Crystallography Open Database

Information card for entry 7009637

Preview

Coordinates	7009637.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H6 Fe2 O17 Ru3 W
Calculated formula	C26 H6 Fe1.999 O17 Ru3.001 W
Title of publication	Syntheses and reactions of some cluster complexes containing C4 ligands with iron, ruthenium and cobalt carbonyls
Authors of publication	Bruce, Michael I.; Low, Paul J.; Zaitseva, Natasha N.; Kahlal, Samia; Halet, Jean-François; Skelton, Brian W.; White, Allan H.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	17
Pages of publication	2939
a	8.442 ± 0.002 Å
b	23.94 ± 0.005 Å
c	16.422 ± 0.003 Å
α	90°
β	90.941 ± 0.005°
γ	90°
Cell volume	3318.5 ± 1.2 Å³
Cell temperature	153 K
Ambient diffraction temperature	153 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.075
Residual factor for significantly intense reflections	0.039
Weighted residual factors for all reflections	0.047
Weighted residual factors for all reflections included in the refinement	0.042
Goodness-of-fit parameter for all reflections	1.044
Goodness-of-fit parameter for all reflections included in the refinement	1.177
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	7009637.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009637.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009637.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009637.cif