Crystallography Open Database

Information card for entry 7009689

Preview

Coordinates	7009689.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H38 N2 Nb Si3
Calculated formula	C17 H38 N2 Nb Si3
Title of publication	Synthesis and structural characterization of new organo-diimido and organo-imido niobium and titanium complexes
Authors of publication	Dorado, Iván; Garcés, Andrés; López-Mardomingo, Carmen; Fajardo, Mariano; Rodríguez, Ana; Antiñolo, Antonio; Otero, Antonio
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	14
Pages of publication	2375
a	19.306 ± 0.008 Å
b	16.0717 ± 0.0007 Å
c	19.428 ± 0.004 Å
α	90°
β	117.19 ± 0.02°
γ	90°
Cell volume	5362 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.2174
Residual factor for significantly intense reflections	0.08
Weighted residual factors for significantly intense reflections	0.1545
Weighted residual factors for all reflections included in the refinement	0.2417
Goodness-of-fit parameter for all reflections included in the refinement	1.008
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179800 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/96.	7009689.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009689.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009689.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009689.cif