Crystallography Open Database

Information card for entry 7011688

Preview

Coordinates	7011688.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H39 As F6 P2 Pd
Calculated formula	C18 H39 As F6 P2 Pd
Title of publication	Mono- and di-nuclear palladium(ii) complexes with bulky arsino(phosphino)methanes in different coordination modes
Authors of publication	Schmidt, Ulrich; Ilg, Kerstin; Brandt, Carsten D.; Werner, Helmut
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	14
Pages of publication	2815
a	9.0217 ± 0.0018 Å
b	17.072 ± 0.003 Å
c	9.0882 ± 0.0018 Å
α	90°
β	113.81 ± 0.03°
γ	90°
Cell volume	1280.6 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0278
Residual factor for significantly intense reflections	0.0251
Weighted residual factors for significantly intense reflections	0.061
Weighted residual factors for all reflections included in the refinement	0.062
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
213973 (current)	2019-03-05	cod/ Removed potentially copyrighted or irrelevant data items from 1289 entries.	7011688.cif
179820	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/16.	7011688.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7011688.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7011688.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7011688.cif