Crystallography Open Database

Information card for entry 7011015

Preview

Coordinates	7011015.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H32 N8 O22 P2 Pu1.5
Calculated formula	C36 H32 N8 O22 P2 Pu1.5
Title of publication	Synthesis and crystal structure of a ten-coordinate plutonium(iv) ion complexed by 2-[(diphenylphosphino)methyl]pyridine N,P-dioxide: [Pu(NO3)3{2-[(C6H5)2P(O)CH2]C5H4NO}2][Pu(NO3)6]0.5
Authors of publication	Matonic, John H.; Neu, Mary P.; Enriquez, Alejandro E.; Paine, Robert T.; Scott, Brian L.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	11
Pages of publication	2328
a	12.0407 ± 0.0006 Å
b	14.2228 ± 0.0007 Å
c	15.6363 ± 0.0007 Å
α	65.195 ± 0.001°
β	80.571 ± 0.001°
γ	72.381 ± 0.001°
Cell volume	2314.58 ± 0.19 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0318
Residual factor for significantly intense reflections	0.0256
Weighted residual factors for significantly intense reflections	0.0601
Weighted residual factors for all reflections included in the refinement	0.0632
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7011015.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7011015.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7011015.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7011015.cif