Crystallography Open Database

Information card for entry 7009656

Preview

Coordinates	7009656.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Li(tmeda)2][(tsi)Al(StBu)3].2.5(benzene)
Formula	C49 H101 Al Li N4 S3 Si3
Calculated formula	C49 H101 Al Li N4 S3 Si3
Title of publication	Syntheses and crystal structures of some lithium di- and tri-(thiolato)[tris(trimethylsilyl)methyl]aluminates
Authors of publication	Chen, Wu-Yong; Eaborn, Colin; Gorrell, Ian B.; Hitchcock, Peter B.; Smith, J. David
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	14
Pages of publication	2313
a	34.256 ± 0.007 Å
b	11.863 ± 0.003 Å
c	30.519 ± 0.004 Å
α	90°
β	99.88 ± 0.02°
γ	90°
Cell volume	12218 ± 4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1906
Residual factor for significantly intense reflections	0.086
Weighted residual factors for significantly intense reflections	0.166
Weighted residual factors for all reflections included in the refinement	0.2114
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179800 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/96.	7009656.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009656.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009656.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009656.cif