Crystallography Open Database

Information card for entry 7008458

Preview

Coordinates	7008458.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H41 Cl3 F10 N6 O6 Pd2
Calculated formula	C33 H41 Cl3 F10 N6 O6 Pd2
Title of publication	Pentafluorophenyl imidato palladium(II) complexes: catalysts for Suzuki cross-coupling reactions.
Authors of publication	Ruiz, José; Vicente, Consuelo; Cutillas, Natalia; Pérez, José
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	11
Pages of publication	1999 - 2006
a	15.288 ± 0.001 Å
b	14.317 ± 0.001 Å
c	20.788 ± 0.001 Å
α	90°
β	107 ± 0.01°
γ	90°
Cell volume	4351.2 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.074
Residual factor for significantly intense reflections	0.045
Weighted residual factors for significantly intense reflections	0.1154
Weighted residual factors for all reflections included in the refinement	0.1309
Goodness-of-fit parameter for all reflections included in the refinement	0.774
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179788 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/84.	7008458.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008458.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008458.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7008458.cif