Crystallography Open Database

Information card for entry 7021137

Preview

Coordinates	7021137.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H34 Ag2 F12 N8 O P2 S
Calculated formula	C32 H34 Ag2 F12 N8 O P2 S
Title of publication	Synthesis of polynuclear Ag(i) and Au(i) complexes from macrocyclic tetraimidazolium salts.
Authors of publication	Schulte To Brinke, Christian; Pape, Tania; Hahn, F. Ekkehardt
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	20
Pages of publication	7330 - 7337
a	11.1472 ± 0.0006 Å
b	14.5134 ± 0.0007 Å
c	31.8567 ± 0.0012 Å
α	90°
β	99.567 ± 0.003°
γ	90°
Cell volume	5082.2 ± 0.4 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.087
Residual factor for significantly intense reflections	0.0744
Weighted residual factors for significantly intense reflections	0.1988
Weighted residual factors for all reflections included in the refinement	0.2119
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179916 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/11.	7021137.cif
86041	2013-05-09	cif/ Adding structures of 7021135, 7021136, 7021137, 7021138, 7021139, 7021140 via cif-deposit CGI script.	7021137.cif