Crystallography Open Database

Information card for entry 7008320

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Coordinates	7008320.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H56 Cl N2 Sm
Calculated formula	C39 H56 Cl N2 Sm
Title of publication	Synthesis and characterization of mono beta-diketiminatosamarium amides and hydrocarbyls.
Authors of publication	Cui, Chunming; Shafir, Alexandr; Schmidt, Joseph A. R.; Oliver, Allen G.; Arnold, John
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	8
Pages of publication	1387 - 1393
a	10.6492 ± 0.0004 Å
b	12.0177 ± 0.0005 Å
c	15.7839 ± 0.0006 Å
α	104.152 ± 0.001°
β	97.11°
γ	106.841 ± 0.001°
Cell volume	1833.02 ± 0.13 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0361
Residual factor for significantly intense reflections	0.0332
Weighted residual factors for significantly intense reflections	0.0859
Weighted residual factors for all reflections included in the refinement	0.088
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179787 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/83.	7008320.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008320.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008320.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7008320.cif