Crystallography Open Database

Information card for entry 7022015

7022014 << 7022015 >> 7022016

Preview

Coordinates	7022015.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C168 H162 Cl21 P12 Pd6 Te4
Calculated formula	C168 H162 Cl21 P12 Pd6 Te4
Title of publication	Reactivity of 2-chalcogenopyridines with palladium-phosphine complexes: isolation of different complexes depending on the nature of chalcogen atom and phosphine ligand.
Authors of publication	Chauhan, Rohit Singh; Kedarnath, G.; Wadawale, Amey; Slawin, Alexandra M. Z.; Jain, Vimal K.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	1
Pages of publication	259 - 269
a	14.2448 ± 0.0004 Å
b	18.8456 ± 0.0006 Å
c	18.9875 ± 0.0005 Å
α	81.392 ± 0.002°
β	83.613 ± 0.002°
γ	69.894 ± 0.003°
Cell volume	4722.9 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1837
Residual factor for significantly intense reflections	0.0958
Weighted residual factors for significantly intense reflections	0.1997
Weighted residual factors for all reflections included in the refinement	0.2258
Goodness-of-fit parameter for all reflections included in the refinement	1.177
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179925 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/20.	7022015.cif
89945	2013-11-17	cif/ Adding structures of 7022012, 7022013, 7022014, 7022015 via cif-deposit CGI script.	7022015.cif