Crystallography Open Database

Information card for entry 7022005

7022004 << 7022005 >> 7022006

Preview

Coordinates	7022005.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H69 N6 Sm
Calculated formula	C54 H69 N6 Sm
SMILES	c1(c(cccc1C(C)C)C(C)C)N1c2[n](c(ccc2)C)[Sm]231(N(c1c(cccc1C(C)C)C(C)C)c1[n]2c(ccc1)C)N(c1c(cccc1C(C)C)C(C)C)c1[n]3c(ccc1)C
Title of publication	Divalent europium and ytterbium complexes supported by a bulky 2-pyridyl amido ligand: synthesis, structure and reactivity studies.
Authors of publication	Ku, Ka Wai; Au, Chi Wai; Chan, Hoi-Shan; Lee, Hung Kay
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	8
Pages of publication	2841 - 2852
a	12.673 ± 0.002 Å
b	12.673 ± 0.002 Å
c	18.424 ± 0.003 Å
α	90°
β	90°
γ	120°
Cell volume	2562.6 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	147
Hermann-Mauguin space group symbol	P -3
Hall space group symbol	-P 3
Residual factor for all reflections	0.0451
Residual factor for significantly intense reflections	0.0336
Weighted residual factors for significantly intense reflections	0.0846
Weighted residual factors for all reflections included in the refinement	0.1025
Goodness-of-fit parameter for all reflections included in the refinement	1.143
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179925 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/20.	7022005.cif
89943	2013-11-17	cif/ Adding structures of 7022002, 7022003, 7022004, 7022005, 7022006, 7022007, 7022008 via cif-deposit CGI script.	7022005.cif