Crystallography Open Database

Information card for entry 7009250

Preview

Coordinates	7009250.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	compound 6d(Ni)
Formula	C38 H46 Cl4 Co2 N2 Ni2 O26 P6
Calculated formula	C38 H28 Cl4 Co2 N2 Ni2 O26 P6
Title of publication	An entry to half-sandwich complexes of first row transition metals (Ni, Co, Mn) containing the Kläui tripodal ligand, LOMe: synthesis and crystal structures of oligomeric, [LOMeM(μ-X)(L)]n (n = 2, 4), and monomeric complexes, LOMeM(L2)(X)
Authors of publication	De-qiang Ma; Shiro Hikichi; Munetaka Akita; Yoshihiko Moro-oka
Journal of publication	J. Chem. Soc., Dalton Trans.
Year of publication	2000
Journal issue	7
Pages of publication	1123 - 1134
a	14.389 ± 0.004 Å
b	18.824 ± 0.003 Å
c	14.313 ± 0.01 Å
α	112.36 ± 0.007°
β	119.89 ± 0.03°
γ	88.509 ± 0.013°
Cell volume	3043 ± 3 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1099
Residual factor for significantly intense reflections	0.1039
Weighted residual factors for significantly intense reflections	0.2765
Weighted residual factors for all reflections included in the refinement	0.2839
Goodness-of-fit parameter for all reflections included in the refinement	2.267
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179796 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/92.	7009250.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009250.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009250.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009250.cif