Crystallography Open Database

Information card for entry 7009412

Preview

Coordinates	7009412.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H24 Li N O
Calculated formula	C19 H24 Li N O
Title of publication	Solid state structures of the chiral lithium amide complexes (S )-[(Ph(Me)CH)(PhCH2)NLi·thf]2 and (R)-[(Ph(Me)CH)(PhCH2)NLi·pmdta] †
Authors of publication	Andrews, Philip C.; Duggan, Peter J.; Fallon, Gary D.; McCarthy, Tom D.; Peatt, Anna C.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	12
Pages of publication	1937
a	11.527 ± 0.001 Å
b	11.527 ± 0.001 Å
c	25.481 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	3385.7 ± 0.4 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	96
Hermann-Mauguin space group symbol	P 43 21 2
Hall space group symbol	P 4nw 2abw
Residual factor for all reflections	0.0981
Residual factor for significantly intense reflections	0.0682
Weighted residual factors for significantly intense reflections	0.1178
Weighted residual factors for all reflections included in the refinement	0.127
Goodness-of-fit parameter for all reflections included in the refinement	1.082
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179798 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/94.	7009412.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009412.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009412.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009412.cif