Crystallography Open Database

Information card for entry 7009098

Preview

Coordinates	7009098.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43.5 H73 As Li N2 O P3
Calculated formula	C43.5 H73 As Li N2 O P3
Title of publication	A synthetic and structural study of the formation of cyclic [(RP)nE]− anions and Zintl compounds using E(NMe2)3 (E = As, Sb)
Authors of publication	Bashall, Alan; Beswick, Michael A.; Choi, Nick; Hopkins, Alexander D.; Kidd, Sara J.; Lawson, Yvonne G.; Mosquera, Marta E. G.; McPartlin, Mary; Raithby, Paul R.; Wheatley, Andrew A. E. H.; Wood, Jody A.; Wright, Dominic S.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	4
Pages of publication	479
a	12.518 ± 0.006 Å
b	17.347 ± 0.004 Å
c	11.166 ± 0.004 Å
α	100.07 ± 0.02°
β	112.31 ± 0.03°
γ	79.9 ± 0.03°
Cell volume	2192.8 ± 1.5 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0763
Residual factor for significantly intense reflections	0.0518
Weighted residual factors for significantly intense reflections	0.1205
Weighted residual factors for all reflections included in the refinement	0.1328
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7009098.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009098.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009098.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009098.cif