Crystallography Open Database

Information card for entry 7011539

Preview

Coordinates	7011539.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H38 Cl2 N2 O4 P Rh S3
Calculated formula	C32 H38 Cl2 N2 O4 P Rh S3
Title of publication	Reactivity of Rh(i) and Rh(iii) complexes containing a PNO hydrazonic ligand toward HCl
Authors of publication	Pelagatti, Paolo; Bacchi, Alessia; Bobbio, Carla; Carcelli, Mauro; Costa, Mirco; Fochi, Andrea; Pelizzi, Corrado
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	8
Pages of publication	1820
a	13.939 ± 0.005 Å
b	12.862 ± 0.005 Å
c	20.133 ± 0.005 Å
α	90°
β	92.1 ± 0.05°
γ	90°
Cell volume	3607 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0871
Residual factor for significantly intense reflections	0.0606
Weighted residual factors for significantly intense reflections	0.1728
Weighted residual factors for all reflections included in the refinement	0.1973
Goodness-of-fit parameter for all reflections included in the refinement	0.934
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
213973 (current)	2019-03-05	cod/ Removed potentially copyrighted or irrelevant data items from 1289 entries.	7011539.cif
179819	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/15.	7011539.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7011539.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7011539.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7011539.cif