Crystallography Open Database

Information card for entry 7010434

Preview

Coordinates	7010434.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H56 Ag B F4 O11 P2
Calculated formula	C44 H52 Ag0.5 B F4 O11 P2
Title of publication	Calix[4]arene-derived diphosphines, diphosphinites and diphosphites as chelating ligands for transition metal ions. Encapsulation of silver(I) in a calix-crown diphosphite
Authors of publication	Jeunesse, Catherine; Dieleman, Cedric; Steyer, Stéphane; Matt, Dominique
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	6
Pages of publication	881
a	11.9325 ± 0.0002 Å
b	17.6619 ± 0.0002 Å
c	21.2455 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	4477.5 ± 0.11 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	7
Space group number	56
Hermann-Mauguin space group symbol	P c c n
Hall space group symbol	-P 2ab 2ac
Residual factor for all reflections	0.066
Residual factor for significantly intense reflections	0.049
Weighted residual factors for all reflections	0.101
Weighted residual factors for all reflections included in the refinement	0.062
Goodness-of-fit parameter for all reflections	1.757
Goodness-of-fit parameter for all reflections included in the refinement	1.158
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	Mo-Kα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179808 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/04.	7010434.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7010434.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7010434.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7010434.cif