	C16 Al As Br4 F36 O4
Calculated formula	C16 Al As Br4 F36 O4
Title of publication	Preparation of stable AsBr4+ and I2As-PI3+ salts. Why didn't we succeed to prepare AsI4+ and As2X5+? A combined experimental and theoretical study.
Authors of publication	Gonsior, Marcin; Krossing, Ingo
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	7
Pages of publication	1203 - 1213
a	19.062 ± 0.004 Å
b	13.874 ± 0.003 Å
c	13.588 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	3593.6 ± 1.3 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0925
Residual factor for significantly intense reflections	0.0394
Weighted residual factors for significantly intense reflections	0.0861
Weighted residual factors for all reflections included in the refinement	0.1022
Goodness-of-fit parameter for all reflections included in the refinement	0.855
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179785 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/81.	7008137.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008137.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008137.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7008137.cif