Crystallography Open Database

Information card for entry 7008913

Preview

Coordinates	7008913.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H20 Cl Si
Calculated formula	C19 H20 Cl Si
Title of publication	A novel α,ω silyl dianionic salt. The synthesis and characterization of remotely connected benzannulated silole monoanions
Authors of publication	Choi, Seok-Bong; Boudjouk, Philip
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	6
Pages of publication	841
a	8.9575 ± 0.001 Å
b	9.4809 ± 0.0011 Å
c	11.2364 ± 0.0013 Å
α	98.377 ± 0.002°
β	112.958 ± 0.002°
γ	96.817 ± 0.002°
Cell volume	853 ± 0.17 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1135
Residual factor for significantly intense reflections	0.0696
Weighted residual factors for significantly intense reflections	0.152
Weighted residual factors for all reflections included in the refinement	0.1913
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179793 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/89.	7008913.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008913.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008913.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7008913.cif