Crystallography Open Database

Information card for entry 7016048

Preview

Coordinates	7016048.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44.5 H119 Ge9 Li Mo N4 O3 Si12
Calculated formula	C44.5 H119 Ge9 Li Mo N4 O3 Si12
Title of publication	[Si(SiMe(3))(3)](3)Ge(9)M(CO)(3)(-) (M = Cr, Mo, W): Coordination Chemistry with metalloid Clusters.
Authors of publication	Henke, Florian; Schenk, Christian; Schnepf, Andreas
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	25
Pages of publication	6704 - 6710
a	25.696 ± 0.004 Å
b	25.696 ± 0.004 Å
c	26.818 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	17708 ± 5 Å³
Cell temperature	149 ± 2 K
Ambient diffraction temperature	149 ± 2 K
Number of distinct elements	8
Space group number	114
Hermann-Mauguin space group symbol	P -4 21 c
Hall space group symbol	P -4 2n
Residual factor for all reflections	0.1695
Residual factor for significantly intense reflections	0.0677
Weighted residual factors for significantly intense reflections	0.1029
Weighted residual factors for all reflections included in the refinement	0.1309
Goodness-of-fit parameter for all reflections included in the refinement	0.801
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7016048.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7016048.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7016048.cif
23615	2011-08-09	../uploads/cif-deposit/cod/cif Adding structures of 7016048, 7016049, 7016050, 7016051 via cif-deposit CGI script.	7016048.cif