Crystallography Open Database

Information card for entry 7008453

Preview

Coordinates	7008453.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H42 Cl4 N4 P2 Pt
Calculated formula	C42 H42 Cl4 N4 P2 Pt
Title of publication	The first examples of metal-mediated addition of a phosphorus imine to nitriles; the preparation and X-ray crystal structures of [PtCl4{NH=C(Et)N=PPh3}2] and [PtCl2(EtCN){NH=C(Et)N[double bond, length as m-dash]PPh3}].
Authors of publication	Bokach, Nadezhda A.; Kukushkin, Vadim Yu; Kelly, Paul F.; Haukka, Matti; Pombeiro, Armando J. L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	8
Pages of publication	1354 - 1356
a	10.121 ± 0.0002 Å
b	13.7987 ± 0.0004 Å
c	15.6217 ± 0.0004 Å
α	73.89 ± 0.001°
β	86.897 ± 0.002°
γ	89.625 ± 0.002°
Cell volume	2092.85 ± 0.09 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0468
Residual factor for significantly intense reflections	0.0301
Weighted residual factors for significantly intense reflections	0.0695
Weighted residual factors for all reflections included in the refinement	0.0761
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179788 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/84.	7008453.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008453.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008453.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7008453.cif