Crystallography Open Database

Information card for entry 7021593

Preview

Coordinates	7021593.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H67 B N3 Si6 U
Calculated formula	C26 H67 B N3 Si6 U
Title of publication	Uranium(iv) amido-borohydrides as highly active diene polymerisation catalysts.
Authors of publication	Mansell, Stephen M.; Bonnet, Fanny; Visseaux, Marc; Arnold, Polly L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	25
Pages of publication	9033 - 9039
a	18.1815 ± 0.0004 Å
b	12.0062 ± 0.0002 Å
c	18.7241 ± 0.0004 Å
α	90°
β	101.721 ± 0.002°
γ	90°
Cell volume	4002.07 ± 0.14 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1132
Residual factor for significantly intense reflections	0.1109
Weighted residual factors for significantly intense reflections	0.2793
Weighted residual factors for all reflections included in the refinement	0.2806
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179920 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/15.	7021593.cif
87134	2013-07-14	cif/ Adding structures of 7021593, 7021594 via cif-deposit CGI script.	7021593.cif