Crystallography Open Database

Information card for entry 7010663

Preview

Coordinates	7010663.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H36 Cl3 Ir2 N6 O12 S6 V
Calculated formula	C12 H36 Cl3 Ir2 N6 O12 S6 V
Title of publication	Synthesis, characterization and reactivity of linear-type S-bridged trinuclear complexes containing vanadium(III) ion. Crystal structures of [VIII{M(aet)3}2](ClO4)3 (M = RhIII, IrIII; aet = 2-aminoethanethiolate)†
Authors of publication	Miyashita, Yoshitaro; Hamajima, Masato; Yamada, Yasunori; Fujisawa, Kiyoshi; Okamoto, Ken-ichi
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	14
Pages of publication	2089
a	14.578 ± 0.009 Å
b	14.578 ± 0.009 Å
c	26.47 ± 0.02 Å
α	90°
β	90°
γ	120°
Cell volume	4872 ± 6 Å³
Cell temperature	296.2 K
Number of distinct elements	8
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for significantly intense reflections	0.0417
Weighted residual factors for all reflections included in the refinement	0.0474
Goodness-of-fit parameter for all reflections included in the refinement	1.36
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7010663.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7010663.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7010663.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7010663.cif