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Information card for entry 7010732
Preview
| Coordinates | 7010732.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | Bromodimethyl(2-diphenylphosphinoethyl-C,O)stannane |
|---|---|
| Formula | C16 H20 Br O P Sn |
| Calculated formula | C16 H20 Br O P Sn |
| SMILES | [Sn]1(Br)([O]=P(CC1)(c1ccccc1)c1ccccc1)(C)C |
| Title of publication | Monomer‒polymer forms of solid, unsolvated, 5-coordinate halodimethyl(2-diphenylphosphinylethyl)stannanes, XMe2SnCH2CH2P(O)Ph2 (X = Cl, Br or I). Effects of different recrystallisation media |
| Authors of publication | Harrison, William T. A.; Howie, R. Alan; Munro, Craig M.; Wardell, James L. |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2001 |
| Journal issue | 18 |
| Pages of publication | 2593 |
| a | 9.815 ± 0.0004 Å |
| b | 15.2192 ± 0.0007 Å |
| c | 12.8056 ± 0.0006 Å |
| α | 90° |
| β | 109.608 ± 0.001° |
| γ | 90° |
| Cell volume | 1801.93 ± 0.14 Å3 |
| Cell temperature | 301 ± 2 K |
| Ambient diffraction temperature | 301 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/a 1 |
| Hall space group symbol | -P 2yab |
| Residual factor for all reflections | 0.0329 |
| Residual factor for significantly intense reflections | 0.0239 |
| Weighted residual factors for significantly intense reflections | 0.0584 |
| Weighted residual factors for all reflections included in the refinement | 0.061 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 213973 (current) | 2019-03-05 | cod/ Removed potentially copyrighted or irrelevant data items from 1289 entries. |
7010732.cif |
| 179811 | 2016-03-25 | cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/07. |
7010732.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7010732.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7010732.cif |
| 3896 | 2010-12-08 | cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/. |
7010732.cif |
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