Crystallography Open Database

Information card for entry 7009964

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Coordinates	7009964.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H20 F6 N4 O2 Os P
Calculated formula	C26 H20 F6 N4 O2 Os P
SMILES	[P](F)(F)(F)(F)(F)[F-].c12cccc[n]2[Os]23([n]4c1cccc4)(Oc1ccccc1O3)[n]1c(cccc1)c1cccc[n]21
Title of publication	Polynuclear osmium‒dioxolene complexes: comparison of electrochemical and spectroelectrochemical properties with those of their ruthenium analogues
Authors of publication	Barthram, Anita M.; Reeves, Zöe R.; Jeffery, John C.; Ward, Michael D.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	18
Pages of publication	3162
a	11.8056 ± 0.0014 Å
b	14.869 ± 0.003 Å
c	14.909 ± 0.003 Å
α	90 ± 0.011°
β	104.011 ± 0.01°
γ	90 ± 0.014°
Cell volume	2539.2 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0252
Residual factor for significantly intense reflections	0.0224
Weighted residual factors for significantly intense reflections	0.0545
Weighted residual factors for all reflections included in the refinement	0.0549
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179803 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/99.	7009964.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009964.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009964.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009964.cif