Crystallography Open Database

Information card for entry 7008316

Preview

Coordinates	7008316.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C323 H314 Cu48 O2 P18 S24
Calculated formula	C323 H314 Cu48 O2 P18 S24
Title of publication	Functionalised trimethylsilyl reagents in cluster synthesis: reactions of Ph2P(S)SSiMe3 with group 11 salts.
Authors of publication	Shafaei-Fallah, Maryam; Anson, Christopher E.; Fenske, Dieter; Rothenberger, Alexander
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	13
Pages of publication	2300 - 2304
a	29.874 ± 0.005 Å
b	33.135 ± 0.006 Å
c	37.402 ± 0.005 Å
α	90°
β	110.237 ± 0.012°
γ	90°
Cell volume	34738 ± 10 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1042
Residual factor for significantly intense reflections	0.0616
Weighted residual factors for significantly intense reflections	0.1559
Weighted residual factors for all reflections included in the refinement	0.1789
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179787 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/83.	7008316.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008316.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008316.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7008316.cif