Crystallography Open Database

Information card for entry 7010213

Preview

Coordinates	7010213.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H38 N4 Sb2
Calculated formula	C32 H38 N4 Sb2
SMILES	c1c(C)c(N[Sb]2N(c3c(cccc3C)C)[Sb](Nc3c(cccc3C)C)N2c2c(cccc2C)C)c(cc1)C
Title of publication	Antimony imido and imido‒amido compounds: a new route to an imidoantimony macrocycle
Authors of publication	Bryant, Richard; James, Siân C.; Jeffery, John C.; Norman, Nicholas C.; Orpen, A. Guy; Weckenmann, Ulrike
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	22
Pages of publication	4007
a	7.9276 ± 0.0019 Å
b	10.012 ± 0.003 Å
c	11.075 ± 0.004 Å
α	101 ± 0.02°
β	110.705 ± 0.014°
γ	107.892 ± 0.014°
Cell volume	736.9 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0417
Residual factor for significantly intense reflections	0.0337
Weighted residual factors for significantly intense reflections	0.0684
Weighted residual factors for all reflections included in the refinement	0.0735
Goodness-of-fit parameter for all reflections included in the refinement	1.117
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179806 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/02.	7010213.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7010213.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7010213.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7010213.cif