Crystallography Open Database

Information card for entry 7010609

Preview

Coordinates	7010609.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H72 Ga2 K2 N8
Calculated formula	C32 H72 Ga2 K2 N8
Title of publication	In further pursuit of the carbene analogy: preparation and crystal structure of (N,N,N ',N '-tetramethylethylenediamine)potassium [cis-ethene-1,2-di(tert-butylamido)]gallate(I)
Authors of publication	Schmidt, Eva Susanne; Schier, Annette; Schmidbaur, Hubert
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	5
Pages of publication	505
a	10.3925 ± 0.0002 Å
b	10.7648 ± 0.0002 Å
c	10.9534 ± 0.0003 Å
α	101.728 ± 0.001°
β	92.051 ± 0.001°
γ	114.45 ± 0.001°
Cell volume	1082.28 ± 0.04 Å³
Cell temperature	143 ± 2 K
Ambient diffraction temperature	143 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0333
Residual factor for significantly intense reflections	0.0309
Weighted residual factors for significantly intense reflections	0.074
Weighted residual factors for all reflections included in the refinement	0.0753
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
213973 (current)	2019-03-05	cod/ Removed potentially copyrighted or irrelevant data items from 1289 entries.	7010609.cif
179810	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/06.	7010609.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7010609.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7010609.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7010609.cif