Crystallography Open Database

Information card for entry 7022002

7022001 << 7022002 >> 7022003

Preview

Coordinates	7022002.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H66 K2 N4 O2
Calculated formula	C44 H66 K2 N4 O2
SMILES	[K]123([O](CC)CC)[N]4(c5c(cccc5C(C)C)C(C)C)c5[n]1(c(ccc5)C)[K]41([O](CC)CC)[N]2(c2c(cccc2C(C)C)C(C)C)c2[n]13c(ccc2)C
Title of publication	Divalent europium and ytterbium complexes supported by a bulky 2-pyridyl amido ligand: synthesis, structure and reactivity studies.
Authors of publication	Ku, Ka Wai; Au, Chi Wai; Chan, Hoi-Shan; Lee, Hung Kay
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	8
Pages of publication	2841 - 2852
a	10.2513 ± 0.0009 Å
b	11.083 ± 0.0009 Å
c	11.6691 ± 0.001 Å
α	62.187 ± 0.001°
β	89.257 ± 0.002°
γ	77.994 ± 0.002°
Cell volume	1141.54 ± 0.17 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0722
Residual factor for significantly intense reflections	0.052
Weighted residual factors for significantly intense reflections	0.1368
Weighted residual factors for all reflections included in the refinement	0.1517
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179925 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/20.	7022002.cif
89943	2013-11-17	cif/ Adding structures of 7022002, 7022003, 7022004, 7022005, 7022006, 7022007, 7022008 via cif-deposit CGI script.	7022002.cif