Crystallography Open Database

Information card for entry 7011488

Preview

Coordinates	7011488.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H30 Cl4 N4
Calculated formula	C17 H30 Cl4 N4
Title of publication	Bidentate N-heterocyclic carbene complexes of Group 13 trihydrides and trihalides
Authors of publication	Baker, Robert J.; Cole, Marcus L.; Jones, Cameron; Mahon, Mary F.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	9
Pages of publication	1992
a	13.401 ± 0.003 Å
b	15.748 ± 0.003 Å
c	11.461 ± 0.002 Å
α	90°
β	109.4 ± 0.03°
γ	90°
Cell volume	2281.4 ± 0.9 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0375
Residual factor for significantly intense reflections	0.0311
Weighted residual factors for significantly intense reflections	0.0742
Weighted residual factors for all reflections included in the refinement	0.0771
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
213973 (current)	2019-03-05	cod/ Removed potentially copyrighted or irrelevant data items from 1289 entries.	7011488.cif
179818	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/14.	7011488.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7011488.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7011488.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7011488.cif